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52results about How to "Available for mass production" patented technology

Doped graphene and method for preparing same

The invention discloses a doped graphene and a preparation method thereof. The doped graphene is prepared by adopting a chemical vapor deposition method, which comprises the steps as follows: a substrate with catalyst is put into a reaction kettle without oxygen, with the temperature of the substrate being 500 DEG C to 1200 DEG C; then material with carbon element and doped elements is piped into the reaction kettle, and the doped graphene is obtained; the catalyst is metal or metallic compound. The doped graphene prepared by the invention has good quality, and the preparation method is simple and feasible and can be conveniently operated and used for large-scale production.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Inorganic ion doped carbon nitride photocatalyst and preparation method thereof

The invention provides an inorganic ion doped carbon nitride photocatalyst and a preparation method thereof. The inorganic ion doped carbon nitride photocatalyst has a molecular formula shown in a formula (I). The preparation method comprises the following steps of: sufficiently mixing carbon and nitrogen sources and inorganic salt in a water solution, then drying and calcining to obtain the inorganic ion doped carbon nitride photocatalyst which has the molecular formula shown in the formula (I). According to the photocatalyst, inorganic ions enter a crystal lattice or an interlayer of C3N4, and visible-light catalytic activity of the C3N4 photocatalyst provided by the invention is greatly enhanced through the doping of the inorganic ions. Experiments indicate that the visible-light catalytic activity of the inorganic ion doped C3N4 photocatalyst with a two-dimensional structure is 1.5-3 times higher than that of a photocatalyst without C3N4 doped. Besides, the preparation method provided by the invention is moderate in condition, easy to operate and favorable to large-scale production.
Owner:重庆传森迅特科技有限公司

Method for preparing three-dimensional porous graphene material by solution

The invention discloses a method for preparing a three-dimensional porous graphene material by solution. The method comprises the following steps of: immersing a three-dimensional porous template into a graphene oxide solution, and then depositing the graphene oxide on the template to realize three-dimensional assembling of the graphene oxide on the template, and then preparing the three-dimensional porous graphene material containing the template by reduction; removing the template from the three-dimensional porous graphene material containing the template, and then washing to obtain the three-dimensional porous graphene material. The aperture of the three-dimensional porous graphene material can be regulated and controlled by using the templates with different apertures the material prepared by the invention has the advantages of low density, high specific surface area, high heat conductivity, high-temperature resistance, and corrosion resistance; the preparation method is economical and simple and suitable for large-scale production. And the prepared material is applicable to aspects such as catalytic carriers, preparation of flexible conductors, and stretchable electronics.
Owner:HUAZHONG UNIV OF SCI & TECH

Composite lithium metal negative electrode based on MXene aerogel and synthesis method thereof

The invention discloses a composite lithium metal negative electrode based on an MXene aerogel and a synthesis method thereof, which belong to the field of lithium batteries. The composite lithium metal negative electrode comprises metal lithium and the MXene aerogel, wherein the MXene aerogel is assembled by cross-linking of two-dimensional MXene sheets and has a three-dimensional hierarchical porous structure; the MXene aerogel pores are filled with the metal lithium; and the thickness of the MXene aerogel is 300 mum to 800 mum. According to the composite lithium metal negative electrode prepared in the invention, rich pro-lithium functional groups on the surface of the MXene aerogel can be specifically combined with the lithium ions, uniform nucleation of lithium is thus realized, formation of lithium dendrites is suppressed, and the coulombic efficiency, the safety and the cycle life of the lithium metal negative electrode are effectively improved.
Owner:DALIAN UNIV OF TECH

