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64 results about "Oxygen flux" patented technology

Soft measurement method for fire box temperature of multi-nozzle opposed coal water slurry gasification furnace

The invention relates to a soft measurement method for fire box temperature of a multi-nozzle opposed coal water slurry gasification furnace. The method comprises the following steps of: choosing a plurality of measurable process status auxiliary variables, including dried basis coal, oxygen flux at furnace entrance center, coal to oxygen ratio and content of H2, Co and CH4 synthesized at an exit, as input variables of a soft measurement model; simultaneously, acquiring practical operation data of an industrial device, and preprocessing the acquired data; and based on a BP artificial neural network, choosing a 6*6*1 three-layer network topology to train the model through a Levenberg-Marquardt learning algorithm so as to implement the soft measurement for the fire box temperature of the multi-nozzle opposed coal water slurry gasification furnace. The soft measurement technology can provide effective fire box temperature information for the multi-nozzle opposed coal water slurry gasification furnace so as to guide optimal running operations in a gasification process, and the method is also suitable for the soft measurement for the fire box temperature of coal water slurry gasification furnaces of other prior technologies.
Owner:EAST CHINA UNIV OF SCI & TECH

Method for preparing 2-ethyl hexanoic acid by catalytically oxidizing 2-ethylhexanal by molybdovanadophosphoric acid

The invention discloses a method for preparing 2-ethyl hexanoic acid by catalytically oxidizing 2-ethylhexanal by molybdovanadophosphoric acid, and relates to a method for preparing a chemical preparation. The method comprises the following steps: weighing molybdovanadophosphoric acid and dissolving the molybdovanadophosphoric acid in distilled water at first and then in hydrochloric acid to prepare a catalyst solution; adding 2-ethylhexanal and the prepared catalyst in an ordinary-pressure reaction device, slowly heating and stirring the mixture, regulating oxygen flux, and starting to introduce oxygen when the temperature rises to the reaction temperature; after the reaction is ended, separating out the aqueous phase solution on the lower layer to obtain organic phase matter on the upper layer; and depressurizing and distilling the organic phase matter to obtain colorless transparent and pungent oily liquid, 2-ethyl hexanoic acid. By changing the ratio of molybdenum to vanadium of the catalyst and optimizing the reaction condition, the conversion rate of the 2-ethylhexanal reaches above 99%, and the selection and yield of the 2-ethyl hexanoic acid reach above 98% respectively.
Owner:SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY

Apparatus for actively simulating autonomous respiration of human body in vitro and gas analyzing method employing the same

The invention, which belongs to the psychological research filed of respiratory medicine, relates to an apparatus for actively simulating autonomous respiration of a human body in vitro and a gas analyzing method employing the same. The apparatus includes a circulating gas circuit formed by a driving respirator, a dual-cavity simulation lung device and a head dead space model; and the output end of the dual-cavity simulation lung device is connected with the head dead space model by a gas analyzing device. The gas analyzing method comprises the following steps that: data are collected; integration is carried out on results by multiplication of obtained real-time oxygen concentration inside the apparatus and inspiration /expiration flow rates so as to obtain oxygen fluxes and tidal volumes of expiration/ inspiration in each respiratory cycle; and division operation is carried out on the oxygen fluxes and tidal volumes to obtain mean effective inspired oxygen concentration in inspiratory/expiratory phases. According to the invention, the apparatus having a compact structure can be applied to scientific research and training of various ventilation modes; and the applied gas analyzing method enables a detection result to be accurate and to approach a real one.
Owner:THE FIRST HOSPITAL OF CHINA MEDICIAL UNIV +1

Multi-diffusion manufacturing method for polycrystalline silicon wafer

ActiveCN102544238ASolve the problem that the front and back colors are not easy to distinguishFinal product manufactureDiffusion/dopingDiffusionSurface layer
The invention discloses a multi-diffusion manufacturing method for a PN junction manufactured of a polycrystalline wafer. The multi-diffusion manufacturing method comprises the following steps of: S1, depositing, by constant source diffusion, an impurity source of certain concentration on the surface layer on which a P layer is required to be formed; S2, heating finite source diffusion to perform internal diffusion on a deposited impurity source phase polycrystalline wafer to control junction depth of the PN junction and gradient distribution of an impurity source; S3, depositing, by the constant source diffusion, the impurity source of the certain concentration on the surface layer of the P layer of the polycrystalline wafer again; S4, increasing, by oxygenation constant source diffusion, flux of oxygen under the conditions of unchanged temperature and a continuous flux source, wherein the step aims to increase the surface color of the P layer of the polycrystalline wafer, so that a front face and a back face of the polycrystalline wafer are differentiated during subsequent operation, and the hydrophilicity of the P layer can also be improved by increase in oxygen flux, so that an over large etching edge is reduced; and S5, repeating the step S2 to the step S4. Through the steps, the aim of solving the problem of difficulty in differentiating the colors of the front face and the back face existing after manufacturing of the PN junction of the polycrystalline wafer can be fulfilled.
Owner:YINGLI ENERGY CHINA

