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41results about How to "Broad research prospects" patented technology

Preparation of ordered mesoporous carbon doped with nitrogen atom and preparation and application in immobilized laccase sensor thereof

ActiveCN102320589AGood direct electrochemical behaviorImprove Sensing PerformanceMaterial electrochemical variablesAnilineNitrogen gas
The invention relates to preparation of ordered mesoporous carbon doped with nitrogen atoms and preparation and an application in an immobilized laccase sensor thereof. SBA-15 and pure aniline are dissolved in hydrochloric acid with dissolved ammonium persulfate, and vacuum drying is performed; ammonium persulfate is dissolved in hydrochloric acid, and is added into the dried mixture, and vacuum drying is performed; the prepared mixture is carbonized with the protection of nitrogen atmosphere; the obtained product is soaked with 40 wt% hydrofluoric acid, filtered, washed, and dried to obtain a constant weight. The preparation of an N-OMC modified gold electrode comprises the following steps: buffing and polishing an Au electrode, flushing with distilled water, performing ultrasonic cleaning, performing activation for 10 cycles by cyclic voltammetry scan in a PBS solution with a pH of 5.0, adding the acidified N-OMC into a prepared 1.0-2.0 mg / mL laccase solution, stirring, performing centrifugation separation, and removing the supernatant. The N-OMC modified immobilized laccase gold electrode has good electrocatalytic activity, a wide linear response range, and high sensitivity and selectivity for catechol.
Owner:JIANGSU XINYUEHUA ENERGY SAVING GLASS TECH CO LTD

Method for leaching lithium form coal ash

ActiveCN107130119AImprove refined utilization valueAvoid pollutionProcess efficiency improvementMuffle furnaceGrinding mill
The invention discloses a method for leaching lithium form coal ash. The method includes the steps of 1), a sintering process, namely weighing the coal ash, sodium carbonate and calcium carbonate in the mass ratio of 1:0:1-1:0:0.8:1, performing even mixing in a corundum crucible, placing the mixture in a muffle furnace for roasting for 60-100 minutes at the temperature ranging from 1000DEG C to 1200DEG C, cooling to indoor temperature and grinding the mixture to 200 mesh with a ball grinding mill; 2), a leaching process, namely evenly mixing a well-ground clinker with a sodium carbonate solution 3-8% in concentration in the solid-to-liquid ratio of 1:15-1:25 prior to transferring to a colloid grinder, subjecting the mixture to mechanical grinding for 30 minutes prior to transferring to a high-pressure kettle, cooling mixed liquid in the high-pressure kettle after high-pressure cooking for 20-60 minutes at the temperature ranging from 100DEG C to 150DEG C is completed prior to performing extraction filtration to obtain lithium leaching liquid. The method for leaching the lithium form the desiliconized coal ash through alkali sintering-dilute alkali dissolution is put forward for the first time, broad research prospects for extracting the lithium form the coal ash are achieved, a foundation is laid for research in developing lithium resources and application strategies, and meanwhile, industrial utilization valve of the coal ash is improved.
Owner:HEBEI UNIV OF ENG

Environment-friendly high-strength lignocellulose plate and preparing method thereof

The invention discloses an environment-friendly high-strength lignocellulose plate and a preparing method thereof. The preparing method of the environment-friendly high-strength lignocellulose plate comprises the following steps that firstly, plant raw material pretreatment is conducted, lignocellulose powder with the size smaller than 40 meshes is directly taken, or, plant raw materials rich in lignocellulose fiber are utilized for conducting flash explosion treatment, and the lignocellulose fiber is obtained, wherein the size of the plant raw materials rich in lignocellulose fiber ranges from 2 meshes to 80 meshes; secondly, the lignocelluloses fiber is mixed with a bonding agent, and the bonding agent is PVA and / or gelatin; thirdly, paving is conducted; fourthly, hot pressing is conducted; and fifthly, cooling forming is conducted. The preparing method of the environment-friendly high-strength lignocellulose plate is simple in process, usage of reagents such as acid and alkali is avoided in the whole process, pollution is avoided, and environment friendliness is achieved. The prepared environment-friendly high-strength lignocellulose plate is high in mechanical strength, and pollution-free and high-valued comprehensive utilization of renewable resources is achieved.
Owner:SOUTH CHINA UNIV OF TECH

