The utility model discloses a kind of anti-clogging continuous glacial
acetic acid rectification purification device, including sequentially connected
raw material tank, preheater, rectifying
tower, the outside of the
raw material tank is equipped with first heat-preservation jacket, the outside of the rectifying
tower is equipped with second heat-preservation jacket, the pipeline between the rectifying
tower and the preheater is equipped with
polymerization inhibitor
injection port;The
gas phase outlet of the top of the rectifying tower is connected with main condenser, the main condenser connects
reflux tank, the
reflux tank is connected product cooler by
reflux pump, and the product cooler is connected with product
storage tank;The
liquid phase outlet of the bottom of the rectifying tower is connected with
reboiler, and the
reboiler is also connected with the rectifying tower, and the pipeline between the
liquid phase outlet and the
reboiler is also equipped with
recovery tank.The utility model can present glacial
acetic acid's high-purity continuous stable production, solve or greatly alleviate
crystallization plugging problem in rectification process.