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88results about How to "Reduce enrichment costs" patented technology

Method for concentrating and purifying titanium dioxide waste acid by using complex acid

The invention discloses a method for concentrating and purifying titanium dioxide waste acid by using complex acid. The method comprises the following specific steps of: titanium recovery: primarily concentrating waste acid produced in a titanium dioxide production process by using waste heat of calcining tail gas of a ring kiln to achieve the mass concentration being 25-32%, and then recovering titanium; acid mixing: uniformly mixing the waste acid subjected to titanium recovery and concentrated sulfuric acid in an acid mixing tank according to a mass proportion of (1.2-4):1 to obtain mixed acid; and crystallization: carrying out gradient cooling, crystallizing, curing and filtering on the mixed acid gradually in the acid mixing tank, and when the temperature of the mixed acid is reduced to 60-65 DEG C, pumping the mixed acid into a filter press for solid-liquid separation to obtain concentrated sulfuric acid and ferrous dregs. The method disclosed by the invention has the advantage of changing the traditional method for concentrating the titanium dioxide waste acid by depending on natural gas, steam, fire coal hot gas and other heat sources, is free from consuming a large amount of energy sources and capable of reducing the cost in waste acid concentration, and is high in recovery rate of the waste acid.
Owner:SICHUAN LOMON TITANIUM IND CO LTD

High-desalting-rate seawater desalination method and device based on liquefied natural gas cold energy

The invention discloses a high-desalting-rate seawater desalination method based on liquefied natural gas cold energy, which comprises the following steps: sufficiently carrying out indirect heat exchange on liquefied natural gas and a gas-state secondary coolant, and sufficiently carrying out indirect heat exchange on the obtained liquid-state secondary coolant and seawater to obtain ice and concentrated seawater; (2) taking the ice obtained in the step (1), standing under atmospheric pressure until the melting rate of ice is 10-50%, recovering the liquid, and taking the residual ice for later use; (3) crushing the residual ice obtained in the step (2) to obtain ice crystal granules, centrifuging, recovering the liquid, and taking the ice crystal granules for later use; and (4) completely melting the ice crystal granules obtained in the step (3). The invention also discloses a seawater desalination plant based on liquefied natural gas cold energy. The method utilizes the cold energy released in the liquefied natural gas gasification process, comprehensively utilizes the freeze desalting, gravity desalting and centrifuging desalting techniques, has the advantages of simple steps, energy saving and environment friendliness, and enhances the seawater desalting rate on the basis of freeze desalting.
Owner:CHINA PETROLEUM & CHEM CORP +1

Production scheme and preparation method of converting biogas slurry into organic fertilizer

The invention relates to the field of preparation of high-quality organic fertilizer by recycling waste, and concentrates biogas slurry to obtain organic fertilizer and reusable water by utilizing the principle of reverse osmosis. The invention particularly relates to a production scheme and a preparation method of converting biogas slurry into organic fertilizer. The production scheme and the preparation method of converting biogas slurry into organic fertilizer are characterized by comprising the following steps: (A) sand filtration treatment: pumping the biogas slurry into a steel tank filled with quartz sand, and filtering out the large dross; (B) reverse osmosis treatment: pressurizing the biogas slurry, and separating water from the biogas slurry by using the principle of reverse osmosis, thereby obtaining the biogas slurry concentrate; (C) ozone sterilization: sterilizing the water obtained through the reverse osmosis with ozone, and recycling the water; (D) addition of effective ingredients: recycling the concentrated biogas slurry, carrying out the chemical examination, and adding corresponding ingredients according to different operating requirements; and (E) fermentation with beneficial bacteria: fermenting the prepared concentrate with beneficial bacteria and packaging.
Owner:王耘

Dilute sulfuric acid vacuum concentration device and method

The invention relates to a dilute sulfuric acid vacuum concentration device and method. The method comprises the following steps: performing metering control on 65-75% of dilute sulfuric acid, enabling the dilute sulfuric acid to enter an acid-acid heat exchanger, preheating the raw material acid by utilizing waste heat of acid discharged by a secondary sulfuric acid thickener, and treating in a primary sulfuric acid thickener; overflowing the treated acid in the secondary sulfuric acid thickener to be treated; enabling acid-containing water vapor produced by the primary sulfuric acid thickener to enter a primary tail gas condenser, overflowing condensed and separated water vapor to enter a wastewater collection tank, and discharging noncondensable gas, acid gas and a small amount of watervapor by a multistage steam jet vacuum pump set and feeding into an accident chlorine tail gas tower to be purified; enabling the acid-containing water vapor produced by the secondary sulfuric acid thickener to enter a secondary tail gas condenser, overflowing the condensed and separated water vapor to enter a wastewater collection tank, and discharging the noncondensable gas, acid gas and a small amount of water vapor by the multistage steam jet vacuum pump set and feeding into the accident chlorine tail gas tower to be purified. The dilute sulfuric acid vacuum concentration device disclosedby the invention has the advantages of being low in cost, low in energy consumption, good in treatment effect, high in reliability, stable in operation and the like.
Owner:杭州东日节能技术有限公司

