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134results about How to "Not easy to curl" patented technology

High adhesion-promotion salt resistant water-soluble copolymer, preparation method and application thereof

The invention discloses a water soluble copolymer with high viscosity and salt resistance, and a preparation method and an application thereof. The preparation method comprises the steps of: adding acrylamide 20 weight parts, an anionic monomer or/and a cationic monomer 0.1-15 weight parts,, a vinyl polycyclic aromatic hydrocarbon 0.05-4 weight parts,, a surfactant 0.5-90 weight parts,, and deionized water 70-900 weight parts, into a three-neck reaction bottle, adjusting the solution pH to 2.5-9, introducing N2 for 30min, adding an initiator persulfate 0.001-0.2 weight parts, at 20-70DEG C, and reacting for 6-36 hours to obtain a low-molecular weight water soluble copolymer with molecular association ability, high viscosity and salt resistance, which can be used in intermediate-permeability oil reservoir and low-permeability oil reservoir development. An associated water soluble polymer oil displacement agent is obtained by preparing the copolymer into an aqueous solution with copolymer concentration of 0.3-3 g/L and surfactant concentration of 0.01-4 mmol/L, adding into a mixer with a stirring device, and stirring uniformly at room temperature; and the obtained oil displacement agent has high viscosity, salt resistance, temperature resistance and shear resistance, and can be used in intermediate-permeability oil reservoir and the low-permeability oil reservoir development.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Comb-typed amphiphilic water-soluble co-polymer, method for preparing same and use

The invention discloses a comb-type amphipathicity water-solubility multipolymer and a method for making the same as well as an application. The method is characterized in that: 20 portions of acrylamide, 0.1 to 10 portions of negative ion monomer, 0.5 to 15 portions of at least one of the surface activity macromolecular monomer 4-vinyl benzyl alkylphenol polyoxyethylene ether or / and allyl alkylphenol polyoxyethylene ether and 30 to 600 portions of deionized water are added into a three-necked reaction bulb, the pH value of the solution is adjusted to between 4 and 9, N2 is introduced into the solution for 30 minutes, 0.002 to 0.3 portion of evocating agent sulphate is added at the temperature of between 30 and 70 DEG C to react 12 to 36 hours in order to prepare PABE which is diluted by water to obtain the PABE strong solution; the comb-type amphipathicity water-solubility multipolymer which can viscosify, has salt resistance and the low surface tension as well as the molecular association ability and can be used for the fuel scavenge. The multipolymer is prepared into a water solution with a mass concentration between 0.3 and 3g / L and a surface active agent concentration between 0.01 and 2mmol / L, the water solution is added into a blending container with a stirring device and is stirred evenly at room temperature so that the polymer oil-displacing agent which can viscosify and shear-resistant and has excellent anti-aging performance in a hyperhaline state and at the temperature of 70 DEG C. The PABE has the double function of a tackifier and a macromolecule surfactant. Infinitesimal low molecular surface active reagent is added into the PABE solution, thereby evidently increasing the apparent viscosity of the solution, reducing the surface tension and the oil-water boundary tension of the solution and contributing to improving the recovery ratio.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Temperature-resistant water-soluble copolymer, preparation and use thereof

InactiveCN101274974AImprove solution performanceImprove rigidityDrilling compositionSolubilityPersulfate
The invention discloses a copolymer with temperature resistance and water solubility and the preparation method and application thereof, which is characterized in that: 20 portions of acrylic amide, 0.1 to 10 portions of anion monomer or/and cation monomer, 0.05 to 3 portions of fluorine-containing styrene or/and perfluoroalkyl styrene hydrophobic monomer, 0.5 to 60 portions of surface active agent and 50 to 700 portions of deionized water are put into a three-necked reaction bulb; after the solution pH is regulated to be equal to 2.5 to 9 and N2 is connected for 30 minutes, 0.001 to 0.2 portion of an evocating agent of persulfate is added under temperature of 20 to 70 DEG C, reacting for 6 to 36 hours, and PATF is prepared. Then water is used for diluting so as to prepare PATF concentrated solution, thus obtaining a copolymer that has medium molecular weight and water solubility, is high-temperature resistant, has an ability of molecular association and can be used in high temperature and high salinity reservoir. The copolymer is prepared into aqueous solution with a mass concentration of 0.3 to 3g/L and a surface-active-agent concentration of 0.01 to 4mmol/L, which is put in a blending container with a dasher and is stirred even at room temperature to prepare a polymer oil-displacing agent which is high-temperature resistant, high tackifying and anti-sharing and has excellent aging resistance under high salinity and the temperature of 110 DEG C. The prepared oil-displacing polymer has excellent solution properties owing to the supermolecular structure formed by the association between molecules of fluorine-containing cinnamene or/and alkylbenzene hydrophobic groups, thus having favorable application prospects in high temperature and high salinity reservoir exploitation.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Method for preparing allyl surface-active macromonomer