Method of improving buried resistance printed wire board resistance precision

The invention provides a method of improving buried resistance printed wire board resistance precision. The method of improving the buried resistance printed wire board resistance precision comprises the following steps: (1) supplying a board with a buried resistance layer, wherein the board with a buried resistance layer comprising an insulating medium layer, the buried resistance layer and a copper foil layer, (2) attaching a first light resistance film, proceeding a first time exposure, printing a circuit figure of a negative film on the first light resistance film, proceeding a first time develop, the circuit figure comprising a resistance circuit and a normal circuit, increasing 6 mil to a long side unilateral of circuit width of the resistance circuit, and increasing 1.25 mil to a broadside unilateral of circuit width of the resistance circuit, (3) proceeding a first time etching and a second time etching, (4) attaching a second light resistance film, proceeding a second time exposure, printing a circuit figure of a positive film on the second light resistance film, proceeding a second time develop, reducing 0.6 mil to a long side unilateral of circuit width of the resistance figure, and increasing 6 mil to a broadside unilateral of circuit width of the resistance figure, (5) proceeding a third time etching, and (6) proceeding brown oxide processing, controlling micro etching amount between 1.3-1.7um,proceeding a -17% extra compensation to the resistance figure of the positive film.
Owner:DONGGUAN SHENGYI ELECTRONICS

Grass carp reovirus S11 gene eukaryotic expression recombinant plasmid preparation method and application thereof in serving as nucleic acid vaccine

The invention discloses a grass carp reovirus S11 gene eukaryotic expression recombinant plasmid preparation method and application thereof in serving as nucleic acid vaccine, and belongs to the technical field of gene engineering and molecular immunology. The preparation method disclosed by the invention is characterized by comprising the steps of extracting viral genome RNA, performing reverse transcription to convert the viral genome RNA into cDNA, amplifying a corresponding DNA sequence out, constructing the DNA sequence to pcDNA-3.1(+) plasmid, converting Escherichia coli DH5alpha, screening out positive clone bacteria containing recombinant plasmid, culturing a lot of the positive bacteria and extracting recombinant plasmid S11-pcDNA3.1 contained in the bacteria. The recombinant plasmid is utilized as nucleic acid vaccine to perform intramuscular injection on the grass carps, and the nucleic acid vaccine enters the muscle cells and expresses VP35 protein of the grass carp reovirus in the muscle cells; thus, fish body immune cell proliferation is stimulated, antiviral related gene expression is up regulated, fish bodies are stimulated to generate antiviral antibodies, and capability of grass carps in resisting grass carp reovirus infection is effectively improved; furthermore, the grass carp reovirus S11 gene eukaryotic expression recombinant plasmid can be used for preventing a grass carp hemorragic disease caused by the grass carp reovirus in aquaculture.
Owner:HENAN NORMAL UNIV

Hierarchical porous nickel-aluminum alloy membrane with electrocatalytic performance and preparation method thereof

The invention discloses a hierarchical porous nickel-aluminum alloy membrane with the electrocatalytic performance and a preparation method thereof. According to the method, a certain proportion of nickel-aluminum powder is taken, is mixed and pressed, and then is molten into a porous alloy membrane in a sintering mode, then the interior of the porous alloy membrane is enabled to form a microporous morphology through chemical corrosion, the alloy membrane forms a nano-pore structure with high specific surface area and high catalytic activity due to the fact that nickel-aluminum alloy is corroded by sodium hydroxide, so that the membrane separation and the electrocatalysis function are integrated without adding an additional supported catalyst, and therefore the processing capacity of the alloy membrane to dye wastewater is greatly improved, and the decolorization rate of the alloy membrane at the maximum flux is increased from 55% to 95% or above.
Owner:宁波杰士兄弟工具有限公司

Method for improving accuracy of resistance value of buried resistance printed circuit board

The invention provides a method for improving the accuracy of a resistance value of a buried resistance printed circuit board. The method comprises the following steps of: 1, providing a board with a buried resistance layer, wherein the board comprises an insulating dielectric layer, the buried resistance layer and a copper foil layer; 2, pasting a first photoresist film, performing primary exposure, printing a line graph of a negative film on the first photoresist film, and performing primary development, wherein the line graph consists of a resistance line and a normal line, each of long sides of a line width of the resistance line is prolonged by 6mil, and each of wide sides of the line width of the resistance line is prolonged by 1.25mil; 3, performing primary etching and secondary etching; 4, pasting a second photoresist film, performing secondary exposure, printing a resistance graph of a positive film on the second photoresist film, and performing secondary development, wherein each of long sides of a line width of the resistance graph is shortened by 0.6mil, and each of wide sides of the line width of the resistance graph is widened by 6mil; 5, performing tertiary etching; and 6, performing blackening treatment on the surface of the board in a way of controlling a microetching amount within 1.1 to 1.5 mu.m, and performing additional compensation of -12 percent on the resistance graph of the positive film.
Owner:DONGGUAN SHENGYI ELECTRONICS

