15results about How to "Improve response quality" patented technology

The invention provides a multi-channel uniform injection loop reaction device for preventing liquid phase implosion, and belongs to the technical field of injection loop reaction, and a material pretreatment unit is used for filtering raw materials and adjusting the temperature of the raw materials, so that the quality of the raw materials and the stable feeding state are ensured; the jet reaction unit adopts a mode of combining multi-channel jet and material dispersion to realize uniform mixing and reaction of materials; the temperature and concentration regulation and control unit monitors in real time and precisely regulates the temperature and concentration of the reaction system; the implosion early warning and regulation and control unit dynamically judges the implosion risk based on a risk assessment model and starts hierarchical regulation and control measures; the emergency pressure relief unit quickly relieves pressure when the pressure is abnormal, and accident expansion is prevented. Through the synergistic effect of all the units, an all-dimensional and multi-layer anti-explosive polymerization system is formed, the technical problem of implosion prevention and control in the liquid phase reaction is solved, the reaction efficiency and the product quality are improved, and remarkable economic value and social benefit are achieved.

This invention relates to the field of iron oxide preparation technology, and discloses a reactor for preparing iron oxide by precipitation. The reactor includes a hollow main body, a storage component fixed inside the main body, a spraying component sequentially fixed along the length of the storage component, an adjusting component located on top of the storage component and fixed to the main body, and a rotating stirring component located at the bottom of the adjusting component and connected to the storage component and the spraying component. This invention effectively avoids the accumulation of large amounts of iron filings at the bottom of the reaction vessel, preventing slow reaction rates and incomplete reactions. It uses pressurized gas to spray the precipitated iron filings upwards, ensuring thorough contact and mixing with the solution, thus improving the efficiency and quality of secondary oxidation of the iron filings. The mixture of solution and iron filings is achieved through vertical compression, vibration, and stirring, increasing the mixing contact time and ensuring sufficient contact between the oxidizing gas and the solution, thereby improving the reaction environment and enhancing the reaction rate and quality.

The application discloses an intelligent scheduling system and method for semantic clustering conversation based on artificial intelligence, relates to the technical field of semantic analysis, and synchronously acquires voice call data and online customer service text flow, adopts an attention mechanism to fuse a joint semantic vector and a user value mapping vector, and generates a context coding vector in combination with a decay factor; an initial topic node is constructed based on the context coding vector, a node weight is dynamically updated through a conversation frequency decay factor, and a topic correlation graph with a weighted edge is generated; for a historical conversation associated with a graph node, a three-dimensional performance model is constructed, a performance score of a customer service reply technique is analyzed, and a knowledge base sorting update is triggered; a value index change rate of a topic node is monitored in real time, when a sudden increase of a high net worth user group associated conversation is detected, a fuse mechanism is automatically triggered and a dedicated agent is dynamically allocated. The application improves the customer service response quality and improves the service experience of users.

The present application relates to mixed reaction device, more particularly to fixed reactor technical field, and disclose a kind of viscous material mixing reaction device containing pitch and its process, including horizontal reactor and with one body kettle body, the kettle body is provided with driving portion, the driving portion is connected with positioning portion and swing portion, the positioning portion and swing portion are connected with reaction portion, the reaction portion is connected with material shaking portion, the horizontal reactor is provided with feeding port, the feeding port is equipped with feeding portion, the driving portion includes driving motor, the driving motor is installed on the shell of horizontal reactor, by the cooperation of helical blade and stirring rod, the rotation of stirring rod is realized in the process of revolution by viscous material flow, cooperate with the swing action of hinged ring one as axis, realize multidimensional strong disturbance mixing, different from traditional single stirring form, significantly improve material dispersion uniformity and reaction consistency, guarantee the overall stability of finished product.

The application discloses a kind of cut cylinder and bypass heat supply multi-mode working condition self-adaptive switching decision system and method, belong to steam turbine control technical field, it includes obtaining the real-time operating parameter and external demand parameter of unit, obtains current working condition state vector;Current working condition state vector and the demand prediction parameter of future time period are carried out multidimensional rolling optimization calculation, and optimization decision instruction is generated;Using current working condition state vector index pre-stored working condition control mapping relationship set, continuous control instruction is calculated;Current working condition state vector, the execution feedback data of continuous control instruction and the execution effect data of optimization decision instruction are associated with evaluation, and rule update instruction is generated;Rule update instruction is executed, and working condition control mapping relationship set is revised.The application uses the strategy that prospective rolling optimization and closed loop self-learning rule revision are combined, and the economic, stable and intelligent adaptive control of mode switching of steam turbine under variable working condition can be realized.

