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156results about How to "Shorten Diffusion Time" patented technology

In situ deposit-aqueous interface water-quality sampler and sampling method thereof

The invention relates to an in situ deposit-aqueous interface water-quality sampler and a sampling method thereof. The sampler adopts a group of sampling plates and a group of protecting plates to clamp osmosis membranes and fix the osmosis membranes together by screws; the sampling plate is divided into an interstitial water sampling section of deposit and an overlying water sampling section of an interface in longitudinal direction; a plurality of transverse grooves which have longitudinal intervals of 2mm to 3mm are arranged on the interstitial water sampling section of deposit and the overlying water sampling section of the interface; the volume of the groove is between 2000microlitre to 4000microlitre; an interfacial limiting plate is arranged between the interstitial water sampling section of deposit and the overlying water sampling section of the interface; the sampler realizes in situ collection of deposit-aqueous interface water-quality samples, adopts an interfacial limiting device, and can accurately determine the deposit-aqueous interface; the sampler is equipped with a weight drop and a retrieve rope, can be used in aquatic deeper lakes, and has operability, site throwing and convenient retrieving; and the volume of each layer of water-quality sampling room reaches to 4000microlitre and can complete more index analysis simultaneously.
Owner:CHINESE RES ACAD OF ENVIRONMENTAL SCI

Method for preparing large powder metallurgy TZM blank with uniform carbon and oxygen distribution

The invention discloses a method for preparing a large powder metallurgy TZM blank with uniform carbon and oxygen distribution, which comprises the following steps of: 1, weighing raw materials; 2, mixing powder, namely mixing the weighed four raw materials twice under vacuum or the protection of inert gas, mixing titanium hydride powder, zirconium hydride powder and carbon black powder to prepare mixed powder, adding a volatile organic solvent into the mixed powder, uniformly stirring to prepare suspension, adding the weighed molybdenum powder into the suspension for uniform mixing, and adding residual molybdenum powder for uniform mixing; 3, performing cold isostatic pressing; and 4, sintering by keeping the temperature at stages, namely adopting a vacuum sintering furnace and sintering at three stages, wherein the process comprises the following steps of: raising the temperature at the first stage, raising the temperature at the second stage, and sintering at high temperature. The preparation method has the advantages of reasonable design, simple and convenient operation, and good using effect. The carbon content in the center and on the surface of the prepared larger-size TZM blank can be controlled to be approximately consistent, and the oxygen content in the center and on the surface of the TZM blank also can be reduced to a lower level.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

LiMn1-XFexPO4 positive electrode material having core-shell structure, and preparation method thereof, and lithium ion battery

The invention provides a core-shell structure positive electrode material, which comprises an inner core and a shell, wherein the inner core is LiMn1-XFexPO4 nanoparticles, the shell is a mixture of carbon and a lithium-containing metal salt, the lithium-containing metal salt is a lithium-containing metal phosphate and/or lithium-containing metal pyrophosphate, and x is more than 0 and is less than 0.5. According to the present invention, the LiMn1-XFexPO4 nanoparticles are adopted as the inner core, wherein the lithium ion diffusion path can be shortened, the time of the diffusion of the lithium ions among the particles can be reduced, and the material ion transmission performance can be improved with the nano-treatment of the material; and the mixture of the carbon and the lithium-containing metal phosphate and/or lithium-containing metal pyrophosphate is adopted as the coating layer, wherein the conductivity of the material ions can be increased and the carbon coating effect is effectively improved with the addition of the lithium-containing metal phosphate and/or lithium-containing metal pyrophosphate, such that the rate performance and the cycle performance of the core-shell structure positive electrode material are significantly improved, and the high compaction density is provided.
Owner:CHINA AVIATION LITHIUM BATTERY LUOYANG

Multicomponent gas adsorption simulation experiment method and device

The invention discloses a multicomponent gas adsorption simulation experiment method and a multicomponent gas adsorption simulation experiment device. The device includes a quantitative gas-charging system, an isothermal adsorption and desorption system, a vacuumizing device and a gas concentration analysis system. The method comprises the steps: firstly, carrying out high pressure gas injection experiments, injecting non methane gas by using high pressure to be mixed with methane, recording the adsorption equilibrium state of a coal body to the mixed gas, followed by, carrying out an isobaric diffusion experiment, and mixing the gas by using diffusion caused by concentration difference. Through qualitative and quantitative comparative analysis of two groups of experiments, the pressure effect can be separated from the comprehensive effects, and then a mechanism of action of the non methane gas on the methane in coal is studied. A complete set of experimental research system is developed, some technical problems under the isobaric diffusion experimental conditions are solved, diffusion problems of long diffusion path and small channels are solved, and the method and the device have important significance on studying adsorption characteristics of the gas in the coal.
Owner:HENAN POLYTECHNIC UNIV

Pcr-free sample preparation and detection systems for high speed biologic analysis and identification

