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38results about How to "Strong resistance to hydrolysis" patented technology

Underground gel-forming blocking agent suitable for medium-high temperature high-salt low-permeability reservoirs and preparation method therefor

ActiveCN104974724AStrong ability to delay polycondensation and solidificationEffective blockingDrilling compositionChromatographic separationConcentration ratio
The invention provides an underground gel-forming blocking agent suitable for medium-high temperature high-salt low-permeability reservoirs and a preparation method therefor. By taking the total weight of the blocking agent as reference, the blocking agent comprises the following raw materials: 1% to 4% of water-soluble phenol-formaldehyde resin, 0.5% to 2% of stabilizer, 0 to 10% of flexibilizer and the balance of water. The preparation method of the blocking agent comprises the following steps: selecting the raw materials in proportion, and uniformly mixing so as to obtain the underground gel-forming blocking agent suitable for the medium-high temperature high-salt low-permeability reservoirs. The blocking agent provided by the invention is a homogeneous-phase, transparent and low-viscosity water solution before gel forming; the blocking agent can be selectively injected in a deep stratum water flow preferential migration passage, the shearing, adsorption and chromatographic separation of a stratum for the blocking agent can be ignored, and deep placement does not influence the concentration ratio of the blocking agent; and the polycondensation is delayed at the high temperature in the deep stratum, so that the formed gel has the advantages of high blocking rate, high blocking strength, water flow impact resistance, high temperature resistance and high hydrolysis resistance.
Owner:PETROCHINA CO LTD

Well drilling waste brick making method

The invention discloses a well drilling waste brick making method. The well drilling waste brick making method comprises the following steps that dirt elimination and desiccation treatment is conducted on well drilling waste to be treated with a dirt elimination and desiccation agent; a construction binding material and a construction aggregate are added to the well drilling waste, to be treated, obtained after dirt elimination and desiccation treatment, even mixing is conducted, and then a brick making mixture is obtained; the brick making mixture is solidified and pressed to be green bricks with the density not smaller than 80% by means of a static pressure type brick making machine; strength maintenance is conducted on the green bricks; the green bricks obtained after strength maintenance is completed are sprinkled or coated with waterborne waterproof coating or dipped in the waterborne waterproof coating, so that an environment-friendly blocking layer with the thickness being 1-10 mm is formed on the surfaces of the green bricks obtained after strength maintenance is completed, and then the finished bricks are made. By the adoption of the well drilling waste brick making method, the well drilling waste can be processed into the brick making raw material which is loose and dry and meets relative environment-friendly standard at a low cost, the brick making raw material can be finally made into the finished bricks which are ideal in compressive strength, ageing resistance, hydrolysis resistance, freezing-thawing resistance, corrosion resistance and environmental protection stability, and therefore harmless and resourceful treatment of the well drilling waste is achieved.
Owner:北京泾渭智能环保有限公司

Amido boron phosphate and preparation method of amido boron phosphate

The invention relates to amido boron phosphate, which comprises the following ingredients: organic amine, dibutyl phosphite, formaldehyde and bononizing agents according to a ratio being 1:(2-3):(2-3):1. A preparation method of the amido boron phosphate comprises the following steps that a, the dibutyl phosphite and the formaldehyde are added into a reaction kettle, then, the organic amine is completely dripped into the reaction kettle under a stirring condition, the temperature in the reaction kettle is controlled to be smaller than or equal to 30 DEG C, and the stirring is continuously carried out for 1 to 2 hours when the temperature in the kettle is not raised; b, the bononizing agents are added into the reaction kettle, a water distribution device is started, temperature is raised to 110 to 130 DEG C through heating, the backflow reaction is carried out for 3 to 5 hours, the reaction is completed when the liquid surface of water in the water distribution device is not increased, cooling is carried out to the room temperature, and a target product is obtained. The synthetized amido boron phosphate belongs to a B-N-P type multifunctional Y lubricating oil additive, when the amido boron phosphate is added into water-base metal processing liquid, the anti-corrosion performance and the anti-rust performance of the processing liquid can be improved, and the lubricating performance of the water-base metal processing liquid can also be improved.
Owner:SHENYANG POLYTECHNIC UNIV

Flexible series-parallel imbricated photovoltaic module and manufacturing method thereof

The invention discloses a flexible series-parallel imbricated photovoltaic module and a manufacturing method thereof, and belongs to the technical field of photovoltaic power generation. The photovoltaic module comprises a front plate, a front adhesive film, an imbricated battery piece group, a rear adhesive film and a back plate, wherein the imbricated battery piece group is packaged between thefront plate and the back plate, the front adhesive film is arranged between the front plate and the imbricated battery piece group, the back adhesive film is arranged between the imbricated battery piece group and the back plate, the front surface and the back surface of each battery piece in the imbricated battery piece group are respectively provided with an electrode, and the front plate and the back plate are flexible plates. The front plate and the rear plate are made of flexible materials, and the conductive adhesive is a silicon-based conductive silver adhesive; after being packaged, the conductive adhesive has excellent elasticity after being cured; the series-parallel imbricated photovoltaic module has the advantages that the partial stress of the series-parallel battery pieces isreduced, the problem of subfissure of the battery pieces can be well solved, the foundation settlement resistance is high, the combination with a building is good, the high-power advantage of the series-parallel imbricated photovoltaic module can be exerted in various occasions, and the application range of the series-parallel imbricated photovoltaic module is expanded.
Owner:CHINA HUANENG GRP CO LTD +1