The invention discloses a method for preparing an allyl surface-active macromonomer, which is characterized by comprising the following steps: adding 20 portions of alkylphenol polyoxyethylene ether (CmH2m+1-C6H4-O-(CH2CH2O)nH, n is equal to 1 to 60, and m is equal to 1 to 20), 10 to 900 portions of solvent and 0.1 to 15 portions of catalyst into a three-mouth reaction flask with a reflux condensation device, and reacting the mixture for 1 hour under stirring at the room temperature; increasing temperature to 30 to 95 DEG C, adding 0.5 to 20 portions of allyl chloride into the reaction product, and continuously reacting for 6 to 48 hours; distilling the reaction product under reduced pressure to remove the solvent so as to obtain a crude product; and performing silica gel column chromatographic separation to obtain allyl alkylphenol polyoxyethylene ether with the yield of 70 to 95 percent. The allyl alkylphenol polyoxyethylene ether has excellent surface activity, and can be directly used as a surfactant. A water-soluble copolymer synthesized by taking the allyl alkylphenol polyoxyethylene ether as a surface-active macromonomer has the function of tackifying, or reducing solution surface tension and water-oil interfacial tension, and can be taken as a tackifying copolymer or a macromolecular surfactant for improving the oil recovery ratio.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Circumcision assembly of one-time circumcision stapler

The invention relates to a circumcision assembly of a one-time circumcision stapler, and belongs to medical apparatuses and instruments. The circumcision assembly of the one-time circumcision stapler is particularly suitable for being matched with the one-time circumcision stapler for use and comprises a glans penis cover, a knife cushion ring, a visible annular cutting knife, a transparent needle bin sleeve and a transparent needle pushing piece. The glans penis cover is provided with a glans penis cover body. A short tube is arranged on the rear portion of the glans penis cover body, internal threads are arranged inside the short tube, and positioning protrusions are arranged outside the short tube. The knife cushion ring is mounted inside the glans penis cover body, the transparent needle pushing piece is mounted inside the transparent needle bin sleeve, and the visible annular cutting knife is mounted inside the transparent needle pushing piece. The transparent needle pushing piece is provided with a transparent needle pushing piece body, a transparent annular knife mounting hole is formed in the transparent needle pushing piece body, and a positioning tube is arranged on the rear portion of the transparent needle pushing piece body. Positioning grooves are formed in the positioning tube, and the positioning grooves are matched with the positioning protrusions arranged outside the short tube of the glans penis cover. The visible annular cutting knife is in an integrated annular shape, and a knife ring of the visible annular cutting knife is provided with visible windows.
Owner:WUXI SHENKANG MEDICAL INSTR EQUIP

Method for preparing 4-vinyl benzyl surface-active macromonomer

The invention discloses a method for preparing a 4-vinyl benzyl surface-active macromonomer, which is characterized by comprising the following steps: adding 20 portions of alkylphenol polyoxyethylene ether (CmH2m+1-C6H4-O-(CH2CH2O)nH, n is equal to 1 to 60, and m is equal to 1 to 20), 10 to 900 portions of solvent and 0.1 to 15 portions of catalyst into a three-mouth reaction flask with a reflux condensation device, and reacting for 1 hour under stirring at the room temperature; increasing temperature to 30 to 90 DEG C, adding 0.5 to 25 portions of 4-vinyl benzyl chloride into the reaction product, and continuously reacting for 6 to 48 hours; distilling the reaction product under reduced pressure to remove the solvent so as to obtain a crude product; and performing silica gel column chromatographic separation to obtain 4-vinyl benzyl alkylphenol polyoxyethylene ether with the yield of 62 to 94 percent. The 4-vinyl benzyl alkylphenol polyoxyethylene ether has excellent surface activity, and can be directly used as a surfactant. A water-soluble copolymer synthesized by taking the 4-vinyl benzyl alkylphenol polyoxyethylene ether as a surface-active macromonomer has the function of tackifying, or reducing solution surface tension and water-oil interfacial tension, and can be taken as a tackifying copolymer or a macromolecular surfactant for improving the oil recovery ratio.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Dyeing-finishing pretreatment technology capable of recycling waste water

The invention discloses a dyeing-finishing pretreatment technology capable of recycling waste water. The technology comprises the following steps that firstly, fabric is conveyed into a full-width boiling machine and boiled; after the fabric is boiled, the fabric enters a padding and impregnating machine and is subjected to padding and impregnating treatment; after the fabric is subjected to the padding and impregnating treatment, the fabric is conveyed into a steaming box and steamed; after the fabric is steamed, the fabric is subjected to high-pressure washing in three or more washing machines in sequence, and then cloth is discharged. A water inlet of a water tank of the last washing machine is communicated with a clear water pipe, an overflow port of a water tank of the first washing machine is communicated with a water storage barrel, water in the water tank of the last washing machine can forward overflow to all the washing machines in sequence and is used for washing, waste water in the water storage barrel can be pumped into a waste water storage tank and stored, waste water in the waste water storage tank can flow into a first chemical material cylinder and a second chemical material cylinder through fall difference separately and is used for recycling chemical materials. According to the pretreatment technology, pretreated waste water can be recycled, during dyeing, the edges of pretreated fabric cannot be easily rolled, the fabric is good in permeability, and the dyeing defect cannot be easily generated.
Owner:JIANGSU DONGDU TEXTILE GRP +1