The utility model relates to the technical field of cyclohexanone-oxime, and particularly provides a device for catalyzing cyclohexanone ammoximation reaction by using a water system large-aperture silicon-titanium molecular sieve. The device comprises an oximation reactor, a bottom discharge port of the oximation reactor is connected to a feed port of a cross-flow membrane filter through a pipeline and a circulating pump, a turbid liquid outlet of the cross-flow membrane filter is connected to a feed port of the oximation reactor through a pipeline, and a clear liquid outlet of the cross-flow membrane filter is connected to a cyclohexanone-oxime refining process. A gas ammonia, cyclohexanone and hydrogen peroxide feeding pipe is also arranged on the pipeline between the turbid liquid outlet and the feeding hole of the oximation reactor; the device further comprises a catalyst preparation system, the system is provided with a catalyst storage tank, the catalyst storage tank is connected to a catalyst feeding tank through a catalyst feeding pump, and the catalyst feeding tank is further connected with a desalted water adding pipe and a catalytic promoter adding pipe. And the discharge port of the catalyst feeding tank is connected between the discharge port of the oximation reactor and the feed port of the cross-flow membrane filter through a pipeline. The ammoximation process of a water system can be realized, the reaction quality is improved, and the cost is reduced.

The utility model belongs to chemical machinery and equipment technical field relates to a kind of low pressure large-capacity overlapping half-pipe reaction kettle, including cylinder, lower end of the cylinder is welded with lower head, upper end of cylinder is welded with upper head;The top surface of the upper head installs drive assembly;The drive assembly drives the built-in stirring assembly of cylinder, and stirring assembly includes stirring shaft, and the lower end of stirring shaft is sequentially installed bottom bearing, bottom stirrer, flat paddle from bottom to top, wherein bottom stirrer is located in lower head, and flat paddle is provided with multiple layers along the axial direction of stirring shaft;Cylinder outer surface is welded with the cylinder half-pipe of helically arranged, and cooling cavity is formed between cylinder half-pipe and cylinder surface, and the upper end of cylinder half-pipe is provided with first cooling water outlet, and the lower side of first cooling water outlet is provided with first cooling water inlet.The reaction kettle is high in heat transfer efficiency, and can meet the requirement of fast and uniform temperature change of material in the reaction kettle.

The application provides a method for preparing an intermediate of abubinitin by using a micro-channel reactor, 3-oxocyclobutane acyl chloride and sodium azide are respectively dissolved and pumped into a micro-channel reactor I to perform an acyl azide reaction, and the intermediate reaction solution is continuously pumped into a micro-channel reactor II to perform a reaction with benzyl alcohol to obtain 3-oxocyclobutyl benzyl carbamate. The micro-channel reactor is used as a core reaction equipment, continuous acyl azide reaction and continuous Curtius rearrangement reaction are realized, the method has the advantages of high yield, good quality, reduced reaction risk, high mass and heat transfer efficiency, safe and simple operation and the like, and is beneficial to the large-scale production and application of the intermediate.

The application discloses a kind of gas-liquid two-phase mixing type reaction kettle for pharmaceutical intermediates production and drive control method, it is related to pharmaceutical intermediates production equipment technical field.In the application: the bottom of reaction kettle is equipped with gas inlet end, inner cavity is configured with driving shaft and stirring paddle, top cover is configured with gas concentration sensor and multiple inverted cone, and inner cavity is provided with floating mixing disc.The piston ring is arranged on the side of floating mixing disc, the main shaft sleeve and the flow guide pipe are arranged on the top of floating mixing disc, the jet nozzle is arranged on the top end of flow guide pipe, and the liquid outlet of jet nozzle is opposite to the lowest point of inverted cone.The floating mixing disc is provided with flow guide slope and flow guide channel, the flow blocking component is elastically installed at the flow guide channel, a liquid level meter is further arranged, and the reaction kettle is provided with a hydraulic system for driving the floating mixing disc to rise and fall.The application realizes efficient mixing of gas-liquid two-phase by dynamically controlling the rising and falling of floating mixing disc, improves reaction efficiency and product quality, and is suitable for gas-liquid two-phase reaction production of pharmaceutical intermediates.

The utility model belongs to the technical field of organic synthesis equipment, and particularly relates to a monomethyl cyclopentadiene dripping type cyclic sodium reaction device which comprises a support frame, a cyclic sodium reaction kettle, two liquid storage tanks, a mounting frame, a driving component, a hollow shaft, a stirring component, two dripping feeding components and a reaction endpoint judging component, the cyclic sodium reaction kettle and the two liquid storage tanks are fixedly installed on the supporting frame, the two liquid storage tanks are located on the two sides of the cyclic sodium reaction kettle respectively, the two dropwise adding and feeding assemblies are arranged on the cyclic sodium reaction kettle and connected with the corresponding liquid storage tanks respectively, and the installation frame is fixedly installed at the top of the cyclic sodium reaction kettle. The hollow shaft is rotatably mounted on the sodium annulus reaction kettle, and the driving assembly is arranged on the mounting frame and is connected with the hollow shaft. The reaction kettle is reasonable in design, has the advantages of compact structure, good stirring effect, accurate dropwise adding, accurate reaction endpoint judgment, convenience in operation and the like, and has higher practical value and application prospect.

