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32results about How to "Good density" patented technology

Method for comprehensively recycling valuable minerals in rare-earth tailings

InactiveCN103394408ATake advantage ofOptimized flotation collectionFlotationWet separationResource utilizationNiobium
The invention relates to a method for comprehensively recycling valuable compositions of rare earth, iron, niobium and fluorite in rare-earth tailings, and belongs to the fields of comprehensive resource utilization technologies and mineral processing engineering. The rare earth, the iron, the niobium and the fluorite in the rare-earth tailings are efficiently and comprehensively recycled by the method including 'grinding the rare-earth tailings, performing low-intensity magnetic separation, performing high-intensity magnetic separation on weak-intensity magnetic tailings, performing flotation on high-intensity magnetic tailings to obtain fluorite in the high-intensity magnetic tailings, performing flotation separation on high-intensity magnetic concentrates to obtain rare earth, iron and niobium in the high-intensity magnetic concentrates, reducing and roasting base flows, performing low-intensity magnetic separation to obtain iron and niobium in the base flows and performing flotation on low-intensity magnetic tailings to obtain niobium in the low-intensity magnetic tailings according to characteristics that the rare-earth tailings contain the various valuable compositions. Compared with a method for singly recycling one or two valuable compositions, the method has the advantages that the purpose of comprehensively recycling the valuable compositions in the rare-earth tailings can be effectively achieved, secondary resources can be sufficiently utilized, and the method has excellent economical and social benefits.
Owner:UNIV OF SCI & TECH BEIJING

Graphite crucible

The invention provides a graphite crucible and relates to a crucible. The graphite crucible has a size of Phi (1200-1500)mm, an inner diameter of Phi (960-1260)mm and a depth of (1750-1900)mm. The graphite crucible is acquired based on the following steps: adding accessories into a raw material of forged petroleum coke grains, thereby acquiring a mixture; crushing the mixture, adding the mixture into a mixing kneading pot and stirring; adding liquid pitch into the mixing kneading pot and wetting the petroleum coke grains with the pitch; after molding a crucible blank, putting the crucible blank into a crucible roaster for roasting, thereby acquiring a roasted crucible product; steeping the roasted crucible product, thereby acquiring a steeped crucible; and graphitizing the steeped crucible, thereby acquiring the graphite crucible. The graphite crucible is once formed and the surface thereof is directly extruded and rubbed by a grinding tool, so that the compactness of the graphite crucible is better and pores are few. The graphite crucible is subjected to twice high-pressure steeping, so that the surface of the graphite crucible is more compact, the liquid metal is difficult to immerse and the service life is long. A test proves that physicochemical indexes of the acquired graphite crucible are as follows: the volume density is more than 1.75g/cm<3> and the compression strength reaches 25MPa.
Owner:福建兴朝阳硅材料股份有限公司

Sample preparation method and compaction device for immature soil base materials

The invention discloses a sample preparation method and a compaction device for immature soil base materials. The method comprises the steps that the interior of a mold is coated with a lubricating oil layer, the immature soil base materials are put into the mold layer by layer, the immature soil base material layers in the mold are compacted through a jack every time one layer of immature soil base material is laid, and therefore a sample to be detected is obtained; the compaction speed of the jack is 0.5 mm/s, the compaction pressure of the jack is 18-19 K/N, and the compaction time of the jack is 3-5 min; the compaction device comprises a test bed, the test bed is sequentially provided with a first platform and a second platform in parallel in the horizontal direction from top to bottom, the second platform is coaxially provided with the jack, a gasket, the mold and a pressing column in sequence from bottom to top in the vertical direction, and the top end of the pressing column abuts against the first platform. Compared with a traditional hammer test, a press compaction test and a jack compaction test, the compressive strength of a test piece compacted by the jack is more stable than the compressive strength of a test piece compacted by the other two test methods, test piece overall deformation is good, and the test piece has good ductility when compacted.
Owner:CHANGAN UNIV

Method for producing lithium iron phosphate

The invention discloses a method for producing lithium iron phosphate without inert atmosphere protection, aiming at realizing the aim of reducing the manufacturing cost of positive material of a lithium iron phosphate battery. The method comprises the steps: the prepared precursor material is put into a semi-enclosed box body and pressed to be compact to exhaust the air in the precursor material; a high temperature resistant plate which is higher than the box body is arranged, and a gap is left between the high temperature resistant plate and the box body; then, the semi-enclosed box body and the high temperature resistant plate are arranged inside another semi-enclosed box body in a inverted way, and a carbon dust layer is filled into the box body; the high temperature resistant plate provided with the slim holes is laid on carbon dust or the gap is left between the high temperature resistant plate and the box body; the obtained semi-enclosed box body that is provided with the precursor and the carbon dust is firstly vacuumized and then filled with non-oxidizing gas for replacing the air in the precursor and the carbon dust; the box body is placed into a calcination device and heated from the room temperature to be 600-800 DEG C at the speed of 5-20 DEG C/min; after that, the temperature is maintained for 6-24h for calcination, and then the product is cooled to be the room temperature along with a furnace.
Owner:YUNNAN NENGTOU HUILONG TECH

Lithium zirconate ceramic ball tritium breeding material and preparation method thereof