End face coupler and manufacturing method therefor

The invention discloses an end face coupler and a preparation method therefor, and the coupler comprises a silicon substrate; a buried oxide layer which is formed on an upper surface of the silicon substrate; top silicon which is formed in the buried oxide layer, and has first top silicon and second top silicon; silicon nitride waveguides formed on the top silicon, wherein the silicon nitride waveguides include a first silicon nitride waveguide and a second silicon nitride waveguide, wherein the central lines of the first silicon nitride waveguide and the second silicon nitride waveguide are located on the central line of the top silicon. The beneficial effects are that by growing a plurality of silicon nitride waveguides at different heights above the top silicon, a light field of a largeplaque size is realized, and the length of the longitudinal structure is reduced by combining the design of a longitudinal wedge structure, and finally a waveguide end face coupler with the high coupling efficiency is formed; the end face coupler is simple in fabrication process, is compatible with CMOS process, can be used for mass production, has low cost, and has a high industrial utilizationvalue.
Owner:南通赛勒光电科技有限公司

Double modified carboxymethyl chitosan derivative and preparation method thereof

The invention discloses a double modified carboxymethyl chitosan derivative and a preparation method thereof. The molecular structural formula of the product is shown as formula (1), wherein x, y, z and n are natural numbers; x is more than or equal to 1 but less than or equal to 10000; y is more than or equal to 1 but less than or equal to 10000; z is more than or equal to 1 but less than or equal to 10000; and n is more than or equal to 1 but less than or equal to 30. The preparation method comprises the step of causing carboxymethyl chitosan, quaternary ammonium salt and (oligomeric) arginine to react under a catalyzing condition, thereby acquiring the double modified carboxymethyl chitosan derivative. The preparation method is mild in reaction condition, requires no high-temperature high-pressure treatment, requires no organic solvent or strong acid, is green and environment-friendly and is suitable for large-scale production. According to the invention, the quaternary ammonium salt and the (oligomeric) arginine are simultaneously grafted on a main chain of carboxymethyl chitosan, so that the derivative has excellent water solubility, antibacterial performance and biocompatibility.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Purification method for high-purity organic solvent normal propyl alcohol

The invention relates to a purification method for high-purity organic solvent normal propyl alcohol. The method includes steps: subjecting raw normal propyl alcohol to removal of high ultraviolet absorption impurities by the aid of activated carbon, utilizing desiccants such as anhydrous calcium sulfate or calcium hydride for drying and dehydration, rectifying, filtering and packaging to obtain the high-purity organic solvent normal propyl alcohol. By the purification method for the high-purity organic solvent normal propyl alcohol, chromatographic-grade normal propyl alcohol products with the purity higher than 99.8% can be obtained, the yield is higher than 95%, the acceptance rate is higher than 93%, and application requirements of users in aspects of scientific researches, subject studies and the like of the high-purity organic solvent (HPLC) normal propyl alcohol can be met. In addition, compared with conventional methods, the purification method for the high-purity organic solvent normal propyl alcohol is high in product purity, simple and convenient to operate and stable in product quality and can be used for large-scale production.
Owner:天津康科德医药化工有限公司

Collagenase inhibitor composition, anti-aging moisture dew and preparation method of anti-aging moisture dew

