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280results about How to "Reduce agglomeration" patented technology

High temperature self-repairing conductive silver adhesive and preparation method thereof

The invention provides a high temperature self-repairing conductive silver adhesive. The high temperature self-repairing conductive silver adhesive is prepared from the following raw constituents by parts: 100 parts of epoxy resin, 10-30 parts of curing agent, 10-40 parts of epoxy diluent, 240-990 parts of silver pieces, 3-20 parts of coupling agent and 5-20 parts of self-repairing microcapsule; wherein the self-repairing microcapsule is composed of the following raw constituents by parts: 100 parts of epoxy resin, 8-20 parts of latent curing agent, 30-60 parts of diluents, 0.5-2.5 parts of emulsifying agent, 500-800 parts of nano silver wires, 5-16 parts of coupling agent, 60-120 parts of capsule wall material, 0.5-2 parts of antifoaming agent and 150-900 parts of deionized water. The invention also provides a preparation method of the high temperature self-repairing conductive silver adhesive. The high temperature self-repairing conductive silver adhesive has the positive effects that the repairing efficiency is high, the repairing effect is expanded on the basis of the original conductive network, crack-conductive network double repairing is realized, and the long-term using effect of the conductive adhesive is guaranteed, the cost is saved, and the reliability and service life of the conductive adhesive in high temperature working environment are improved.
Owner:CHINA ELECTRONIC TECH GRP CORP NO 38 RES INST

Functionalized graphene adsorbent and preparation method and application thereof

The invention discloses a functionalized graphene adsorbent and a preparation method and application of the functionalized graphene adsorbent. The adsorbent is mainly composed of grapheme and cetyl trimethyl ammonium bromide. The cetyl trimethyl ammonium bromide inserts into the edge or surface layer of the layered grapheme and or embeds into the edge or surface layer of the layered grapheme through the function of non-covalent bond. The mass fraction of the cetyl trimethyl ammonium bromide in the adsorbent is 40%-50%. The invention discloses the preparation method of the functionalized graphene adsorbent. The method comprises the steps of dispersing the graphene oxide into the water, adding cetyl trimethyl ammonium bromide to the dispersed suspension liquid and stirring to make reaction, then adding suspension liquid to the heated reaction system and conducting suction filtration, washing and drying to the black cotton-shaped precipitate obtained by reduction. The functionalized graphene adsorbent can wipe out the chrome in the waste. The adsorbent is added into the chromate waste water, control the temperature of the waste, then after the full adsorption and complete oscillatory removal of the chromate is completed. The functionalized graphene adsorbent and a preparation method and application of the functionalized graphene adsorbent has the advantages of being simple, high efficient, green, economical and environmental and the like.
Owner:湖南红普创新科技发展有限公司

Compound grapheme absorption agent, method for preparing compound grapheme absorption agent and application of compound grapheme absorption agent

The invention discloses a compound grapheme absorption agent which comprises grapheme, nanometer zero-valent iron and cetyl trimethyl ammonium bromide. The invention further discloses a method for preparing the compound grapheme absorption agent. The method for preparing the compound grapheme absorption agent includes the following steps that firstly, oxidized grapheme is dispersed in water with ultrasonic waves and oxidized grapheme suspension liquid is obtained; secondly, the nanometer zero-valent iron and the cetyl trimethyl ammonium bromide are added into the oxidized grapheme suspension liquid obtained in the first step, fully stirred and fully reacted and a reaction solution is obtained; thirdly, the reaction solution obtained in the second step is added with reductive agents and fully reacted and black flocks are obtained; fourthly, the black flocks obtained in the third step are filtered, washed and dried to obtain the compound grapheme absorption agent. The compound grapheme absorption agent is efficient, green, economic, friendly to environment, and suitable for large-scale production. The preparing method is simple and conditions are easy to control.
Owner:SOUTH CHINA UNIV OF TECH

Oxidized graphite flake layer/polyaniline composite material and method for preparing the same