Stainless steel doped perovskite ceramic two-phase composite hollow fiber oxygen-permeating membrane and preparation method thereof

The invention belongs to the technical field of inorganic membranes, and particularly relates to a stainless steel doped perovskite ceramic two-phase composite hollow fiber oxygen-permeating membrane and a preparation method thereof. Being doped with 3 to 10 percent of stainless steel powder, a perovskite ceramic hollow fiber oxygen-permeating membrane can be greatly higher in strength. The preparation method comprises the following steps: preparing a casting solution containing perovskite ceramic powder, stainless steel powder, a polymer binder, a solvent and an additive; preparing a stainless steel/perovskite ceramic two-phase composite hollow fiber oxygen-permeating membrane precursor adopting an asymmetric structure according to a spinning phase inversion method; preparing the stainless steel doped perovskite ceramic two-phase composite hollow fiber oxygen-permeating membrane according to a certain high-temperature sintering program. The stainless steel doped perovskite ceramic two-phase composite hollow fiber oxygen-permeating membrane prepared according to the method is high in oxygen flux and mechanical strength, is easy to be assembled into a membrane component, and has the advantages that the practicability of a ceramic hollow fiber oxygen-permeating membrane is improved; the preparation process is simple; no complex equipment is required; convenience is brought for industrial production.
Owner:上海穗杉实业股份有限公司 +1

Method for treating cold-state lead-rich slag with hot slag side-blowing reduction furnace

The invention relates to a method for treating cold-state lead-rich slag with a hot slag side-blowing reduction furnace, and belongs to the technical field of thermometallurgy. The method comprises the following steps: (1) adding 70-90 t of hot-state lead-rich slag, 3-6 t/h of cold-state lead-rich slag, 1.5-2.5 t/h of limestone, 3-4 h/t of iron calcine, 2-3 t/h of coke nut and 0.8-1.6 t/h of crushed coal; (2) after a siphon mouth lead liquid level rises to the lead liquid flowing height in a lead-rich slag adding process, carrying out lead tapping and ingotting; (3) adding 3-10 t of zinc calcine, 2.2-3.5 t of limestone, 3-6 t of iron calcine, 2-3.5 t of coke nut, and 2.5-4 t of crushed coal into each furnace, and controlling the gas flux, oxygen flux, molten pool temperature and in-furnace negative pressure within 3200 to 3600 Nm<3>/h, 950 to 1200 Nm<3>/h, 1100 to 1300 DEG C and -20 to -40 pa respectively; (4) after the lead-rich slag adding process is finished, continuously adding crushed coal at 1000-1250 DEG C for 1-2 hours' smelting, observing the lead content of molten slag with a slag detection bar till the lead content is lower than or equal to 2.2%, and then carrying out 0.5 hour's heating for slag tapping; (5) conducting waste heat recovery and dust collection on flue gas in a smelting process, and then sending the treated flue gas into a desulphuration system. The method is simple in technology and has the advantages that the conventional technology is sufficiently utilized, the defect in stockpiling of the cold-state lead-rich slag is effectively overcome, the recovery rate of valuable metal is improved, and the like.
Owner:YUNNAN CHIHONG ZINC & GERMANIUM

Ultraviolet radiation-oxygen-temperature-humidity coupled asphalt aging testing device and method

The invention discloses an ultraviolet radiation-oxygen-temperature-humidity coupled asphalt aging testing device and method. The ultraviolet radiation-oxygen-temperature-humidity coupled asphalt aging testing device comprises a control box, an environment box, a power assembly arranged in the control box, an object carrier stage and a rotating shaft, wherein the object carrier stage and the rotating shaft are arranged in the environment box; a control panel is arranged on the control box; the control box is positioned at the bottom of the environment box; an output shaft of the power assemblyis connected with the lower end of the rotating shaft; the object carrier stage is arranged on the upper part of the rotating shaft and is distributed aslant; a sample accommodating dish is arrangedon the object carrier stage; a plurality of ultraviolet lamps and sensor groups for detecting temperature, humidity and oxygen concentration in the environment box are arranged on the inner wall of the environment box; an outlet of an air blast system communicates with an air inlet of the environment box; the control panel is connected with a control end of the air blast system, the output ends ofthe sensor groups and the control end of the power assembly. According to the device and the method disclosed by the invention, an asphalt aging test on intensity of ultraviolet rays, the temperature, the oxygen flux and the humidity under constant and transforming modes can be realized.
Owner:CHANGAN UNIV