The invention discloses a collagenase inhibitor composition, an anti-aging moisture dew and a preparation method of the anti-aging moisture dew. The collagenase inhibitor composition comprises 50-99%of a Chinese wolfberry extract and 1-50% of a ginseng extract, and the mass ratio of the ginseng extract to the Chinese wolfberry extract is preferably 1: 3-15. The anti-aging moisture dew comprises the collagenase inhibitor composition and a penetration enhancer, the addition amount of the collagenase inhibitor composition is 0.01-10%, and the collagenase inhibitor composition comprises 50-99% ofthe Chinese wolfberry extract and 1-50% of the ginseng extract; wherein the addition amount of the penetration enhancer is 0.01%-10%, and the penetration enhancer is bis-diethoxydiethylene glycol cyclohexane 1, 4-dicarboxylate. According to the collagenase inhibitor composition, the Chinese wolfberry extract and the ginseng extract are matched, so that a synergistic effect is achieved, and the activity of collagenase can be well inhibited. The anti-aging moisture dew can reduce degradation of collagen, has an anti-aging effect, also has moisturizing and water locking effects, can prevent moisture loss, and creates a moisturizing barrier for the skin.
Owner:GUANGZHOU KENENG COSMETICS RES CO LTD +1

Purification method of highly pure organic solvent n-propanol

The invention relates to a purification method of highly pure organic solvent n-propanol. The method comprises the following steps of: removing the impurities with high ultraviolet absorption in the raw material n-propanol by active carbon; drying and dewatering the treated n-propanol by a drying agent of anhydrous calcium sulphate or calcium hydride; rectifying; filtering; and packing to obtain the highly pure organic solvent n-propanol. The purification method provided by the invention can obtain the chromatographic-grade n-propanol product with the purity more than 99.8%; the yield of the n-propanol is more than 93%; the qualified rate of the n-propanol is more than 93%; the application need of users of highly pure organic solvent n-proanol (HPLC) (high performance liquid chromatography) in the scientific research and the subject research can be satisfied; compared with the traditional methods, the n-propanol obtained by the method provided by the invention is high in the purity; the operation is simple; the quality of the product is stable, and thus the method can be applied to the large-scale production.
Owner:天津康科德医药化工有限公司

Co-combustion preparation method of sulfur doped graphene quantum dot

ActiveCN105540578AModulation structureModulation levelNanotechnologyDoped grapheneMaterials science
The invention provides a co-combustion preparation method of a sulfur doped graphene quantum dot and relates to a preparation method of a graphene quantum dot, in particular to the co-combustion preparation method which adopts cheap liquid paraffin and carbon disulfide as raw materials for preparation of the sulfur doped graphene quantum dot with a co-combustion method. According to the co-combustion preparation method of the sulfur doped graphene quantum dot, a structure and an energy level of the graphene quantum dot are effectively modulated through doping of heterogeneous sulfur atoms, so that photoelectrical properties of the graphene quantum dot are modulated, and the co-combustion preparation method of the sulfur doped graphene quantum dot is characterized in that the sulfur doped graphene quantum dot is obtained with the co-combustion preparation method, an ultrasonic preparation method and the like. According to the co-combustion preparation method of the sulfur doped graphene quantum dot, the overall technical route is innovative, the price is low, sulfur doped carbon nanospheres prepared with the co-combustion method are subjected to ultrasonic liquid-phase stripping, the sulfur doped graphene quantum dot is successfully prepared and has excellent photoelectrical properties, the extra energy level of the graphene quantum dot is increased, and the performance of the graphene quantum dot is effectively improved.
Owner:KUNMING INST OF PHYSICS

Preparation method for copper-doped multilayer graphene

The invention relates to a preparation method for copper-doped multilayer graphene, and relates to graphene. According to the preparation method for copper-doped multilayer graphene, through doping ofheterogeneous copper atoms, the structure and the energy stage of the multilayer graphene are effectively regulated, and the photoelectric property of the multilayer graphene is improved. According to the preparation method, a graphite target material and a copper target material are used as raw materials, direct current radio frequency joint sputtering of magnetron sputtering is adopted, a copper element is led into a carbon substrate, and the structure and the energy stage of the multilayer graphene are effectively improved. According to the preparation method, low-cost easily-obtained andnontoxic graphite target material and copper target material are used as the raw materials, the copper element is led into the carbon substrate, the structure and the energy stage of the multilayer graphene are effectively improved, and the electron transition mode is more diverse; and the photoelectric property of the multilayer graphene is effectively changed, and the multilayer graphene can beused for detectors, light emitting diodes, solar batteries, supercapacitors, lithium ion batteries, fluorescent materials and other fields.
Owner:KUNMING INST OF PHYSICS