The invention belongs to the technical field of nuclear energy and particularly relates to a lithium zirconate ceramic ball tritium breeding material and a preparation method thereof. According to the preparation method disclosed by the invention, an isostatic pressing method is adopted for preparing ceramic balls, and the density is higher than those prepared by rotational molding, wet process dehydration molding and wet process ZrO2 addition molding. The ceramic balls prepared by other methods are molded under the situation that external pressure does not exist, and the degree of compaction of components is lower than that of the isostatic pressing method. Simultaneously, the structure can release carbon dioxide during the sintering process, and the density of the balls is lower; and however, in the preparation method disclosed by the invention, powder is firstly prepared and can realize full reaction and release the carbon dioxide, and when the sintering of the ceramic balls is performed in the second step, the released carbon dioxide is very little, and the density of the prepared lithium zirconate ceramic balls is higher. In addition, if the density of the ceramic balls needs to be improved continuously, the pressure for isostatic pressing can be improved, and then the density of the obtained ceramic balls can be increased.
Owner:TSINGHUA UNIV

Barium magnesium niobate light-emitting ceramics and preparation method thereof

The invention relates to barium magnesium niobate light-emitting ceramics and a preparation method thereof.The formula of the barium magnesium niobate light-emitting ceramics is Ba(1-x)Smx(Sn0.1Mg0.3Mg0.3Nb0.6)O3, wherein 0.005</=x</=0.03.The preparation method includes the steps of firstly, performing ball milling on a barium-source compound, a samarium-source compound, a magnesium-source compound, a tin-source compound and a niobium-source compound according to the weight requirements of the formula, then sintering under 1300-1350 DEG C to obtain products, and performing secondary ball milling on the products to obtain ceramic powder; secondly, adding a polyvinyl alcohol aqueous solution into the ceramic powder for pelleting, aging, crushing to obtain ceramic particles, forming the ceramic particles to obtain ceramic bodies, and preparing the ceramic bodies into even-pressure ceramic bodies through isostatic cool pressing; thirdly, sintering the even-pressure ceramic bodies under oxygen atmosphere after the even-pressure ceramic bodies discharge glue, cooling along with a furnace, and coarsely polishing and finely polishing to obtain the barium magnesium niobate light-emitting ceramics, wherein sintering temperature is 1500-1600 DEG C, and the temperature is kept for 48-60 hours.The barium magnesium niobate light-emitting ceramics have the advantages that the crystal boundary of the ceramics has no impurity phases, and the ceramics are good in compactness, even in grain size, high in chemical stability, and good in physical performances such as compressive strength; the ceramics have evident absorption peak in the visible light range, the quenching concentration can reach 2%mol, and high light-emitting intensity is achieved.
Owner:WUHAN UNIV OF TECH

Silver-nickel alloy powder and preparation method thereof and conductive slurry including silver-nickel alloy powder

The invention discloses silver-nickel alloy powder. The particle size of nickel particles ranges from 0.1 micrometer to 5.0 micrometers, and silver accounts for 0% to 60% of the total weight of silverparticles and the nickel particles. A method for preparing the silver-nickel alloy powder comprises the steps that a reducing agent I is used firstly, the silver particles are primarily separated outon the surfaces of the nickel particles, and therefore a precursor is prepared; and then the precursor is in full contact with a dispersing agent, a complexing agent, the silver particles and a reducing agent II of the silver particles in deionized water, and therefore silver is further replaced and separated out on the surface of the precursor. A silver coating layer on the surfaces of the silver particles and the nickel particles prepared through the method is high in density and has fewer holes, and therefore surface oxidization of the nickel particles and resistance reduction of the silver-nickel alloy powder can be controlled well, it is guaranteed that the conductive performance of the silver-nickel alloy powder after long-time storage is still good, and the silver-nickel alloy powder can be applied to conductive slurry.
Owner:宁波广新纳米材料有限公司

Method for preparing SiC ceramic-based composite material from spongy silicon carbide nanofiber preform

The invention discloses a method for preparing a SiC ceramic-based composite material from a spongy silicon carbide nanofiber preform. The method comprises: filling a glass tube with a spongy SiCnf material, and pre-compressing the spongy SiCnf material by external force to obtain a pre-compressed body; soaking the pre-compressed body in a low-concentration phenolic resin solution, taking out the pre-compressed body after soaking, drying the pre-compressed body to be half-dry, putting the pre-compressed body into a mold, carrying out pressing, drying, cracking, and repeating for multiple times; carrying out vacuum impregnation with a PCS solution, taking out the product, carrying out drying and cracking, and repeating for multiple times; after completely cooling, carrying out vacuum impregnation with a high-concentration phenolic resin solution, carrying out drying and cracking, and repeating for multiple times; and placing the above in a crucible, uniformly covering the surface with Si powder, and then firing. According to the invention, the characteristics of high strength, wear resistance, corrosion resistance and the like of SiC ceramic are retained, and the composite material also has the advantages of low density, high toughness and stable high-temperature performance, so that preparation of the SiCnf/SiC composite material with high volume fraction, high compact network structure, low porosity and low residual silicon is realized, and the composite material has excellent mechanical properties of a SiCnf reinforcement.
Owner:ZHEJIANG SCI-TECH UNIV
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