Milt-functional metal surface treatment additive containing boride diethanolamine phosphates and preparation method

The invention relates to a method for preparing a milt-functional metal surface treatment additive containing boride diethanolamine phosphates, which comprises steps: diethanolamine and phosphate esterification agents are added into a reaction kettle to react, are hydrolysed and concentrated to obtain a viscous liquid, a water-carrying agent is added into the viscous liquid, a boriding agent is added to react by stirring, and the water-carrying agent is boiled up by decompressing to obtain a target product. The milt-functional metal surface treatment additive which is prepared through the method comprises 30-60% boride diethanolamine phosphates and 20-60% diethanolamine double phosphate esters. The method for preparing the milt-functional metal surface treatment additive containing the boride diethanolamine phosphates has the beneficial effects that the milt-functional metal surface treatment additive containing the boride diethanolamine phosphates has excellent antifriction, antioxidant, rust-proof and lubrication performance and the like because phosphates which are used as main components in the milt-functional metal surface treatment additive containing the boride diethanolamine phosphates contain active elements such as N, P and B and the like, is strong in anti-hydrolytic property, can improve lubricity and anti-rust property of a water-base metal working fluid by being added into the water-base metal working fluid, also can improve extreme pressure property and prolongs service life of the water-base metal working fluid simultaneously, and is an excellent multi-functional water-soluble additive.
Owner:CHANGZHOU VOCATIONAL INST OF ENG

Nanofiltration separation membrane and preparation method thereof

The invention relates to a nanofiltration separation membrane which is prepared by dopa and / or dopamine through stem grafting and crosslinking after being stably auto-polymerized on the surface of a basement membrane. A poly-dopa or poly-dopamine composite layer which can be firmly combined with the basement membrane is obtained based on the principle of biological adhesion, and the composite layer is directly reacted with amino or sulfydryl in a long-chain molecule for crosslinking so as to prepare a series of nanofiltration separation membranes with different surface roughnesses, modified layer thicknesses, membrane pore diameters and hydrophilias. The nanofiltration separation membrane has the following advantages: (1) the composite strength between the composite layer and the basement membrane is large; (2) the seawater erosion resistant and hydrolytic resistance performances are strong so that the service life of the membrane is greatly prolonged; (3) the surface is smooth and uniform; (4) the surface hydrophilia is strong so that the permeability performance of the membrane can be improved; (5) the antibiosis is strong so that the pollution of the microbial membrane can be restrained; (6) the water flux is large and the separation efficiency of divalent ions is high; and (7) the process is simple, the condition is mild, and the realization is easy.
Owner:OCEAN UNIV OF CHINA

Water-resistant acrylate emulsion adhesive and preparation method thereof

The invention relates to the technical field of coatings, in particular to a water-resistant acrylate emulsion adhesive and a preparation method thereof. The preparation method of the water-resistant acrylate emulsion adhesive comprises the following steps: mixing polystyrene methyl methacrylate, methyl acrylate, hydroxyethyl acrylate, hydroxyethyl methylacrylate, hexyl acrylate, 2-ethylhexyl acrylate and methyl methacrylate, stirring and dissolving for 60-80 minutes at the temperature of 45-50 DEG C; adding a defoaming agent, a thickening agent and a surfactant for continuous reaction, wherein the reaction temperature is 50-55 DEG C, and the reaction time is 25-35 minutes; and adding an emulsifying agent and deionized water for emulsifying at the emulsifying temperature of 55-60 DEG C for 25-35 minutes, and stopping heating to obtain the water-resistant acrylate emulsion adhesive. According to the preparation method, the reaction temperature and the reaction time in the preparation process can be effectively reduced, so that the energy consumption is effectively reduced, the production efficiency is improved, and the problems of high energy consumption and low production efficiency in the preparation process of the existing adhesive are solved.
Owner:佛山市鹏达家居有限公司