Purification method for high-purity organic solvent n-butyl alcohol

The invention relates to a purification method for high-purity organic solvent n-butyl alcohol. The purification method comprises the steps that raw material of n-butyl alcohol is adsorbed by silica gel and kieselguhr column to remove most of impurities of aldehydes, ketones and esters, then is dried and dewatered by drying agents such as anhydrous magnesium sulfate or anhydrous potassium carbonate, and finally rectified, filtered and packed to obtain a high-purity organic solvent n-butyl alcohol product. The high-purity organic solvent n-butyl alcohol product with the purity larger than 99.9% can be obtained through the purification method, the yield is more than 92%, the percent of pass is higher than 92%, and the application requirements of the high purity organic solvent (HPLC) n-butyl alcohol in fields of scientific researches, research projects and the like are met. Simultaneously, compared with a general method, the purification method is high in production purification, simple to operate, stable in product quality and suitable for scale production.
Owner:天津康科德医药化工有限公司

Purification method of highly pure organic solvent n-butanol

The invention relates to a purification method of highly pure organic solvent n-butanol. The method comprises the following steps of: removing most aldehyde, ketone and ester impurities in the raw material n-butanol by adsorption of silica gel and a diatomite column; drying and dewatering by a drying agent of anhydrous magnesium sulphate or anhydrous potassium carbonate; rectifying; filtering; and packing to obtain the highly pure organic solvent n-butanol. The purification method provided by the invention can obtain the highly pure organic solvent n-butanol with the purity over 99.9%; the yield of the n-butanol is more than 92%; the qualified rate of the n-butanol is more than 92%; the application need of users of highly pure organic solvent n-butanol (HPLC) (high performance liquid chromatography) in the scientific research and the subject research can be satisfied; compared with the traditional methods, the n-butanol obtained by the method provided by the invention is high in the purity; the operation is simple; the quality of the product is stable, and thus the method is applied to the scale production.
Owner:天津康科德医药化工有限公司

Low-water-absorption PA56T/PET composite material and preparation method thereof

PendingCN114479440AGood mechanical properties and dimensional stabilityGood antioxidant propertiesAnoxomerPolyethylene terephthalate
The invention discloses a PA56T / PET composite material, and relates to the technical field of engineering. The composite material is prepared from the following raw material components in parts by weight: 15-85 parts of PA56T; 15 to 85 parts of PET (Polyethylene Terephthalate); 2 to 20 parts of a compatilizer; 0.2 to 0.8 part of an antioxidant; 20 to 40 parts of glass fiber; and 0.2 to 1 part of a lubricant. According to the composite material and the preparation method thereof, the raw materials are low in price and environment-friendly, compared with the prior art, the PA56T / PBT alloy prepared from the bio-based PA56T combines the advantages of the PA56T and PET, the tensile strength and modulus are obviously improved, the impact strength is not lower than that of pure PA56T, the water absorption rate of the PA56T is greatly reduced, the dimensional stability of the PA56T is improved, and the composite material is suitable for industrial production. By means of the breakthrough, the alloy can be widely applied to materials of air conditioner parts, power distribution parts, automobile parts and the like, the production process is simple, and the excellent market prospect is achieved.
Owner:EAST CHINA UNIV OF SCI & TECH

Ultra-high molecular weight polyethylene fiber bulletproof composite material and preparation method

The invention relates to the technical field of high-resistance bulletproof composite materials and discloses an ultra-high molecular weight polyethylene fiber bulletproof composite material and a preparation method. The bulletproof composite material is prepared by compounding modified polystyrene resin and ultrahigh molecular weight polyethylene (UHMWPE) fibers, wherein the modified polystyreneresin is prepared by modifying polystyrene resin by adopting an ethylene-vinyl acetate (EVA) copolymer having high flexibility, elasticity and packing compatibility; the polymer prepared by polymerizing monomer styrene free radicals of the polystyrene resin is colorless and transparent, has high rigidity and is capable of improving wettability of the modified resin on fibers. The bulletproof composite material disclosed by the invention has the advantages of low density, high specific strength and specific modulus, shock absorption property, fatigue resistance, excellent environmental suitability and the like and meets bulletproof requirements. The preparation method disclosed by the invention has the advantages of simple steps and high operability and is capable of realizing batch production.
Owner:UNIT 61489 OF PLA