High-content jujube cyclic adenosine monophosphate extract and preparation method thereof

The invention provides a high-content jujube cyclic adenosine monophosphate extract and a preparation method thereof. The concentration of cyclic adenosine monophosphate in the extract is more than 15mg / 100g, solid or semi-solid jujubes are taken as raw materials, and the preparation method comprises the steps of extracting by a continuous low-temperature extractor with high pressure difference, concentrating an extraction solution, performing vacuum drying and crushing to obtain a jujube crude extract; extracting the crude extract by adopting a supercritical extraction technology to obtain the jujube cyclic adenosine monophosphate extract. The jujube cyclic adenosine monophosphate extract has prominent effects in the aspects of hypoxia resistance, fatigue resistance and improvement of life quality. The preparation method has the following obvious advantages: (1) the extraction transfer rate is high; (2) the production efficiency is high; (3) the quality controllability is high; (4) the operation controllable degree is high; (5) the comprehensive utilization rate of resources is high; (6) the comprehensive operation cost is low; (7) the degree of automation is high; (8) the environmental pollution is little.
Owner:中恩(天津)医药科技有限公司

Reverse osmosis strong brine concentration method and equipment

The invention discloses a reverse osmosis strong brine concentration method and equipment. The concentration method comprises the following processes of (1) a positive osmosis concentration process: using reverse osmosis strong brine as raw material liquid, so that the water in the raw material liquid passes through a positive osmosis film to enter the liquid suction side through the effect of suction liquid, salt in the raw material liquid is intercepted at the raw material liquid side, and the raw material liquid can be concentrated; (2) a film distillation concentration process: conveying the raw material liquid concentrated in the step (1) to a hot side of a film distillation film; performing cooling by circulation water at the cold side of the film distillation film or vacuum suction,so that the water at the hot side passes through the film distillation film in a water vapor form to enter the cold side, the raw material liquid at the hot side loses water, and the raw material liquid is further concentrated. The concentration equipment comprises a positive osmosis device, a film distillation device and a strong brine tank. According to the concentration method and equipment, the positive osmosis is used as the film distillation pretreatment technology to perform deep concentration on the reverse osmosis strong brine, so that the whole energy consumption is reduced; the treatment of the reverse osmosis strong brine and the subsequent resource utilization are realized at low energy consumption and high concentration efficiency.
Owner:BEIJING FORESTRY UNIVERSITY

Adipic acid waste water evaporation and concentration process and device thereof

The invention relates to an adipic acid waste water evaporation and concentration process. The adipic acid waste water evaporation and concentration process comprises the following steps that firstly, a material is preheated; secondly, preheated material enters a film falling heat exchanger to be heated, and gas-liquid mixture is formed; thirdly, the gas-liquid mixture enters the film falling heat exchanger to be subjected to gas-liquid separation, and a concentrated solution returns to the film falling heat exchanger; fourthly, after the concentration ratio of the material in the film falling heat exchanger reaches a preset value, the material is transferred out, heated and concentrated by a forced circulation heat exchanger and then fed into the gas-liquid separator to be subjected to further gas-liquid separation; fifthly, the material is further concentrated in the gas-liquid separator, when the concentration ratio meets the requirement, the material is discharged, secondary steam enters a compressor to be compressed, and after the temperature is raised, the material continues to be heated. The concentration of adipic acid in the adipic acid waste water is effectively increased, the energy consumption is saved, and the concentration cost is reduced; after the concentration of the adipic acid solution is improved, oxalic acid crystals are separated out conveniently, and the environment pollution is reduced.
Owner:JIANGSU RUISHENGHUA ENERGY TECH CO LTD

Method for treating glyphosate mother liquor

The invention provides a method for treating glyphosate mother liquor. The method comprises the following steps: introducing dimethylamine gas into the bottom of a gas-liquid countercurrent packed tower, absorbing the dimethylamine gas through taking the glyphosate mother liquor as an absorbent and collecting alkaline liquid at the bottom of the tower; introducing the liquid into a rectifying tower for rectification to obtain triethylamine and tower bottom liquid; dehydrating the tower bottom liquid at reduced pressure, adding hydrochloric acid to adjust the pH value of the tower bottom liquid to strong acidity, cooling, crystallizing and filtering to obtain glyphosate; and further distilling the filtered filtrate at reduced pressure to obtain dimethylamine hydrochloride. Compared with the prior art, the method provided by the invention has the advantages that the dimethylamine gas is utilized to replace other liquid alkalies to recover the catalyst triethylamine in the glyphosate mother liquor, the obtained glyphosate and the dimethylamine hydrochloride are useful chemical products and no waste is produced, so that the method is high in recovery rate, high in recovery product quality, friendly to environment and economic; in the meanwhile, the gas-liquid countercurrent packed tower is adopted in the method, so that the method is more safe in reaction and is beneficial to the continuous and large scale treatment of the glyphosate mother liquor.
Owner:HEBI NONGLIN PHARMA