Pre-sodium-modified sodium ion battery positive electrode, and pre-sodium-modified method and application thereof

The invention discloses a pre-sodium-modified sodium ion battery positive electrode material, and a pre-sodium-modified method and application thereof. The method comprises the following step: in an inert atmosphere, reacting a sodium-ion battery positive electrode with an aryl sodium-modification reagent solution to obtain a pre-sodium-modified sodium-ion battery positive electrode wherein the aryl sodium modification reagent is one or more of biphenyl sodium, naphthalene sodium, pyrene sodium, anthracene sodium or phenanthrene sodium. A sodium-rich or over-sodium-rich positive electrode is obtained by reacting the positive electrode of the sodium-ion battery with the solution of the aryl sodium modification reagent, the half-battery first-cycle charge specific capacity is obviously improved and is matched with the efficiency of a negative electrode, the first-cycle discharge specific capacity after the whole battery is prepared reaches the theoretical specific capacity of the positive electrode, and the energy density reaches 300Wh/kg; and the method substantially improves the energy density and the cycle life of the battery, has the advantages of wide research prospect and application value, mild reaction conditions, good safety, good stability of the obtained battery, and industrial popularization and application prospect.
Owner:SHENZHEN JANAENERGY TECH CO LTD

Amide bridged organic polymer hole transport material and synthesis method and application thereof

The invention relates to an amide bridged organic polymer hole transport material and a synthesis method and application thereof. According to the design concept, a triarylamine group rich in electrons is used as an electron donating group, so that the conductivity is improved; and the binaphthalene ring structure is favorable for improving pi-pi accumulation among molecules, and meanwhile, the C2 symmetry axis of the binaphthalene ring enables the molecules to have a certain rotation angle, so that molecular aggregation is favorably inhibited. Experimental results prove that the amide bridged organic polymer hole transport material has very high hole mobility and thermal stability. In addition, the dissolvability of the molecule is improved by the non-conjugated structure of the amide group of the molecular skeleton. The designed amide bridged organic polymer molecule has a structure as shown in a formula (AI) defined in the description. The polymer has simple synthesis steps, no catalyst is added in the polymerization process, and the yield is high. The material has relatively high hydrophobicity, thermal stability, film-forming property and ductility, shows good photoelectric property and device stability when being applied to a perovskite solar cell as a hole transport material, and has a wide research prospect.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

Variable pillared ZSM-5 nanosheet molecular sieve and preparation method thereof

The invention discloses a variable pillared ZSM-5 nanosheet molecular sieve and a preparation method thereof, and belongs to the technical field of catalysts. The pillared molecular sieve is composed of orderly arranged nanosheet layers and interlayer MFI structure columns, the pillared height is adjustable in the range of 4-7nm, and the method specifically comprises the following steps: 1) dissolving an inorganic base, an inorganic acid, a small molecule template agent, a silicon source and an aluminum source in water, and uniformly stirring to form gel; 2) aging under a stirring condition; (3) continuously adding a long-carbon-chain amphiphilic surfactant solution and uniformly stirring; 4) aging under a stirring condition; and (5) crystallizing to obtain the pillared ZSM-5 nanosheet molecular sieve. According to the preparation method disclosed by the invention, the limitation of single pillared interlayer spacing in pillared preparation of the nanosheet molecular sieve at the present stage is solved, the nanosheet molecular sieve with the variable pillared interlayer spacing is prepared by a double-template method, and the prepared variable pillared ZSM-5 nanosheet molecular sieve can be used as a catalyst in the catalytic fields of preparation of low-carbon olefins and the like, and has high catalytic activity.
Owner:ZHEJIANG UNIV

