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76results about How to "No need to deal with" patented technology

Method for eliminating dioxins in flue gas

The invention relates to a method used for eliminating dioxin in fume. The method has the following steps that water solution containing substance of hydrazine type is sprayed into the fume containing dioxin or potentially containing dioxin so that the fume fully touches and reacts with the water solution, and the water in the solution is completely evaporated at the temperature above 160 DEG C. In this way, dioxin in the fume is eliminated. The water solution with hydrazine type substance is fresh solution prepared based on 0.05 percent to 1 percent by weight before use, and is sprayed into the fume with the temperature ranging from 200 DEG C to 600 DEG C, or into the fume with the temperature ranging from 600 DEG C to 850 DEG C. At the temperature ranging from 600 DEG C to 850 DEG C, the water in the water solution containing hydrazine can adopt urea or ammonia. At the temperature ranging from 200 DEG C to 600 DEG C, the water to dissolve hydrazine can adopt alkaline solution or urea solution in combination with purification of other noxious gases such as SOx and NOx by using a prior or a late established purification device or system, so that NOx and acidic gases in the fume are eliminated, and toxicant content in fly ash is reduced. By adopting the method, dioxin in the fume is eliminated without production of noxious byproducts. Throughout the course, no waste water or waste solid is produced; the concentration of dioxin in fly ash is reduced; the treating process is simple, and the cost of disposal is low.
Owner:TONGJI UNIV

Preparation process for catalyzing and synthesizing tert-butyl acrylate by using strong acid cation exchange resin as catalyst

The invention discloses a preparation process for catalyzing and synthesizing tert-butyl acrylate by using strong acid cation exchange resin as a catalyst, belonging to the technical field of organic synthesis. The preparation process is characterized by comprising the steps of: adding crylic acid, strong acid cation exchange resin, a polymerization inhibitor A and a polymerization inhibitor B into a closed reaction kettle, dropwise adding liquefied isobutene for carrying out esterification reaction; after dropwise adding is completed, carrying out thermal insulation; after the thermal insulation is finished, releasing the pressure of the closed reaction kettle, filtering, extracting a liquid component to enter a rectifying tower; and sequentially separating byproducts of tertiary butanol and diisobutylene and a target project of the tert-butyl acrylate. The preparation process has the beneficial effects that the liquefied isobutene is adopted to be directly catalyzed together with the crylic acid and the cation exchange resin under the action of the polymerization inhibitor A and the polymerization inhibitor B to form a specific catalysis system, gaseous isobutene is not needed to be dissolved in a solvent containing crylic acid for carrying out esterification reaction under the action of the catalyst, and thus the procedure of absorbing a solvent in subsequent operation is removed, resources are saved and procedures are saved.
Owner:山东敏德化工有限公司

Method of evaporating sample injecting inducted by dielectric barrier discharge microplasma

The invention relates to a method of evaporating sample injecting inducted by dielectric barrier discharge microplasma. The method comprises steps that first a barrier discharge apparatus capable of producing microplasma is prepared, wherein the apparatus comprises a power, a switch, two insulating dielectric layers with concentric cylindrical pipe structure, two electrodes, an air inlet and a steam outlet; a discharge chamber is between the two dielectric layers, and an external electrode is covered outside the outer cylindrical pipe, and an inner electrode is inserted in the inner cylindrical pipe; and two electrodes are connected with the power; then a solution sample is added into a centrifuge tube, the inner cylindrical pipe of the dielectric barrier discharge apparatus is taken out and inserted into the centrifuge tube, and will be inserted back into the apparatus after sampling; carrier gas is let in, and the power is tuned on; the sample is absorbed by microplasma generated by dielectric barrier discharge; generated steam is purged by the carrier gas and enters a detector from the steam outlet, wherein the whole flow is finished in 90 s. The method is simply operated, without sample treatment, at low power dissipation, rapid and is especially suitable for analysis of small volume sample and trace and ultra trace elements.
Owner:CHINA UNIV OF GEOSCIENCES (WUHAN)

Three-dimensional color high-speed printer

InactiveCN104339652APrint job fastLow costEnvironmental resistanceEngineering
The present invention relates to a three-dimensional color high-speed printer, which comprises a moving printing sprayer, a color distribution ink supply box, a work tank, a computer and a peripheral circuit, wherein the work tank comprises a powder supply tank, a forming tank and an overflow tank, the powder supply tank, the forming tank and the overflow tank are laterally and sequentially arranged side by side, a lifting powder supply plate is arranged inside the powder supply tank, a lifting production platform is arranged inside the forming tank, two lateral bracket guide rails are flatly arranged on the work tank, the longitudinal ink roller device capable of laterally moving along the lateral bracket guide rails is arranged on the two lateral bracket guide rails, the two lateral bracket guide rails are further provided with longitudinal guide rails capable of laterally moving, the moving printing sprayer is movably arranged on the longitudinal guide rail, and the material outlet of the color distribution ink supply box is connected with the material inlet of the moving printing sprayer through an ink supply pipe. The three-dimensional color high-speed printer has characteristics of simple structure, easy operation, broad application range, good environmental protection, capability of outputting vibrant color model, and achievement of time-saving and rapid automated operation and easily-used printing process.
Owner:SHAANXI HENGTONG INTELLIGENT MACHINE

