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31results about How to "No complex post-processing required" patented technology

Method for preparing stable compound through gas-liquid plasma technology and application of method

PendingCN112846216AHigh purityUniform product particle sizeMaterial nanotechnologyBiocideSteel tubeActive agent
The invention discloses a method for preparing a stable compound through a gas-liquid plasma technology. The method comprises the following steps: (1) mixing a silver nitrate water solution and a stabilizer water solution to obtain a reaction solution; (2) placing the reaction solution obtained in the step (1) into a container, placing the container at a position below a stainless steel tube cathode of a plasma reactor, and inserting a platinum wire into the reaction solution to serve as an anode; (3) in an inert gas atmosphere, applying direct-current negative bias to the cathode of the plasma reactor, and treating the reaction solution for 10-30 minutes to obtain a colloidal solution containing silver nanoparticles; and (4) adding a cationic surfactant into the colloidal solution containing the silver nanoparticles, and carrying out uniform mixing to obtain the stable compound. According to the method, the colloidal solution containing the silver nanoparticles is prepared by utilizing a high-energy electron one-step method through the gas-liquid plasma technology. The method is simple, feasible, green and efficient, and the compound with stability, transparency and excellent antibacterial performance can be obtained by compounding the colloidal solution with the surfactant.
Owner:JIANGSU XINRI E VEHICLE

Manufacturing method of universal ball cage holder

The manufacturing method of the universal ball cage holder comprises the following steps that A, alloy powder and an adhesive containing polyformaldehyde are mixed in proportion, and feed is obtained; b, the feed is subjected to banburying and granulation to be made into columnar particles with the diameter phi being 3 * 5 mm; c, preparing the columnar particles into a green body through an injection molding process; d, polyformaldehyde in the green body is removed through a catalytic degreasing technology, and then the universal ball cage holder is obtained through high-temperature sintering; wherein the alloy powder comprises ASTM 86 series low-alloy steel powder, ASTM 51 series low-alloy steel powder and 20CrMnTi alloy steel powder, the mass ratio of the alloy powder to the adhesive is (87.7-91.2)%: (8.8-12.3)%, the mass ratio of polyformaldehyde in the adhesive is 80-95%, the green body comprises a forming body, the size of the forming body is proportionally enlarged according to the size of the universal ball cage holder, and the size of the forming body is larger than that of the universal ball cage holder. According to the manufacturing method, metal material waste approaches to zero, the working procedures are simple, the number of steps is small, the production efficiency is high, the yield is high, stress residues do not exist, cost is low, and the manufacturing method is suitable for mass production of universal ball cage retainers.
Owner:KUNSHAN KADAM NEW MATERIAL TECH CO LTD

Method for producing 2-amino-4-acetamido benzene alkyl ether by reduction with sodium bisulfide

The invention relates to a method for producing 2-amino-4-acetamido benzene alkyl ether by reduction with sodium bisulfide. The method comprises the following steps: adding 2-nitro-4-acetamido benzene alkyl ether in water the mass of which is 3-5 times of that of a reactant; adding glacial acetic acid; regulating the pH value of the material to 5-6 by using liquid caustic soda; raising the temperature to 90-105 DEG C, dropwise adding a 10-25% sodium bisulfide solution, carrying out insulation reaction for 1 hour after dropwise addition; cooling slowly to crystallize and separate out the product; filtering the crystal, washing the crystal with cold water until the pH value of the filtrate is 7 to obtain 2-amino-4-acetamido benzene alkyl ether, wherein the washing sleeve is still used in the next-batch reduction. The method disclosed by the invention has the advantages that (1) the reaction yield is above 90%; (2) the reaction speed is high so that the product is not easy to oxidize, and has good colour and high quality; (3) complex aftertreatment is not required, and the equipment and operation are simple; (4) wastewater is little and easy to treat, thus the method is a low-emission clean process; and (5) resource utilization is realized for recycling and managing hydrogen sulfide waste gas so as to obtain the sodium bisulfide solution in industries such as petrifaction industry, and cost is low.
Owner:YANCHENG OUHUA CHEM IND

A preparation method of rare earth-based fluorite-type high-entropy oxide powder material

The invention discloses a preparation method of a rare-earth-based fluorite type high-entropy oxide powder material and belongs to the field of rare earth oxide powder materials. The method is a low-temperature combustion synthesis method and specifically comprises the following steps: taking rare earth nitride as a metal source and one or a mixture of more of urea, acetic acid, ammonium acetate,oxalic acid and glycine as fuel; and controlling the concentration of metal salt raw materials, types and adding amounts of the fuel, types and adding amounts of a combustion improver and an ignitionmanner to regulate and control properties including granularity, shapes and the like of rare-earth-based fluorite type high-entropy oxide powder. According to the preparation method disclosed by the invention, liquid-phase ingredients are adopted to ensure that a molecular level of the raw materials is uniform and a stoichiometric proportion of a product is realized; meanwhile, the preparation method has the advantages of energy source saving, high production efficiency, greenness and environment protection, no need of complicated post-treatment and the like; and the prepared rare earth oxidepowder has the advantages of high purity, small granularity and uniformity in distribution.
Owner:内蒙古广禾元纳米高科技有限公司
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