The invention provides a morphology-adjustable
molybdenum disulfide preparation method and relates to a method for preparing morphology-adjustable
molybdenum disulfide through a mixed
solvent hot method. The preparation method comprises fully stirring
ammonium molybdate and
thiourea as initial reactants through a
magnetic stirrer through adjustment of a ratio of
ethanol to deionized water in a mixed
solvent until the drugs are fully dissolved so that a uniform, stable and transparent solution is obtained, pouring the solution into the lining of a
polytetrafluoroethylene reactor, putting the
polytetrafluoroethylene reactor into a stainless steel-made
high pressure reaction vessel, carrying out a
solvent heat reaction process under control of a
reaction temperature and reaction time, cooling the product to the
room temperature in air, collecting the samples, and carrying out
centrifugation, washing and
drying to obtain morphology-adjustable
molybdenum disulfide. At a certain temperature, in a certain reaction time,
molybdenum disulfide products with different morphologies are obtained through control of
reaction conditions. The
molybdenum disulfide products with different morphologies can effectively adjust
catalysis performances. The preparation method has the advantages of simple processes, good product uniformity and
batch production feasibility.