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95results about How to "Increase the number of nuclei" patented technology

Method for synthesizing kaolin microsphere in-situ crystallized product containing small crystal grain NaY molecular sieves

The invention relates to a method for synthesizing a kaolin microsphere in-situ crystallized product containing small crystal grain NaY molecular sieves. Kaolin is used as a raw material. The method comprises the following steps of: adding deionized water and sodium silicate or sodium pyrophosphate into the kaolin, mixing and slurrying, performing spray drying on the mixed slurry to prepare kaolin spray microspheres with particle diameters of 20 to 110 microns, roasting a part of the kaolin spray microspheres for 1 to 3 hours at the temperature of between 920 and 1,000 DEG C to obtain high-temperature roasted microspheres, and roasting the other part of the kaolin spray microspheres for 1 to 3 hours at the temperature of between 700 and 900 DEG C to obtain metakaolin microspheres; mixing the high-temperature roasted microspheres and the metakaolin microspheres in a mass ratio of 9:1-1:9, adding sodium silicate, directing agent, sodium hydroxide solution, deionized water and organic additive into the mixture, and crystallizing for 16 to 36 hours at the temperature of between 90 and 95 DEG C; and filtering, removing mother solution, and drying the filtrate to obtain the kaolin microsphere in-situ crystallized product containing NaY molecular sieve crystal grains of 200 to 400 nanometers.
Owner:PETROCHINA CO LTD +1

As-cast high pearlite quantity and high vermicular rate vermicular graphite cast iron and preparation method thereof

The invention discloses as-cast high pearlite quantity and high vermicular rate vermicular graphite cast iron and a preparation method thereof. The vermicular graphite cast iron is prepared from the following components by weight percent: 3.5-3.8% of C, 2.2-2.4% of Si, 0.8-1% of Mn, 0.2-0.4% of Cu, 0-0.4% of Mo, 0.08-0.1% of Sn, 0.2-0.4% of Cr, 0.2-0.5% of Ni, 0.05-0.1% of Nb, less than or equal to 0.06% of S, less than or equal to 0 .06% of P, and the balance of Fe and impurities introduced by raw materials. The vermicular graphite cast iron with a high creep rate (90-98%) is obtained by using an Mg-RE creeping method for controlling; furthermore, by means of micro-regulation of multiple alloy elements, the vermicular graphite cast iron with a high high pearlite quantity (90%-100%) can bestably obtained; the tensile strength of the vermicular graphite cast iron is greater than or equal to 500MPa, the elongation of the vermicular graphite cast iron is greater than or equal to 1.5%, Brinell hardness of the vermicular graphite cast iron is 230-260HBW, and the microhardness of pearlite is 300-320HV. The vermicular graphite cast iron provided by the invention has the characteristics of being good in mechanical properties, thermal fatigue resistance, thermal crack resistance and wear resistance under the extremely harsh working conditions; the preparation method is simple in control method and can stably produce castings with excellent comprehensive performance, thus being suitable for industrial mass production.
Owner:西安洪盛冶金科技有限公司

Ultrasonic-vibration activation-assisted sintering box-type resistance furnace

The invention provides an ultrasonic-vibration activation-assisted sintering box-type resistance furnace aiming at actual demands of research and development of new materials upon a sintering technology, inherent defects of the resistance furnace and the advantages of an ultrasonic technology. The ultrasonic-vibration activation-assisted sintering box-type resistance furnace comprises a furnace shell, a heating element, a furnace door, a crucible, an amplitude-change pole, an amplitude-change pole supporting frame, an ultrasonic generator and an ultrasonic transducer; ultrasonic power and loading time are controlled through the ultrasonic generator, electrical signals generated from the ultrasonic generator are converted into ultrasonic vibration through the ultrasonic transducer, the ultrasonic vibration transfers to-be-sintered samples through the amplitude-change pole and the crucible, the to-be-sintered samples are enabled to be in the ultrasonic vibration state during sintering, matter particulates of the to-be-sintered samples vibrate at a high speed under high temperature to promote crystal particulates of the to-be-sintered samples to evenly nucleate and grow up or evenly melt. By the arrangement, micro-structure of the massive sintering samples is evener and more compact, and powdery sintering samples can be more evenly dispersed.
Owner:CHONGQING UNIVERSITY OF SCIENCE AND TECHNOLOGY

Battery cathode diachylon formulation high in utilization rate of active substance and preparation method of battery cathode diachylon formulation