Preparation method of flame-retardant composite over-rust antirust paint

The invention discloses a preparation method of a flame-retardant composite over-rust antirust paint, belonging to the technical field of antirust paint preparation. The preparation method comprises the following steps: drying and pulverizing tung seeds and Maofeng, mixing with lime water to regulate the pH value, standing, filtering, airing the filter residue, adding distilled water, grinding into slurry, heating to keep the temperature under ultrasonic actions, mixing with n-hexane, filtering to obtain the filtrate while keeping the temperature, stirring and mixing with hectorite, talcum powder and the like, adding zinc oxide, keeping the temperature, respectively adding polyurethane, iron oxide and barium sulfate, stirring and mixing, and keeping the pressure, thereby obtaining the flame-retardant composite over-rust antirust paint. The method has the advantage of simple preparation steps. The obtained product has the advantages of favorable adhesive force, favorable uniformity and compactness, favorable flowability, high shock strength (greater than 50kg.cm) and high hydrolysis resistance. After being immersed in water for 140-145 hours, the paint film does not shed or discolor, and does not generate the bubble phenomenon; the water resistance, alkali resistance, rust resistance and flame retardancy are effectively enhanced; and the paint film can resist the high temperature of 130 DEG C for 6080-7100 hours.
Owner:张静

A method for making bricks from drilling waste

The invention discloses a well drilling waste brick making method. The well drilling waste brick making method comprises the following steps that dirt elimination and desiccation treatment is conducted on well drilling waste to be treated with a dirt elimination and desiccation agent; a construction binding material and a construction aggregate are added to the well drilling waste, to be treated, obtained after dirt elimination and desiccation treatment, even mixing is conducted, and then a brick making mixture is obtained; the brick making mixture is solidified and pressed to be green bricks with the density not smaller than 80% by means of a static pressure type brick making machine; strength maintenance is conducted on the green bricks; the green bricks obtained after strength maintenance is completed are sprinkled or coated with waterborne waterproof coating or dipped in the waterborne waterproof coating, so that an environment-friendly blocking layer with the thickness being 1-10 mm is formed on the surfaces of the green bricks obtained after strength maintenance is completed, and then the finished bricks are made. By the adoption of the well drilling waste brick making method, the well drilling waste can be processed into the brick making raw material which is loose and dry and meets relative environment-friendly standard at a low cost, the brick making raw material can be finally made into the finished bricks which are ideal in compressive strength, ageing resistance, hydrolysis resistance, freezing-thawing resistance, corrosion resistance and environmental protection stability, and therefore harmless and resourceful treatment of the well drilling waste is achieved.
Owner:北京泾渭智能环保有限公司

A kind of multifunctional metal surface treatment additive containing boride diethanolamine phosphate and preparation method thereof

The invention relates to a method for preparing a milt-functional metal surface treatment additive containing boride diethanolamine phosphates, which comprises steps: diethanolamine and phosphate esterification agents are added into a reaction kettle to react, are hydrolysed and concentrated to obtain a viscous liquid, a water-carrying agent is added into the viscous liquid, a boriding agent is added to react by stirring, and the water-carrying agent is boiled up by decompressing to obtain a target product. The milt-functional metal surface treatment additive which is prepared through the method comprises 30-60% boride diethanolamine phosphates and 20-60% diethanolamine double phosphate esters. The method for preparing the milt-functional metal surface treatment additive containing the boride diethanolamine phosphates has the beneficial effects that the milt-functional metal surface treatment additive containing the boride diethanolamine phosphates has excellent antifriction, antioxidant, rust-proof and lubrication performance and the like because phosphates which are used as main components in the milt-functional metal surface treatment additive containing the boride diethanolamine phosphates contain active elements such as N, P and B and the like, is strong in anti-hydrolytic property, can improve lubricity and anti-rust property of a water-base metal working fluid by being added into the water-base metal working fluid, also can improve extreme pressure property and prolongs service life of the water-base metal working fluid simultaneously, and is an excellent multi-functional water-soluble additive.
Owner:CHANGZHOU VOCATIONAL INST OF ENG

Anti-corrosion glass fiber bush and preparation method thereof

The invention discloses an anti-corrosion glass fiber bush and a preparation method thereof, and relates to the technical field of glass fiber bushes. The anti-corrosion glass fiber bush comprises thefollowing components in parts by weight: 30-50 parts of polyhexamethylene terephthalamide resin, 40-50 parts of quartz sand, 20-40 parts of fly ash, 25-35 parts of barium sulfate powder, 10-20 partsof antioxidant, 8-10 parts of flexibilizer, 15-20 parts of weather-proof agent, 10-30 parts of glass fiber, 10-15 parts of glycerol tri(1,2- epoxy) propyl ether, 8-10 parts of defoaming agent and 30-40 parts of glass fiber bush. According to the glass fiber bush beneficial to corrosion prevention and the preparation method of the glass fiber bush, glass fibers with a certain particle size are added into a prepared grouting material, so that the prepared grouting material has excellent impact resistance; and by adding a polyhexamethylene terephthalamide resin, quartz sand, fly ash and barium sulfate powder, the prepared grouting material has good processability and mechanical strength, strong hydrolysis resistance and excellent comprehensive performance, so that when the grouting material is used on a glass fiber bush, the corrosion resistance and the stability of the grouting material are remarkably improved.
Owner:ZHENGZHOU SINO SINA BUILDING MATERIALS CO LTD
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