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199results about How to "Little change in viscosity" patented technology

Li-ion positive electrode slurry and preparation method thereof

InactiveCN103346318AEvenly dispersedSolve the defect of easy reunionCell electrodesLithium iron phosphatePyrrolidinones
The invention provides a Li-ion positive electrode slurry and a preparation method thereof. The preparation method comprises the following steps of: mixing lithium iron phosphate and dry inorganic conductive agent powder, wherein uniform mixing is judged by randomly sampling and measuring the resistance value of the powder, and is considered to be achieved when the difference of the resistance value of each sample powder is less than 5%; then adding PVDF (Polyvinylidene Fluoride) colloidal fluid into the mixture step by step; finally regulating the viscosity of the slurry by utilizing 1-Methyl-2-pyrrolidinone, thereby obtaining the Li-ion positive electrode slurry. The viscosity of the Li-ion positive electrode slurry is 3000-5000cps, and the Li-ion positive electrode slurry comprises 1-methyl-2-pyrrolidinone, as well as lithium iron phosphate, polyvinylidene fluoride and the inorganic conductive agent which are at a mass ratio of (85-95):(3-8):(2-10). According to the preparation method, whether the inorganic conductive agent is uniformly dispersed in lithium iron phosphate is determined by a method of randomly sampling dry powder, mixing samples and measuring the resistance values, and meanwhile, the PVDF colloidal fluid is added step by step in a substep slurry preparation process, so that the conventional thought of firstly mixing solid materials and adding the colloidal fluid in one step in a slurry preparation process in the field is broken through, and a favorable slurry preparation effect is achieved.
Owner:IRICO

Preparation method and usage method of low-viscosity flame-retardant heat-conducting solvent-free polyurethane electronic-pouring sealant

The invention discloses a preparation method and a usage method of a low-viscosity flame-retardant heat-conducting solvent-free polyurethane electronic-pouring sealant. The electronic-pouring sealant comprises a component A and a component B, wherein the component A is prepared by means of the following process: adding 100 parts of castor oil, 5 to 15 parts of flame retardant, 1 to 5 parts of high heat conductive insulation composite powder and 0.05 to 3 parts of an anti-foaming agent into a reaction kettle in parts by mass, performing uniform mixing and vacuum dehydration, then adding 0.05 to 0.3 part of a catalyst, and performing uniform mixing to obtain the component A; and the component B is liquefied diphenylmethylene diisocyanate. In the invention, a high heat conductive insulation composite powder heat conduction technology, a polyurethane in-situ polymerization self-flame-retardant technology and a thermal sensitive catalyst asynchronous catalysis technology are adopted, the product viscosity is smaller than 6000mPa.s, the heat conduction coefficient is greater than 1.85W/MK, the volume resistivity is greater than 4.2*10<12>omega.m, and the flame retardant property can be up to the American FMVSS302 standard.
Owner:SHAANXI UNIV OF SCI & TECH

High-covering black UV silkscreen printing ink

The invention discloses a high-covering black UV silkscreen printing ink. A preparation method for the high-covering black UV silkscreen printing ink comprises the following steps: preheating acrylate and then mixing the preheated acrylate with a part of active monomer; then adding a dispersant and carrying out primary dispersion; then successively adding pigment and a filling material and carrying out secondary dispersion; carrying out grinding to obtain color paste; mixing a phosphine oxide photoinitiator with residual active monomer; and adding the color paste, an organosilicon antifoaming agent and an organosilicon leveling agent and carrying out uniform dispersion so as to obtain the high-covering black UV silkscreen printing ink. The high-covering black UV silkscreen printing ink provided by the invention is reasonable in composition; all the components are in good compatibility; and the prepared printing ink has excellent comprehensive properties and good storage performance, and the viscosity of the printing ink is suitable for silkscreen printing. The printing ink does not need increase in the usage amounts of components like carbon black, prevents unfavorable influence of the components on the appearance and light shading performance of a product, and can meet light shading requirements of the product after only one printing and under the condition of a thickness of 7 to 8 micrometers, so unexpected technical effects are obtained.
Owner:SUZHOU BETELY POLYMER MATERIALS CO LTD

Halogen-free and lead-free solder paste and preparation method

The invention relates to a halogen-free and lead-free solder paste and a preparation method. The preparation method is characterized in that the method comprises the steps of adding diethylene glycol monobutyl ether, castor oil and polyisobutene in a temperature control emulsifying machine and mixing, then adding albolene, polymerized rosin and hydrogenated rosin and mixing again to obtain first mixing solution, reducing the temperature of the first mixing solution, adding succinic acid, sebacic acid and glutaric acid, and mixing again to obtain second mixing solution, reducing the temperature of the second mixing solution, adding polyamide wax and mixing again to obtain third mixing solution, reducing the temperature of the third mixing solution, adding a fluorocarbon surfactant and diethanol amine, then stirring and vacuuming until the temperature is restored to the room temperature, standing for 24h with low temperature, then adding lead-free electronic-grade tin alloyed powder Sn96.5Ag3.0Cu0.5, and stirring to obtain the halogen-free and lead-free solder paste. After being welded, the halogen-free and lead-free solder paste has the advantages and effects of fewer residues, extremely high surface insulation resistance, low corrosion, no needing of cleaning, good thixotropic property and electric conductivity, bright welding points after welding and incapability of collapsing easily.
Owner:惠州市斯泰尔科技有限公司

Carbide high-entropy ceramic precursor containing rare earth, high-entropy ceramic and preparation method

ActiveCN111303581AGood storage performanceLittle change in viscosityRare-earth elementPropanol
The invention discloses a carbide high-entropy ceramic precursor containing rare earth. The precursor comprises at least four transition metal elements and at least one rare earth metal element, and the precursor is dissolved in one or more of methanol, ethanol, isopropanol, n-propanol, n-butanol, isobutanol, ethylene glycol monomethyl ether or ethylene glycol ethyl ether. The precursor is prepared by respectively complexing a plurality of transition metal alkoxides, mixing the obtained complex with a compound containing rare earth elements, carrying out co-hydrolysis, and performing reactionwith a carbon source. According to the preparation method of the precursor, the ratio of all the raw materials in the step is finely adjusted, so that all the elements in the precursor are uniformly distributed at a molecular level, all the metal elements are subjected to short-range diffusion in the cracking process, and all the elements can be subjected to solid solution at a relatively low temperature. The preparation of the high-entropy ceramic is different from laser sintering and oxidation reduction in a traditional method, and the high-performance ceramic with a single crystalline phaseand with all elements in a molecular-level uniform distribution state is prepared on the basis of the precursor.
Owner:INST OF CHEM CHINESE ACAD OF SCI
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