Anti-scour offshore wind power fan

The invention relates to an anti-scour offshore wind power fan. An anti-scour region which is formed by a plurality of splicing layers conducts anti-scour protection on a fan foundation. Supporting frameworks can support geotextile cushion layers, the flatness of the geotextile cushion layers is improved, the corners cannot be prone to curling, and therefore the stability of the structures of thegeotextile cushion layers is improved. The multiple splicing layers are connected with each other in an overlap joint mode and cannot be limited with each other, and therefore different splicing layers can heave along with the terrain of the seabed and preferably cover the seabed. In addition, the anti-scour region can adapt to the terrain of the seabed by itself. The corresponding splicing layerscan also correspondingly adjust the angles and the heights along with the scour deformation of the seabed, and therefore the overlarge gaps are prevented from being formed between the splicing layersand the seabed. As a result, the anti-scour region which is formed by the multiple splicing layers can achieve dynamic adjustment and preferably cover the seabed on the periphery of the fan foundation all the time. It can be seen that the anti-scour offshore wind power fan is good in anti-scour effect.
Owner:CHINA ENERGY ENG GRP GUANGDONG ELECTRIC POWER DESIGN INST CO LTD

Mold release film, method for manufacturing same, and method for manufacturing semiconductor package

Provided are a mold release film, a method for manufacturing the same, and a method for manufacturing a semiconductor package using the mold release film. The mold release film is not easily charged and curled, does not contaminate a mold, and has excellent mold followability. In a method for manufacturing a semiconductor package in which a semiconductor element is arranged in a mold and the mold is sealed with a curable resin, thereby forming a resin-sealed portion, the mold release film is arranged on a surface with which the curable resin on the mold is in contact. The mold release film is provided with a first thermoplastic resin layer being in contact with the curable resin during the formation of the resin-sealed portion, a second thermoplastic resin layer being in contact with the mold during the formation of the resin-sealed portion, and an intermediate layer being arranged between the first thermoplastic resin layer and the second thermoplastic resin layer. The storage elastic moduli of the first thermoplastic resin layer and the second thermoplastic resin layer at 180 DEG C are respectively 10-300 MPa, the difference in the storage elastic modulus at 25 DEG C is 1,200 MPa or less, the thickness is 12-50 [mu]m, and the intermediate layer includes a polymeric antistatic agent.
Owner:ASAHI GLASS CO LTD

Method for preparing 4-vinyl benzyl surface-active macromonomer

The invention discloses a method for preparing a 4-vinyl benzyl surface-active macromonomer, which is characterized by comprising the following steps: adding 20 portions of alkylphenol polyoxyethylene ether (CmH2m+1-C6H4-O-(CH2CH2O)nH, n is equal to 1 to 60, and m is equal to 1 to 20), 10 to 900 portions of solvent and 0.1 to 15 portions of catalyst into a three-mouth reaction flask with a reflux condensation device, and reacting for 1 hour under stirring at the room temperature; increasing temperature to 30 to 90 DEG C, adding 0.5 to 25 portions of 4-vinyl benzyl chloride into the reaction product, and continuously reacting for 6 to 48 hours; distilling the reaction product under reduced pressure to remove the solvent so as to obtain a crude product; and performing silica gel column chromatographic separation to obtain 4-vinyl benzyl alkylphenol polyoxyethylene ether with the yield of 62 to 94 percent. The 4-vinyl benzyl alkylphenol polyoxyethylene ether has excellent surface activity, and can be directly used as a surfactant. A water-soluble copolymer synthesized by taking the 4-vinyl benzyl alkylphenol polyoxyethylene ether as a surface-active macromonomer has the function of tackifying, or reducing solution surface tension and water-oil interfacial tension, and can be taken as a tackifying copolymer or a macromolecular surfactant for improving the oil recovery ratio.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Preparation method and application of graphene conductive paste

The invention relates to a preparation method and application of graphene conductive paste. The graphene conductive paste is a compound of graphene and NMP (N-methylpyrrolidone). The method comprisesthe steps of: adopting a jet mill for crushing and screening raw material crystalline flake graphite; adding an oxidizing agent and an intercalating agent into the crushed raw materials according to acertain ratio for uniform mixing, and fully reacting in a water bath; repeatedly washing the reaction solution with deionized water, and performing centrifuging and drying; performing high-temperature puffing treatment on the dried powder to obtain a precursor; and finally, adding NMP into the precursor, and carrying out ultrasonic treatment for a certain time to obtain the graphene conductive paste. The graphene in the slurry has the characteristics of a small sheet diameter (less than or equal to 20 microns, controllable sheet diameter), the low defect and porosity. The key technical problem that graphene is used as a lithium battery positive electrode conductive agent in engineering application at present is solved. The preparation method is simple, low in cost and suitable for engineering production. The prepared graphene slurry and the carbon nanotube slurry are compounded as a conductive additive to be applied to the cathode of the lithium battery, so that the energy density andthe rate capability of the lithium battery can be remarkably improved.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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