The invention relates to a battery cathode diachylon formulation high in utilization rate of active substance and a preparation method of the battery cathode diachylon formulation and belongs to the technical field of lead-acid storage batteries. The the battery cathode diachylon formulation comprises dilute sulfuric acid of 1.38g/ml in density, deionized water, lignin Vanisperse AT, polyaniline potassium sulfonate PAN-K, nano hollow barium sulfate, acetylene black, emulsion carbon naotube Sus-CNT and lead powder. On the basis of a conventional cathode diachylon formulation, water-soluble PAN-K is adopted to completely replace conventional polyester staple fiber, nano hollow barium sulfate is adopted to completely replace conventional precipitated barium sulfate, and the emulsion carbon nanotube Sus-CNT is adopted to partly replace deionized water for paste mixing. On the premise that circulating life of a cathode produced by the formulation is not shortened, active substance utilization rate and charging receiving capability of the cathode are remarkably improved, and the battery cathode diachylon formulation is about to have great application and popularization prospect in the field of lowering weight of active substance of the cathode and lowering manufacturing cost of the lead-acid storage batteries.
Owner:CAMEL GRP HUAZHONG BATTERY

A kind of tungsten bronze nano short rod particles catalyzed and doped by variable valence metal and its preparation method

The invention provides a variable valency metal catalyzed and doped tungsten bronze Ax-MyWO3 nano-short rod particle and a preparation method thereof. The method consists of: firstly making solid colloidal tungstic acid as a tungsten source, mixing the tungsten source with an M source, an appropriate solvent and an inducing agent, adding a proper amount of a variable valency metal A salt, and carrying out thermal reaction to synthesize the variable valency metal catalyzed and doped tungsten bronze Ax-MyWO3 multifunctional nanoparticle. The synthesized Ax-MyWO3 nano-short rod particle has excellent visible light permeability and near-infrared shielding performance and photothermal conversion ability, can be widely used for preparation of glass transparent thermal insulation paint, transparent and heat insulation compounds, photothermal absorbing coatings, solar thermal collectors, solar water heater coatings, heating fiber and photothermal therapy nanoparticles, etc. At the same time, the synthesized variable valency metal catalyzed and doped tungsten bronze Ax-MyWO3 nano-short rod particle also has excellent photocatalysis ability, and can be widely applied to the photocatalytic degradation field of organic pollutants.
Owner:DALIAN POLYTECHNIC UNIVERSITY

Vibration-solidified low-stress lathe bed casting and casting method thereof

The invention relates to a production method of a lathe bed casting and application, in particular to a vibration-solidified low-stress lathe bed casting and a casting method thereof. The casting method comprises the steps that a sand mould of the lathe bed casting is firstly manufactured; liquid metal is smelted and poured; and three-dimensional vibration solidification is performed. For three-dimensional vibration solidification, through a wavelet spectral analysis technology, after a casting mould cavity is filled with molten iron, a 10-200 Hz low-frequency three-dimensional resonance field is applied; when the molten iron is cooled to a temperature in the range of a Fe-C eutectic point+/-50 DEG C, 200-2000 Hz high-frequency three-dimensional resonance is performed; the casting sand mould is subjected to still standing; a riser and a runner are cut off; and a flash is ground and removed. The low-frequency three-dimensional resonance field enables the mould cavity to be fully filled with the liquid metal, so that pores, impurity mingling, segregation, cavity shrinkage and other casting defects which often happen during a traditional casting process are overcome; by utilizing the high-frequency three-dimensional resonance, the supercooling degree of the molten iron is improved; solidification nucleation is facilitated; the number of nucleation is increased; and the structure refinement of crystals is facilitated. The casting method is simple in process, low in cost, simple for operation and wide in application range and is pollution-free; the quality of the casting can be obviously improved; and the residual stress of the casting is lowered.
Owner:SICHUAN JIANYANG HAITE

Carbonizer for continuously synthesizing calcium carbonate and production method of calcium carbonate

The invention relates to a carbonizer for continuously synthesizing calcium carbonate and a production method of calcium carbonate, an input port of calcium hydroxide, an input port of carbon dioxide are provided on the body of the carbonizer, a discharge port is provided at the bottom of the carbonizer, the input port of calcium hydroxide and the input port of carbon dioxide are positioned at the top of the carbonizer body, the transverse trays with displacement from each other are uniformly arranged from the lower part to the bottom of two input ports in the body of the carbonizer, a layout of a S shape backflow baffle plate or a snaky shape backflow baffle plate is used between the adjacent trays. The calcium hydroxide slurry is a fluid suspension, and enables an equidirectional flow with carbon dioxide on the transverse trays between the trays, the calcium hydroxide slurry enters to the next tray from an outlet, three phases of gas, liquid and solid phase are reacted to generate precipitated calcium carbonate, the reacted material-carbonized boiled slurry is flowed out from the outlet of lower part of the reactor. The product has the advantages of adjustable particle size, narrow grain size distribution and stable quality, dispersibility, stability and alkali efflorescence are improved; the invention has the advantages of less equipment investment, short reaction time, less energy consumption, low cost, and the product enables continuous production.
Owner:连州市凯恩斯纳米材料有限公司