Full-dry purification method of lithium ion battery positive electrode material and lithium ion battery positive electrode material obtained through purification

The invention belongs to the technical field of comprehensive utilization of lithium ion battery positive electrode materials, and particularly relates to a full-dry purification method of a lithium ion battery positive electrode material and the lithium ion battery positive electrode material obtained through purification. The method comprises the following steps: (1) heating crushed materials ofa lithium battery positive electrode recycled material at a low temperature until an adhesive is invalid to obtain a mixture where a current collector and a lithium battery positive electrode to-be-purified material is separated; 2) performing vibration sieving on the mixture where the current collector and the lithium battery positive electrode to-be-purified material is separated to obtain thelithium battery positive electrode to-be-purified material from which the current collector is removed; and 3) carrying out sintering on the lithium battery positive electrode to-be-purified materialfrom which the current collector is removed to obtain the lithium battery positive electrode purified material. Full-dry purification of the lithium ion battery positive electrode material is realized, and the lithium battery positive electrode purified material obtained through purification is high in purity.
Owner:武汉瑞杰特材料有限责任公司

Flame-radiation-based combustion measuring apparatus and measuring method for solid rocket propellant

ActiveCN106482790ARealize online non-contact multi-parameter measurementNo need to deal withMeasurement devicesFiberOptical radiation
The invention provides a flame-radiation-based combustion measuring apparatus for a solid rocket propellant. The apparatus comprises a light convergence part, a plurality of spectral measurement parts, an ignition device, a control part, and a signal processing part. The light convergence part is formed by a plurality of light convergence devices arranged at the same straight line; the light convergence devices corresponding to the spectral measurement parts one by one; and the light convergence devices and the corresponding spectral measurement parts are connected by fibers. The control part is connected with the ignition device, the signal processing part, and the plurality of spectral measurement parts electrically. In addition, a measuring method based on the measuring apparatus is characterized in that temperature and radiance parameters are obtained by fitting of a flame radiation, so that the measuring precision of the optical radiation measuring method can be improved. And with combination of the array arrangement method, a combustion speed parameter can be obtained. For propellant combustion testing, multi-parameter simultaneous on-line non-contact measurement is realized; processing on a medical stick is avoided; and the apparatus is easy to repair.
Owner:ELECTROMECHANICAL ENG INST OF SICHUAN AEROSPACE +1

Separation and purification method for lithium ion battery positive electrode material and obtained lithium ion battery positive electrode material

PendingCN110808430AMild processing temperatureFewer temperature processing stepsPositive electrodesWaste accumulators reclaimingPhysicsChemistry
The invention belongs to the technical field of waste lithium ion battery recovery and resource cyclic utilization, and particularly relates to a separation and purification method for a lithium ion battery positive electrode material and the obtained lithium ion battery positive electrode material. The method comprises the following steps of: (1) heating crushed materials of a lithium battery positive electrode recycled material at a low temperature until an adhesive is invalid to obtain a mixture with a current collector and a to-be-purified lithium battery positive electrode material separated, 2) performing vibration screening on the mixture with the current collector and the to-be-purified lithium battery positive electrode material separated to obtain the to-be-purified lithium battery positive electrode material from which the current collector is separated, and 3) winnowing the to-be-purified lithium battery positive electrode material from which the current collector is separated to obtain the lithium battery positive electrode separation and purification material. Full-dry purification of the lithium ion battery positive electrode material is realized, and the lithium battery positive electrode purification material obtained by purification is high in purity.
Owner:武汉瑞杰特材料有限责任公司