The utility model discloses an efficient energy-saving chemical reaction kettle, which comprises a reaction kettle body, a fixing plate, a cross rod, a charging port, a motor, a communicating pipe and a conveying pipe, the reaction kettle body is in a funnel type design, the fixing plate installed by screws is arranged on one side of the reaction kettle body, the fixing plate is connected with a support or a platform, and the reaction kettle body is fixed by the fixing plate. The top of the reaction kettle body is provided with a feeding port, the feeding port is in a funnel type design, the cross rod is located above the reaction kettle body and can rotate under the manual action, a motor is installed on the outer wall of the lower portion of the reaction kettle body, the bottom of the reaction kettle body is connected with a conveying pipe through a reducer pipe, and a valve is installed on the conveying pipe. After reaction in the reaction kettle body is completed, liquid is conveyed to the next process through the conveying pipe, the communicating pipe is located at the bottom of the reaction kettle body, and liquid is conveyed through the communicating pipe. The device is reasonable in design; and the dredging motor and the dredging rod on the cross rod can timely perform dredging operation when the charging hole is blocked.

This utility model relates to a reaction device, a reaction vessel for resin production, including a stirring shaft and a vessel body. The lower end of the stirring shaft extends into the vessel body along the upper end and is connected to stirring blades and a trigger rod. The upper end of the stirring shaft is connected to a drive motor. The trigger rod includes a rod body perpendicular to the stirring shaft. A groove is formed along the axial direction of the end of the rod body away from the stirring shaft. Limiting grooves are formed on opposite sides of the inner wall of the groove, consistent with the direction of the groove. An alloy contact is provided in the groove. With the cooperation of a spring and a guide block, the alloy contact of this utility model can stably contact the spherical protrusion during stirring, generating regular vibration. This vibration can effectively drive the flow of reactants near the side wall in the vessel body, making the reactants more thoroughly mixed. At the same time, the vibration can reduce the adhesion of reactants to the side wall of the vessel body, significantly improving reaction efficiency, reducing material waste and equipment cleaning difficulty.

The utility model relates to the technical field of hydrolysis reactors, and provides a hydrolysis reactor for industrial carbon dioxide production, which comprises a reaction tank, a first separation ring and a second separation ring which are concentrically distributed are arranged at the bottom in the reaction tank, and the interior of the reaction tank is divided into three reaction chambers by the first separation ring and the second separation ring. A plurality of vertically distributed electric heating rods are embedded in the tank wall of the reaction tank and the first and second separation rings, and a stirring assembly is mounted in the reaction tank. According to the reactor, through multi-chamber synchronous heating and unique stirring assembly design, the reaction efficiency and the product quality are effectively improved. The innovative structure and working mode provide an efficient and reliable solution for the production of industrial carbon dioxide, and have important application value and wide market prospect.

The utility model discloses a microcrystalline cellulose reaction mixing kettle which comprises a mixing kettle body, the top end of a stirring pipe is connected with a motor, electrical bars are installed on the two sides of the bottom of an inner cavity of the mixing kettle body, a water pump is installed on one side of the bottom of the inner cavity of the mixing kettle body, and the output end of the water pump is connected with a water conveying pipe. The water conveying pipe fixedly penetrates through the side wall of the mixing kettle, a top shell is fixedly arranged at the top end of the mixing kettle, one end of the water conveying pipe is communicated and connected with the top shell, one end of the stirring pipe is rotationally connected with the top shell through a sealing bearing, and a plurality of through holes are formed in the side wall, located in an inner cavity of the top shell, of the stirring pipe. The utility model relates to the technical field of microcrystalline cellulose production, the mixing kettle can realize mixing of microcrystalline cellulose and an acid-base solution under the driving of the motor by arranging the stirring pipe, and meanwhile, water in the mixing kettle is heated by the electrical bar and can enter the top shell through the conveying pipe under the driving of the water pump, so that the microcrystalline cellulose and the acid-base solution are mixed. And the microcrystalline cellulose enters the inner cavity of the stirring pipe through the through hole, so that the heating temperature control of the microcrystalline cellulose and the acid-base solution is realized, and the reaction quality is further improved.

The utility model discloses a polymerization reaction kettle for high-efficiency refining treatment of polyether polyol with high EO content, which comprises a reaction kettle, a separation tank and a purification tank, the reaction kettle is provided with a stirring structure, a heating device and a circulating feeding structure, and full mixing, accurate temperature control and circulating reaction of materials are realized; a centrifugal separator is arranged in the separation tank, the purification tank is provided with an adsorbent layer and a distillation device, and product separation and purification can be completed in sequence; the electric three-way valve controls the flow direction of materials, and the containers realize material transmission through connecting pipelines; meanwhile, the equipment is provided with a pressure relief opening and a safety valve to guarantee operation safety, and a bottom sewage draining opening is convenient to maintain. The polymerization reaction kettle solves the problems of non-uniform material mixing, low refining efficiency, poor safety and the like of the existing equipment through multi-structure collaboration, realizes efficient production and refining treatment of polyether polyol with high EO content, is coherent in material treatment flow and high in equipment practicability, and can meet the requirements of large-scale industrial production.