Provided herein are biologic sample preparation and analysis systems that are rapid, portable, robust detection system for multiplexed detection of bio-threats, and which can be ruggedized to operate in harsh environments. A new method of detection called Combinatorial Probe Analysis (CPA), which provides an exponential increase in detection reliability, has been incorporated into these systems. This type of analysis greatly reduces false positives and false negatives; in addition it is reusable and eliminates special storage requirements for reagents. Specific technical advancements in the optimization of hybridization assays for nucleic acid detection on porous polymer monoliths (PPM) are also disclosed. Performing rapid and complete solubilization of viruses, vegetative bacteria and bacterial spores with an ultra high temperature solubilization protocol is also described. The systems provided herein provides the ability to perform rapid highly multiplexed analysis of a variety of bioagents, including bacteria viruses, and protein biotoxins. The systems and assays described herein are perform completely automated sample preparation and analysis, in a time frame of five minutes or less. The assay is simple in design allowing users in personal protective equipment to easily operate the system. The disclosed systems are robust, simple to use, and address the goals of the first responder community.
Owner:FLUIDIGM CORP

Device and method for measuring competitive adsorption quantity of carbon dioxide and alkane in shale

InactiveCN107063919AExperiment operation is simpleThe experimental operation is fastPermeability/surface area analysisAlkaneEngineering
The invention discloses a device for measuring the competitive adsorption quantity of carbon dioxide and alkane in shale. The device is characterized in that a reaction container cover is arranged at the upper end of a reaction container; a piston is arranged in the reaction container; the reaction container cover is communicated with a second three-way joint; the second three-way joint is connected with a first three-way joint; the second three-way joint is connected with a third three-way joint; the third three-way joint is connected with a first storage tank; the third three-way joint is connected with a second storage tank; electronic scales are arranged below the second storage tank and the first storage tank; the lower end of the reaction container is connected with a four-way joint; the four-way joint is connected with a pressure sensor; the four-way joint is connected with a metering pump; a first three-way valve is connected with a vacuum pump; and the first three-way valve is connected with an oil gas separator and a gas meter sequentially. The device has the advantages that whether adsorption is balanced or not is rapidly judged through pressure change, the problem that a shale core is difficult to take is solvd, experimental operation is simple and rapid, and the device has important guiding significance in applying CO2 to develop a shale oil reservoir.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA) +1

Self support high density metal oxide/nitrogen doped graphene composite electrode, and preparation method and application thereof

The invention discloses a self support high density metal oxide/nitrogen doped graphene composite electrode, and a preparation method and application thereof. The composite electrode is prepared by the following steps of firstly obtaining nitrogen doped graphene through water bath reaction; then, dispersing the nitrogen doped graphene into an organic solvent; dripping the organic solvent dissolvedwith metal salt; performing uniform dispersion; then performing hydrothermal reaction; preparing a powdery metal oxide/nitrogen doped graphene composite material; then, adding a small amount of graphene oxide so that the powdery metal oxide/nitrogen doped graphene composite material is uniformly dispersed into graphene oxide; preparing metal oxide/nitrogen doped graphene water gel through secondary hydrothermal reaction; finally performing slicing and natural shrinkage drying. The composite material has a self support structure; the density is greater than 1.0g/cm<3>; through a two-step hydrothermal method, an obtained electrode plate can be directly used as an electrode of a lithium ion battery or a sodium ion battery; the electric chemical performance of high volume capacity, high reversibility and high power performance is realized.
Owner:GUANGDONG UNIV OF TECH

Phosphorous gettering method of metallurgy polycrystalline silicon wafer, silicon wafer and solar cell prepared by silicon wafer

The invention provides a phosphorous gettering method of a metallurgy polycrystalline silicon wafer, a silicon wafer and a solar cell prepared by the silicon wafer The phosphorous gettering method includes: corroding to remove a damaged layer on the surface of the silicon wafer; rinsing the silicon wafer and drying; subjecting the silicon wafer to gettering heat treatment in a diffusion furnace, wherein the diffusion phosphorous source flow volume ranges from 650 to 700ml / min, dry oxygen flow volume ranges from 500 to 700ml / min, diffusing temperature ranges from 920 to 970 DEG C, and the diffusing time ranges from 30-45min; cooling the silicon wafer; corroding to remove a getter layer and PN junctions generated on the surface of the silicon wafer due to phosphorus diffusion; rinsing the silicon wafer and drying to obtain the gettered metallurgy polycrystalline silicon wafer. Service life of the silicon wafer is obviously prolonged, and reverse leakage current and light attenuation of the solar cell prepared by the silicon wafer are obviously reduced. The phosphorous gettering method is short in diffusing time, so that production period is shortened, energy consumption is reduced, and industrial production is suited.
Owner:INNER MONGOLIA RIYUE SOLAR ENERGY TECH
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