Method for preparing CoSb3 nanometer particle film

The invention relates to a CoSb3 thermoelectric material, in particular to a method for preparing a CoSb3 nanometer particle film. The method comprises the following steps of: firstly, weighing CoC12.6H2O powder and Sb powder according to the molar ratio of 1:3; respectively filling the powder into respective crucible; putting the crucibles and glass slide substrates into a quartz pipe; placing the quartz pipe into a horizontal pipe type furnace; vacuumizing and aerating mixed air of 95 percent of argon and 5 percent of hydrogen for multiple times and removing oxygen in the quartz pipe; raising the temperature of the tubular pipe; performing chemical vapor deposition on the glass slide substrates in a low-pressure state to acquire the CoSb3 nanometer particle film; and testing Seebeck coefficient, conductivity and heat conductivity of the CoSb3 nanometer particle film and calculating a zone time (ZT) value of the CoSb3 nanometer particle film. According to the invention, the CoSb3 nanometer particle film is synthesized by one step, the process is simple, and the diameter of the prepared CoSb3 nanometer particle is between 200 and 400nm; and moreover, the CoSb3 thermoelectric material has good conductivity and low heat conductivity, can be directly used for thermoelectricity researches, and is used for novel high-efficiency thermoelectric conversion devices.
Owner:CHANGZHOU UNIV

Silicon carbide smelting waste gas collecting and purifying device

The invention discloses a silicon carbide smelting waste gas collecting and purifying device. The device comprises a fully-closed gas collecting hood of a silicon carbide smelting furnace, the silicon carbide smelting furnace is arranged in the gas collecting hood, one end of the gas collecting hood is communicated with a recycling pipeline system, the recycling pipeline system is communicated with a desulphurization and purification system through a pipeline, the desulphurization and purification system is communicated with an exhaust fan through a pipeline, and the exhaust fan is communicated with a gas storage device through a pipeline; the gas collecting hood is composed of a lower hood body and an upper hood body which are horizontally overlaid, second water sealing tanks are arranged between the lower hood body and the upper hood body and arranged between the lower hood body and the bottom face respectively, and a pressure relieving and sealing device is arranged at the top of the upper hood body. According to the device, collection is conducted through the fully-closed gas collecting hood, and the whole system runs under the micro-positive pressure, the zero pressure and the micro-negative pressure and is closed and not leaked; the hood bodies are divided into multiple sections, the lower hood body sections are installed in an interchanged mode, hoisting is convenient, the desulphurization and purification system can completely remove H2S generated in the smelting process, and collected CO can be directly reutilized without being treated.
Owner:NORTH CHINA UNIV OF WATER RESOURCES & ELECTRIC POWER

Method for catalyzing 2,5-dichlorotoluene reaction by modified H type molecular sieve

The invention relates to a method for catalyzing 2, 5-dichlorotoluene reaction by a modified H type molecular sieve, and belongs to the technical field of chlorotoluene derivatives. The method comprises the following steps: dissolving Cu(NO3)2 3H2O into distilled water, fully mixing and stirring with an H type molecular sieve after completely dissolving, standing for 12 hours under a condition that the environment temperature is 110 DEG C after standing and drying, and drying in a muffle furnace of which the temperature is 400 DEG C for 2 hours; performing a modified molecular sieve, grinding, sieving, and selecting sieved molecular sieve particles as a catalyst; filling a constant-temperature zone of a fixed bed reactor with the catalyst; conveying raw materials to the fixed bed reactor through a constant flow pump, and continuously bringing rapidly vaporized raw material steam in the constant-temperature zone into a catalyst bed layer through a gas; finally collecting a product through water bath condensation. According to the method disclosed by the invention, the modified H type molecular sieve is adopted as the catalyst, no toxicity and no harm exist, better stability and higher catalytic activity are obtained, cyclic and repeated utilization can be carried out, and sustained industrial production is facilitated.
Owner:MINGGUANG FEIZHOU NEW MATERIAL

Flue gas pollutant combination removal method based on high-activity solid absorbent

The invention provides a flue gas pollutant combination removal method based on a high-activity solid absorbent. The flue gas pollutant combination removal method comprises: uniformly mixing an oxidant into boil tail flue gas to obtain oxidized flue gas, wherein the NO in the flue gas is oxidized into a high-valence nitrogen oxide, and the zero-valence mercury is oxidized to a high-valence mercuride; making the oxidized flue gas completely contact solid particles, and simultaneously removing the sulfur oxide, the high-valence nitrogen oxide and the high-valence mercuride in the flue gas so asto obtain pollutant-removed dust-containing flue gas; and carrying out dust removing on the dust-containing flue gas to obtain clean flue gas, wherein the solid particles collected from the bottom portion of a dust removing device are fed into a material storage bin, the partial solid particles are activated and humidified, the activated and humidified solid particles returns to the reactor so asto continuously participate in the reaction, and the remaining solid particles are discharged from the bottom portion of the material storage bin so as to maintain the material balance. According to the present invention, the semi-dry absorption method is used, wherein the calcium-based absorbent is sprayed into the reactor in the form of the humidified solid particles, such that the water consumption is low, the final product is the solid-state product, the treatment of the wastewater is not required, the process is simple, and the method can be widely used in the industrial flue gas treatment.
Owner:CHINA COAL RES INST CCRI ENERGY SAVING TECH CO LTD
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