Industrial boiler

The invention relates to the technical field of boilers, in particular to an in industrial boiler. The industrial boiler comprises a boiler body, a switch door, a storage mechanism, a pressure reliefstructure and an air inlet mechanism. The boiler body for supplying coal to combust and exchange heat is connected to the switch door for adding coal, the boiler body is connected to the storage mechanism used for adding water and discharging steam, the boiler body is connected to the pressure relief structure for relieving pressure of water vapor, the boiler body is connected to the air inlet structure for conveying oxygen to combust the coal, and the air inlet structure is connected to the pressure relief structure; and the pressure relief structure is matched with the air inlet structure touse. The oxygen flux in a storage room is reduced while the pressure of the water vapor in a water storage room is relieved by means of the pressure relief structure, the combustion rate of the coalin the storage room is reduced, and the boiler body is prevented from being damaged as a result of too large pressure in the water storage room, so that the water vapor generation capacity in the pressure relief process of the water storage room is reduced, the water vapor amount flowing from a pressure relief port is reduced, and the loss of the water vapor relived in pressure is reduced.
Owner:日照菁英传媒科技有限公司

Method for measuring dissolved oxygen flux of marine near-bottom boundary layer

The invention discloses a method for measuring the dissolved oxygen flux of a marine near-bottom boundary layer. The method comprises the steps of: (1), adjusting a seabed observation device and parameters; (2), arranging an observation device; (3), obtaining original high-frequency data; (4), pre-processing the original data, and calculating the pulsating quantity of the average flow speed and the average dissolved oxygen concentration; and (5), calculating the horizontal flux and the vertical flux by utilizing the pulsating quantity of the flow speed and the dissolved oxygen concentration calculated in the step (4). The observation device of the observation method comprises a battery compartment, an acoustic Doppler point type current meter and a needle type dissolved oxygen sensor. Themethod in the invention has the benefits that: observation is synchronously carried out through multiple sets of instruments; high-frequency data of the flow speed and the dissolved oxygen concentration in a water body is synchronously obtained in situ; long-time observation and storage are realized; the data resolution is high; and the dissolved oxygen level and the vertical flux can be obtainedmore accurately in a non-interfered water body environment.
Owner:TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY

Surface treatment method for stripping single crystal thin film through ion implantation

The invention belongs to the technical field of single crystal thin films, and particularly relates to a surface treatment method for stripping a single crystal thin film through ion implantation. According to the surface treatment method for stripping the single crystal thin film through ion implantation, argon ion etching is selected for accurately removing a damaged layer on the surface of thesingle crystal thin film prepared through the ion implantation stripping technology; and besides, the problems of oxygen vacancy defects and surface modification of the film after the damaged layer isremoved are solved by respectively controlling the oxygen flux, the working power and the working parameters of the cleaning time in the oxygen plasma cleaning process, the cleaning effect is verified through the contact angle test, and finally, the single crystal thin film is completely infiltrated, so that the subsequent preparation of a graphical device structure is facilitated. According to the method, the single crystal quality of the single crystal thin film is greatly improved, the introduced secondary damage is minimum, and the process complexity is simplified.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

Aluminum-containing biphase mixed conductor oxygen permeation membrane material with good stability and preparation method thereof

The invention designs and prepares an aluminum-containing biphase mixed conductor oxygen permeation membrane material with high oxygen permeation amount, and belongs to the technical field of inorganic functional ceramic manufacturing. The general formula of the biphase mixed conductor oxygen permeation membrane material is 60Ce0.9La0.1O< 2-delta>-40La0.6Sr0.4Co<1-x>AlxO<3-delta> (x is equal to 0.05, 0.1, 0.2, 0.3 or 0.35). The preparation method comprises the steps of preparing required powder by using an improved one-pot-sol-gel method, calcining the powder in a muffle furnace at the temperature of 950 DEG C for 12 hours to obtain a precursor, tabletting the powder, and sintering at the temperature of 1250 DEG C to finally obtain the required mixed conductor oxygen permeation membrane. The mixed conductor oxygen permeation membrane material with high oxygen permeation amount is obtained by regulating and controlling the proportion of the multivalent and economical Al element. The biphase membrane material prepared by the method has excellent oxygen flux under the purging of gases such as helium/carbon dioxide. The material shows good long-term stability in low-oxygen argon and corrosive carbon dioxide atmospheres, and can be used as a novel oxygen source to be applied to the high-temperature complex atmosphere oxygen industry, such as the fields of oxygen-enriched combustion, water decomposition and methane coupling.
Owner:SUN YAT SEN UNIV
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