The invention relates to oxidized graphite sheet layer/polyaniline composite material and a preparation method thereof. The composite material is prepared by the following steps: the oxidized graphite is added into a dispersant for ultrasonic dispersion so as to form homodispersed single-sheet layer oxidized graphite mixed liquor; at the room temperature, aniline is added into the mixed liquor obtained in the first step drop by drop, and the ultrasonic dispersion is carried out to form the mixed liquor; a solution obtained by adding an oxidant into doping acid is dropwise added into the mixed liquor obtained in the second step for stirring and polymerization; the mixed liquor obtained in the third step is centrifugated, washed and dried in vacuum so as to obtain the oxidized graphite sheet layer/polyaniline composite material. The invention takes full advantages of big specific area of the oxidized graphite and surface oxygroup group to form binding sites and is organically combined with polyaniline skeleton by the chemical doping function of carboxylic acid group on the single-sheet layer of the oxidized graphite so as to form oxidized graphite/polyaniline complex; the operation process of preparing the product is simple, the production period thereof is short, the yield is high and the requirements on devices are low.
Owner:NANJING UNIV OF SCI & TECH

Preparation method of graphene heat conducting film

The invention provides a preparation method of a graphene heat conducting film and belongs to the technical field of graphene materials. The problems that according to the conventional preparation method of the graphene heat conducting film, the technology is complicated and obtained graphene is low in orientation degree, poor in heat conducting property and low in tensile strength are solved. The method comprises: first soaking graphite in an acid-blended solution, and then adding an intercalator and stirring the mixture so as to obtain a mixed solution; then, adding an organic reagent into the mixed solution for reaction so as to obtain graphene aqueous dispersion; adding natural plant macrofibers or polymer macrofibers into the graphene aqueous dispersion, and carrying out ultrasonic processing so as to obtain fiber and graphene mixed dispersion; and finally arranging the fiber and graphene mixed dispersion on a substrate, and processing a film obtained after drying at a temperature of 500-900 DEG C for 15-30 minutes so as to obtain the graphene heat conducting film. The graphene heat conducting film prepared by the method has high orientation degree. The heat conducting coefficient can reach 1000-1500W / mK, and the mechanical tensile strength can reach 30-70MPa.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Catalyst for hydrogen production through catalytic cracking of methane and its preparation method

Belonging to the technical field of catalysts for hydrogen production through catalytic cracking of methane, the invention relates to a catalyst for hydrogen production through catalytic cracking of methane and its preparation method. The catalyst in the invention is composed of a nickel salt, copper oxide, a precious metal catalytic promoter, an alkaline earth metal catalytic promoter, and a nanometer ZrO-ZnO composite carrier. The method in the invention comprises: taking the nickel salt, the copper oxide, the precious metal catalytic promoter, the alkaline earth metal catalytic promoter, azirconium salt, a zinc salt, and an alkaline precipitating agent as raw materials, first preparing a nanometer ZrO-ZnO composite carrier, then implementing the simple processes of mixing, ultrasonic dispersion, roasting, and moulding, thus obtaining a product. The method in the invention has the advantages of simple process, mild reaction condition, energy saving, sufficient material and liquid utilization, and no discharge of ''three wastes''. The product prepared by the method of the invention has the characteristics of high activity, good dispersibility, and strong temperature resistance, etc. The catalyst prepared by the method provided in the invention can be widely applied in catalytic cracking of methane, ethane and other low carbon alkanes, and is especially suitable for catalyticcracking of methane in a fluidized bed for hydrogen production.
Owner:CHONGQING UNIV

Aluminum-based material and preparation method thereof

The invention discloses an aluminum-based material. Aluminum nitride, zirconium oxide and tantalum oxide particles are uniformly distributed in an aluminum alloy substrate, MoS2, Al2O3 and SiC are distributed on part of a surface layer of the aluminum alloy substrate, the hardness of aluminum nitride, zirconium oxide and tantalum oxide is high, the hardness and wear-resisting performance of the substrate are significantly improved, and fluorinated graphite powder can improve the anti-friction property. The surface of the substrate is coated with a Mn-Cr coating in a fusion mode to effectivelyimprove the wear-resisting performance and corrosion resistance of the alloy surface. The dispersion strengthening of strengthening phases of Si, Cu, Cr, Ni, Hf, Fe, Ag, Ca, Li, Ba and other elementsin the alloy improves the mechanical properties of the material. A preparation method enables mixed powder to be located in the center of a master alloy solution during casting through a method by adhering the mixed powder to a pure aluminum metal wire, the rapid diffusion and homogenization of micro powder particles is facilitated, the production efficiency is improved, wear-resistant materials are locally added by friction stir machining, and the material utilization ratio is improved.
Owner:ANHUI POLYTECHNIC UNIV MECHANICAL & ELECTRICAL COLLEGE
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