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139results about How to "Short degradation time" patented technology

Three-dimensional porous titanium substrate lead dioxide electrode as well as preparation method and application thereof

The invention discloses a three-dimensional porous titanium substrate lead dioxide electrode which comprises a porous titanium substrate, wherein interlayers are arranged on two side surfaces of the porous titanium substrate in a thermal deposition manner; the interlayers consists of a tin-antimony oxide; a lead dioxide surface active layer is arranged on the interlayer on one side surface of the porous titanium substrate in an electric deposition layer. The invention further provides a preparation method of the three-dimensional porous titanium substrate lead dioxide electrode, and further provides application of the three-dimensional porous titanium substrate lead dioxide electrode in musk ketone in degraded wastewater. In the musk ketone in the degraded wastewater, the three-dimensional porous titanium substrate lead dioxide electrode is taken as an anode, copper foil as a cathode and a sodium sulfate solution as an electrolyte, electrocatalytic oxidation is implemented for 1-2 hours, and then degradation treatment on the musk ketone in the wastewater can be completed. When the musk ketone is degraded by using the three-dimensional porous titanium substrate lead dioxide electrode under an electrifying condition, the degradation time is short, the degradation rate is high, and the operation is convenient.
Owner:SHANGHAI INST OF TECH

Preparation and application of titanium dioxide composite photocatalytic system

The invention discloses preparation and application of a titanium dioxide composite photocatalytic system. A preparation method comprises the steps of (1) nanometer gold preparation; (2) nanometer gold-carbon quantum dot preparation; (3) nanometer gold-carbon quantum dot-titanium dioxide composite system preparation. Visible light is used for performing photocatalytic performance test on the prepared composite material; the excellent photocatalytic performance of the material is proved by degrading organic pollutants of nonyl phenol. By starting from the angle of the composite material, the nanometer gold-carbon quantum dots are used as a titanium dioxide sensitizer; in visible light, after the photolytic activity sensitizer absorbs energy, free electrons are excited out; the electrons aretransferred onto a conduction band of titanium dioxide and then take a reduction reaction with organic matters; a good degradation effect is achieved. Nontoxic and harmless carbon quantum dots are used for modifying the titanium dioxide; a titanium dioxide visible light photocatalytic system is built; the absorption capacity and the catalytic activity of the system are improved; the degradation efficiency on pollutants is enhanced.
Owner:云南健牛环境监测有限公司

Multistage dynamic temporary blocking volume acid fracturing method

The invention discloses a multistage dynamic temporary blocking volume acid fracturing method. According to the multistage dynamic temporary blocking volume acid fracturing method,"multistage physical temporary blocking" and "multistage chemical temporary blocking" are treated as principle thinking, and multistage hydraulic fracturing with sand and multistage injection acid fracturing are combined. According to pump injection sequence of front-loading linear glue with certain concentration to make seams, saturating a reservoir, improving flow conductivity of fractures by propping agents with the small grain size or composite grain size, and injecting degradable acid-resistant fiber temporary blocking fluid, through multistage with large displacement, the fracture physical steering transformation is achieved; and then through a multistage interval type with large displacement, different types of acid liquors "mutual solvent, gelled acid, steering acid..., mutual agent" are injected, and thus fracture chemical temporary blocking steering transformation is achieved. According to the multistage dynamic temporary blocking volume acid fracturing method,the pertinence and the flow conductivity of the reservoir are improved, the loss of the acid liquors are lowered, the etching length of the fractures are increased, the transforming volume of the reservoir is enlarged by fracture steering, and thus the target that the individual well producing rate is improved by effective transformation of the cloud-like carbonate rock reservoir is achieved.
Owner:PETROCHINA CO LTD

Disposable movement tooth protecting socket and preparation method thereof

The invention relates to a disposable movement tooth protecting socket and a preparation method thereof. The preparation method of the disposable movement tooth protecting socket disclosed by the invention comprises purification and modification of konjac glucomannan, preparation of compound gel, degasification, molding and drying. The konjac glucomannan is taken as a carrier and assisted by other assistants; the disposable movement tooth protecting socket has excellent film-forming property, water-tightness, antibacterial property, large tensile strength, and good toughness; the konjac glucomannan is taken as a main material of the disposable movement tooth protecting socket. Compared with the existing movement tooth protecting socket, the disposable movement tooth protecting socket is high in tensile strength, and high in acid and alkali resistance, high-temperature resistance and antibacterial effect. The product is not degraded under normal use, can be completely degraded in soil under the conditions such as water, carbon dioxide, microorganisms, temperature and the like, is short in degradation time, convenient to draw materials, low in price and simple in production technology, accords with the national environment-friendly and low-carbon policy, and accords with the processing and production requirements of the disposable product. The disposable movement tooth protecting socket also has excellent performances such as antibacterial property, water resistance, breaking resistance, softness and the like.
Owner:FUJIAN AGRI & FORESTRY UNIV