Application of murabutide in the preparation of drugs for the prevention and treatment of bone marrow, small intestine and spleen damage caused by ionizing radiation

The invention relates to the field of new applications of medicines, in particular to the application of murabutide in the preparation of medicines for the prevention and treatment of bone marrow, small intestine and spleen damage caused by ionizing radiation. The murabutide provided by the invention has the advantages of low toxic and side effects, obvious prevention and treatment effect on radiation-sensitive organ damage, and the like as a medicine for preventing and treating bone marrow, small intestine, and spleen damage caused by ionizing radiation. It shows the unique advantages of murabutide in the prevention and treatment of multiple radiation-sensitive organ damage caused by ionizing radiation, and the purpose is to explore more efficient and low-toxicity treatment methods for the prevention and treatment of ionizing radiation damage; at present, there is still a lack of effective prevention and treatment of multiple organ damage caused by ionizing radiation at home and abroad Technical means are also one of the key problems that urgently need to be studied and solved in the field of radiology and clinical radiotherapy. Therefore, murabutide has broad development and application prospects in the field of medicine in my country as a drug for the prevention and treatment of multiple organ damage caused by ionizing radiation.
Owner:SECOND MILITARY MEDICAL UNIV OF THE PEOPLES LIBERATION ARMY

A method for leaching lithium from fly ash

ActiveCN107130119BImprove refined utilization valueReflect the value of industrial applicationProcess efficiency improvementFiltrationMass ratio
The invention discloses a method for leaching lithium form coal ash. The method includes the steps of 1), a sintering process, namely weighing the coal ash, sodium carbonate and calcium carbonate in the mass ratio of 1:0:1-1:0:0.8:1, performing even mixing in a corundum crucible, placing the mixture in a muffle furnace for roasting for 60-100 minutes at the temperature ranging from 1000DEG C to 1200DEG C, cooling to indoor temperature and grinding the mixture to 200 mesh with a ball grinding mill; 2), a leaching process, namely evenly mixing a well-ground clinker with a sodium carbonate solution 3-8% in concentration in the solid-to-liquid ratio of 1:15-1:25 prior to transferring to a colloid grinder, subjecting the mixture to mechanical grinding for 30 minutes prior to transferring to a high-pressure kettle, cooling mixed liquid in the high-pressure kettle after high-pressure cooking for 20-60 minutes at the temperature ranging from 100DEG C to 150DEG C is completed prior to performing extraction filtration to obtain lithium leaching liquid. The method for leaching the lithium form the desiliconized coal ash through alkali sintering-dilute alkali dissolution is put forward for the first time, broad research prospects for extracting the lithium form the coal ash are achieved, a foundation is laid for research in developing lithium resources and application strategies, and meanwhile, industrial utilization valve of the coal ash is improved.
Owner:HEBEI UNIV OF ENG

Preparation method and application of graphene-modified conductive polymer gel-coated metal nanoparticles

The invention relates to a preparation method of metal nano-particles coated with graphene modified conductive polymer gel. The method comprises the steps of firstly mixing tin-nickel nano-particles with oxidized graphene solution uniformly, then adding pyrrole, oxidizing agents and dopants, and after full reaction, cooling and drying samples, thus acquiring the metal nano-particles coated with graphene modified conductive polymer gel. The metal nano-particles coated with graphene modified conductive polymer gel prepared by the invention are of three-dimensional porous structures, the particles are uniformly distributed in graphene sheets and gel, and polypyrrole gel is tightly connected with the graphene sheets. An electrode prepared by using tin-nickel nano-particles coated with graphene modified conductive polymer gel has high cycling stability and long service life. Cycle performance of a battery can be improved by taking the tin-nickel nano-particles coated with graphene modified conductive polymer gel prepared according to the method of the invention as the negative electrode material, and a new research method is provided for solving a volume expansion problem caused by taking the tin-base material as the negative electrode material of the lithium ion battery.
Owner:TIANJIN UNIV
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