Processing method of casting zinc dross

The invention discloses a processing method of casting zinc dross. The processing method comprises the steps of adding water and the casting zinc dross into a washing trough when stirring at room temperature, adjusting the final pH value of washing liquid to 9-11 using hydrated lime powder, washing the casting zinc dross for 10-30 minutes, filtering to obtain filtrate and filtration residue, washing the filtration residue using tap water at room temperature and in the liquid-solid ratio of (3:1):(5:1) for 10-30 minutes, filtering to obtain the filtrate and filtration residue, returning the filtration residue to a zinc system to produce electrodeposited zinc, returning the filtrate to the lime water washing procedure, subjecting the lime water washed filtrate to electrodialysis concentration,subjecting the electrodialysis purified liquid to the separation treatment by means of reverse osmosis membrane technology, returning the reverse osmosis concentrated liquid to the electrodialysis procedure for processing, returning the reverse osmosis membrane purified liquid to the tap water washing procedure, and vaporizing and concentrating the electrodialysis concentrated liquid to produce the product of calcium chloride. By adopting the processing method provided by the invention, chlorine can be fast removed from the casting zinc dross, the metal zinc can be recycled, the product of calcium chloride can be simultaneously produced, and the whole process procedures do not produce waste water.
Owner:LAIBIN CHINA TIN SMELTING

Method for preparing concentrated liquid fertilizer by using wastewater containing livestock excrement

The invention discloses a method for preparing a concentrated liquid fertilizer by using wastewater containing livestock excrement. The method comprises the following steps: adding acids to immobilize amino and keep fertilizers; adding quicklime to neutralize excessive acids; performing primary fermentation so as to increase the dissolution degree of organic fertilizers; performing solid-liquid separation; performing negative-pressure concentration; and performing secondary fermentation on a concentrated liquid, thereby obtaining a livestock excrement concentrated liquid fertilizer. The method is simple in concentration process, good in operability and low in concentration cost; the solution degree of fertilizer components in the organic liquid fertilizer is high; due to amino immobilization and fertilizer increase of acids, and alcohol for increasing the dissolution degree of livestock excrement in the wastewater, the organic fertilizers can be relatively thoroughly dissolved in the wastewater, the cost of negative pressure concentration is reduced, the alcohol and the water can be both recycled, and the utilization rate of the livestock excrement is effectively increased; and by adopting the method, wastewater containing livestock excrement generated in the on-scale livestock breeding process can be turned into a high-concentration organic fertilizer, so that wastewater treatment in the on-scale livestock breeding process is solved, and harmonious development of agriculture, on-scale livestock breeding and living environments of people is promoted.
Owner:朱和平

A self-born crystal seed for hydrolysis in titanium dioxide production and a preparing method thereof

The invention relates to a self-born crystal seed for hydrolysis in titanium dioxide production and a preparing method thereof, and belongs to the technical field of chemical engineering. The method includes adding a titanium solution into base water and fully mixing the mixture to obtain self-born crystal seeds. The amount of the base water is calculated to control the total titanium concentration, calculated based on TiO2, of a hydrolysis system to be 155-175 g/L according to the concentration of the initial titanium solution. The base water is prepared by adding sulfuric acid or sodium hydroxide into water and fully mixing the mixture. The dosage of the sulfuric acid or sodium hydroxide meets a condition that when the titanium solution is added into the base water and the amount of theadded titanium solution is 3.0-3.5% of the volume of the total titanium solution, the concentration of sulfuric acid of the whole reaction system is 0.6 +/- 0.02 mol/L. A present process for producingtitanium dioxide self-born crystal seeds through a sulfuric acid method is utilized, the base water amount for initial formation of the self-born crystal seeds and the acidity of a critical point arecontrolled to obtain hydrolysis seeds of a proper amount and proper mass, and pigment titanium dioxide with good structures and excellent performance can be prepared.
Owner:攀枝花兴中钛业有限公司

Multi-step efficient enzyme hydrolysis process method of lignocellulose

The invention discloses a multi-step efficient enzyme hydrolysis process method of lignocellulose. The method comprises the following steps of 1, feeding a fresh lignocellulose raw material, cellulase and water into a first enzyme hydrolysis tank, and performing hydrolysis under a condition of certain temperature and pH value; 2, after the first enzyme hydrolysis reaction in the step 1 is finished, performing solid-liquid separation, wherein the liquid obtained through separation is directly taken out to be used as a sugar product, and the solid obtained through separation is directly fed into a second enzyme hydrolysis tank to be reacted; 3, after the second enzyme hydrolysis reaction in the step 2 is finished, performing solid-liquid separation, wherein the liquid obtained through separation is conveyed into the first enzyme hydrolysis tank to continuously participate in the enzyme hydrolysis reaction, and the solid obtained through separation is directly fed into a third enzyme hydrolysis tank to be continuously reacted; etc.and n, after the (n-1)th enzyme hydrolysis reaction in the step (n-1) is finished, performing solid-liquid separation, wherein the liquid obtained through separation is conveyed into the (n-2)th enzyme hydrolysis tank to continuously participate in the enzyme hydrolysis reaction, and the solid obtained through separation is directly fed into an nth enzyme hydrolysis tank to be continuously reacted.
Owner:QINGDAO INST OF BIOENERGY & BIOPROCESS TECH CHINESE ACADEMY OF SCI
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