Carbon nitride quantum dot/titanium dioxide sol and preparation method thereof

The invention relates to carbon nitride quantum dot / titanium dioxide sol. The titanium dioxide sol is prepared from titanium dioxide crystal grains, and a diffraction angle 2theta of the titanium dioxide sol has diffraction peaks at 8.78+ / -0.2 degrees, 26.66+ / -0.2 degrees, 38.8+ / -0.2 degrees, 46.75+ / -0.2 degrees, and 58.07+ / -0.2 degrees. A catalytic effect of a titanium dioxide composite materialprepared by the preparation method of the carbon nitride quantum dot / titanium dioxide sol is significantly improved, the degradation rate of 20mg commercial titanium dioxide P25 available in the market at present (brought from Degussa of German) for 100mL methyl orange (18mg / L) in 2 hours is 34.4 percent, and the degradation rate of the 20mg product provided by the invention under the same condition is 87.2 percent and is improved by 2.53 times; and the light current and impedance analysis test shows that the electron-hole is easy to separate, the quantum yield is high, no corrosive reagent isintroduced in the preparation process, the preparation method is environmentally friendly and free from secondary pollution, the product is good in stability and higher in catalytic effect when beingstored for 8 months at the room temperature, the preparation process is simple and feasible, and the industrialized production is easy to implement.
Owner:CHONGQING JIAOTONG UNIVERSITY

Calcined anionic clay visible-light catalyst and preparation method and purposes thereof

The invention discloses a calcined anionic clay visible-light catalyst and a preparation method and purposes thereof. The catalyst is prepared by the following steps of preparing mixed solution of metal salts and urea; heating the mixed solution to the temperature of between 100 and 120 DEG, reacting for 36 to 54 h, and obtaining acidic turbid liquid of which the pH value is between 6.0 and 6.5; centrifuging the acidic turbid liquid, taking precipitation out, washing the precipitation by deionized water until the pH value is neutral, and dewatering and drying; and grinding the dried precipitation, calcining the precipitation at the temperature of between 400 and 900 DEG C for 4 to 6 h, and thus obtaining the calcined anionic clay visible light catalyst, wherein the metal salts comprise divalent metal salts and trivalent metal salts. The prepared calcined anionic clay visible light catalyst can catalytically degrade organic wastewater in visible light, ultraviolet light equipment is not required, a feeding ratio is low, the degradation time is short, and the calcined anionic clay visible-light catalyst has low energy consumption and high efficiency and is suitable for the treatment of medium and low-concentration industrial wastewater.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method of nano titanium dioxide with photocatalytic performance

The invention belongs to the technical field of preparation methods of nano titanium dioxide and particularly relates to a preparation method of the nano titanium dioxide with photocatalytic performance. The invention mainly solves the problems of poor photocatalytic performance, long photodegradation period and low degradation rate of the nano titanium dioxide prepared by the existing preparation method. The preparation method comprises the following steps: taking ramie fiber or ramie-fiber carboxymethyl cellulose and tetrabutyl titanate, dimethyl sulfoxide and absolute ethyl alcohol, carrying out ultrasonic reaction under room temperature, after ultrasonic reaction is finished, placing in the air for 8-20 hours of aging under the room temperature, then carrying out suction filtration, cleaning with the absolute ethyl alcohol, drying for 5-10 hours at the temperature of 60-70 DEG C, and thus obtaining nano titanium dioxide / ramie-fiber composite material or nano titanium dioxide / ramie-fiber carboxymethyl cellulose composite material, and then calcining the composite material for 0.5-3 hours in the air atmosphere with the temperature of 200-1000 DEG C and the heating rate of 200 DEG C / h to obtain nano titanium dioxide with photocatalytic performance.
Owner:TAIYUAN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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