Method for improving flaw detection qualification rate of Q345C steel plate with specification of 14-30 mm

The invention provides a method for improving the flaw detection qualification rate of a Q345C steel plate with the specification of 14-30 mm, belongs to the technical field of medium-thickness steel plate production, and comprises a Q345C steel plate and a production method of the Q345C steel plate. The Q345C steel plate comprises the following chemical components of (unit, wt%) 0.15wt% to 0.18wt% of C, 0.20wt% to 0.40wt% of Si, 1.25wt% to 1.35wt% of Mn, P less than or equal to 0.025wt%, S less than or equal to 0.005wt%, 0.015wt% to 0.025wt% of Ti, 0.015wt% to 0.030wt% of Als and the balance Fe and residual elements. According to the method, in the production, the Q345C process technology is strictly controlled, the sulfur content and the manganese content of a finished product are strictly controlled; on the premise that the surface temperature of a casting blank is higher than the third brittleness temperature interval of steel by 900 DEG C or above when the casting blank is straightened, when the secondary cooling water temperature is lower than or equal to 35 DEG C, the secondary cooling specific water flow is controlled to be 0.42 L / kg, and when the secondary cooling water temperature is higher than 35 DEG C, the secondary cooling specific water flow is controlled to be 0.48 L / kg; and the casting blank is rolled after being cut and slowly cooled. Through the implementation of the method, the flaw detection qualification rate of the rolled Q345C steel plate with the specification of 14-30 mm is increased to 99.80% from 98.40%, and the qualification rate is increased.
Owner:NANYANG HANYE SPECIAL STEEL CO LTD

Preparation method and application of nano-molybdenum powder doped with yttrium oxide nano-particles

The invention discloses a preparation method of nano-molybdenum powder doped with yttrium oxide nano-particles. The preparation method comprises the following steps of 1, dispersing commercial micron-sized molybdenum trioxide and carbon nano-particles in a solution, and conducting drying by distillation to obtain composite powder; 2, spraying the ultrafine/nanometer yttrium salt liquid drops intothe composite powder, and conducting drying to obtain a yttrium salt-containing mixture; 3, carrying out segmented heat preservation and reduction on the yttrium salt-containing mixture to obtain ultrafine doped MoO2; and 4, conducting reduction on the ultrafine doped MoO2 by hydrogen to obtain nano-molybdenum powder doped with yttrium oxide nano-particles. The invention also provides an application of the nano-molybdenum powder doped with the yttrium oxide nanoparticles to sintering preparation of a nano-structure oxide dispersion strengthened molybdenum alloy. According to the preparation method, two-step reduction is combined with preparation of the composite powder, so that the nucleation number of a reduction product is increased, the granularity of the reduction product is refined, the granularity of the doping yttrium oxide nano-particles and molybdenum powder is regulated and controlled, and the raw material cost is reduced. The application method is simple and easy to implement.
Owner:西安稀有金属材料研究院有限公司

Brush plating-based surface enhanced Raman spectrum SERS silver-plated active substrate and preparation method thereof

The invention discloses a brush plating-based surface enhanced Raman spectrum SERS silver-plated active substrate and a preparation method thereof, and relates to the technical field of Raman spectrumdetection. The brush plating process is combined with the preparation process of the surface-enhanced Raman spectrum silver-plated active substrate, and the nucleation mechanism of silver crystal grains is converted into the instantaneous nucleation mechanism according to the preparation requirements of the surface of the surface-enhanced Raman spectrum silver-plated active substrate, that is a silver crystal nucleus generation accelerant is added into the prepared brush plating working solution, so that the nucleation quantity in unit time is increased, fine grains are facilitated to be achieved, and all of the best working parameters of the electric brush plating technology are further obtained; and the surface-enhanced Raman spectrum SERS silver-plated active substrate with nano-sizedsilver particles and good uniformity is prepared by a simple preparation process, so that the technical problems of poorer sensitivity and stability of a Raman spectrum metal active substrate in SERSdetection can be solved, and the technical effect of improving the sensitivity and stability of the Raman spectrum metal active substrate in SERS detection is achieved.
Owner:JIAXING UNIV +1
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