Dried fish further processing method

The invention discloses a dried fish further processing method which comprises the following steps: killing the selected fish; conducting salting on the fish according to different categories, and conducting rinsing on the salted dried fish; placing the fish in the natural withering area and conducting initial air drying and stoving after rinsing; cutting and packaging the dried fish after trimming, and conducting vacuum packaging, and product packaging after checking. The invention relates to a dried fish further processing method which contains neither corrosion remover nor food additives, is long in expiration date, convenient to eat, is provided with certain advancement, confidentiality and potential economic value, and solves the potential safety hazard problems that the conventional fish convenient products are less in variety and contain a large amount of corrosion remover and food additives.
Owner:PINGCHANG COUNTY YANGSHI XIANHE YUHUI CO LTD

Composition for inhibiting melanin generation, whitening essence, and preparation method and application thereof

The invention belongs to the field of daily chemicals, and particularly provides a composition for inhibiting melanin generation, whitening essence, and application thereof. The composition for inhibiting melanin generation comprises a cortex phellodendri extract and a licorice extract. The composition for inhibiting melanin generation has a synergistic effect by matching the cortex phellodendri extract and the licorice extract, and can well inhibit the generation of melanin. The whitening essence prepared by applying the composition for inhibiting melanin generation can reduce the generation of melanin, play a role in whitening, increase the moisture content of the cuticle, and block the moisture loss of the deep layer of the skin.
Owner:GUANGZHOU KENENG COSMETICS RES CO LTD +1

PGS/SF electrospun artificial blood vessel and preparation method thereof

ActiveCN111714704AMicro-nano fiber structure is goodImprove adhesionStentsElectro-spinningFiberSpinning
The invention relates to a PGS / SF electrospun artificial blood vessel and a preparation method thereof. The invention discloses a preparation method of the PGS / SF electrospun artificial blood vessel.The method comprises the following steps: 1, dissolving a PGS prepolymer and SF into an organic solvent to obtain a spinning solution; carrying out electrostatic spinning on the spinning solution; receiving micro-nano fibers by adopting a cylindrical receiving device rotating around the axis of the receiving device, winding the micro-nano fibers outside the receiving device to form a tubular PGS / SF electrospun membrane; and drying and solidifying the tubular PGS / SF electrospun membrane after completely spinning to obtain a PGS / SF electrospun artificial blood vessel. According to the PGS / SF electrospun artificial blood vessel, the spinnability and fiber forming property of PGS are improved through the SF, the PGS / SF electrospun artificial blood vessel is successfully obtained, the caliber of the electrospun artificial blood vessel is smaller than 6 mm, and the electrospun artificial blood vessel has the excellent elasticity of the PGS and the excellent biological and mechanical properties of the SF.
Owner:NANTONG TEXTILE & SILK IND TECH RES INST +1

A kind of cufeo2-carbon nanotube nanocomposite and its synthesis method

The invention relates to a CuFeO2-carbon nanotube nanocomposite and a synthesis method thereof. The synthesis includes the following steps: adding an appropriate amount of carbon nanotubes to water and dispersing them ultrasonically to form a carbon nanotube dispersion liquid. Dissolve Fe(III) salt and Cu(II) salt in water, and slowly drop the strong alkali solution under stirring to make the pH ≥ 11. Add carbon nanotube dispersion to the above mixture, stir to obtain a colloidal suspension, then add a reducing agent and mix evenly, then transfer the colloidal suspension to a hydrothermal kettle for hydrothermal reaction, cool, centrifuge, wash, dry. In the CuFeO2-carbon nanotube nanocomposite prepared by the above method, CuFeO2 is nanoparticles and wrapped on the surface of the carbon nanotube. Compared with the existing technology, the present invention introduces carbon nanotubes during the hydrothermal synthesis process to obtain a nanocomposite with good mass transfer conductivity and regular morphology, which is simple and easy to implement and can achieve large-scale production.
Owner:SHANGHAI JIAO TONG UNIV
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