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68results about How to "Overcome the generation" patented technology

Method for extracting indium and preparing iron oxide by slag-free zinc hydrometallurgy of zinc concentrate

InactiveCN101886272AHigh recovery rateOvercome the problem of efficient usePhotography auxillary processesFerric oxidesIndiumSlag
The invention relates to a method for extracting indium and preparing iron oxide by slag-free zinc hydrometallurgy of zinc concentrate, which comprises the following steps of: 1, performing fluidized bed roasting, neutral leaching, low acid leaching, purification and electrodeposition on the zinc concentrate to prepare electric zinc; 2, performing high acid leaching, reduction, preneutralization and displacement to remove copper on low acid leaching residue and waste electrolyte after the electrodeposition to prepare the electric zinc; 3, neutralizing the liquid from which the copper is removed to settle the indium; 4, vulcanizing the liquid in which the indium is settled to remove heavy metal and then adding lime milk to neutralize the liquid to obtain deeply purified liquid; 5, settling iron in the deeply purified liquid by a hydrothermal method to obtain hematite powder; and 6, removing impurities from the hematite powder to obtain soft magnetic iron oxide. In the method, the indium is settled by neutralizing and the iron is settled by the hydrothermal method, so that the indium is separated from the iron, the indium is separated from the zinc, the hematite powder is formed, and the requirement of the soft magnetic iron oxide is met through impurity removal treatment. The method has the advantages of simple process, high recovery rate of the indium and the zinc, short flow for separating the iron from the zinc, high purity of the iron, environmental friendliness, suitability for industrial application, and capability of replacing the conventional slag-free zinc hydrometallurgy process for extracting the indium and making effective use of the iron resource in the zinc concentrate in a form of the soft magnetic iron oxide.
Owner:CENT SOUTH UNIV

Method for processing bean-flavor spiced chicken and bean-flavor spiced chicken

The invention provides a method for processing bean-flavor spiced chicken. The method comprises the following steps of: respectively marinating high-quality chicken and high-quality bean which are used as raw materials by adding multiple natural spices, adding special flavoring oil for flavoring, mixing, performing high-temperature sterilization and vacuum packing, and thus obtaining the bean-flavor spiced chicken. By adopting the method for processing the bean-flavor spiced chicken, the nutrients of the chicken and the bean are furthest kept; when the chicken is marinated, Chinese medicinal herbs with health-care functions are added in a marinating package, so that the marinated chicken has mellow taste, and the health-care effect is added; by mixing and eating the chicken and the marinated bean, the Chinese medicinal herb taste in the conventional health-care marinated chicken is overcome; the bean-flavor spiced chicken has the advantages of rich nutrition, soft, tender and well cooked meat, thick flavor, moderate taste and unique flavor, contains high protein, low fat and high calcium, and has the effects of strengthening spleen, promoting appetite, moistening lung, reducing blood fat, nourishing, supplementing calcium, detoxifying, beautifying and removing acnes. The method is scientific, and nitrites are not produced in the processing process.
Owner:ANHUI GUANGZHENG FOOD

Surface pretreatment agent before metal coating and preparation method and use method thereof

The invention discloses a surface pretreatment agent before metal coating, consisting of components with the following weight ratio: 15-19 portions of film-forming agents; 15-19 portions of coupling agents; 18-23 portions of water-soluble F-containing complex compounds; and 85-90 portions of water. A method for preparing the surface pretreatment agent before metal coating is as follows: firstly wetting the film-forming agents sufficiently with water; and then adding the coupling agents, the F-containing complex compounds or the salts thereof, and the balance of water to be evenly mixed; the method for using the surface pretreatment agent before metal coating comprises the following steps of: firstly using water to dilute the surface pretreatment agent before metal coating until the pH value thereof is 4.5-6; spraying or infiltrating the surface of the treated metal with the treatment time of 30s-90s; and by adopting the technical scheme, the film can be tightly combined with the coating on the metal surface, forms a middle layer with very strong combination force between the metal and the coating, has very good combination force both with the metal surface and the coating, and cancompletely replace the phosphating agent.
Owner:安徽天航机电有限公司

Process method for improving woven dark cloth wet rubbing fastness

The invention discloses a process method, and particularly relates to a process method for improving woven dark cloth wet rubbing fastness. The process method includes the steps: (1) cloth distribution; singeing, cooling reaction and desizing; scouring and bleaching; mercerizing; pad dyeing or jig dyeing; wet rubbing fastness improver and auxiliary selection and preparation; wet rubbing fastness improver finishing; over-soft sizing; pre-shrinking; finished product inspection. According to the process method for improving the woven dark cloth wet rubbing fastness, production processes of all procedures are controlled, the capillary effect of a fabric is effectively improved, the surface finish degree of the fabric is improved, friction resistance is reduced, surface dyeing is decreased by strengthening soaping and washing after dyeing, wet rubbing fastness improvers of waterborne polyurethane complexes (Jiangxi Luxi County Xianghua Fine Chemical Co., Ltd., similarly hereinafter) are added after dyeing, under the assistant effects of assistant stabilizers 203 and cracking agents 109, the process method effectively solves the problem that oil floating points are generated in continuous production for 2000 meters or more when single wet rubbing fastness improvers are added in the past, the wet rubbing fastness of dark dyed cloth is improved by one level or more, corresponding washing fastness is improved, pH (potential of hydrogen) values meet requirements, continuous production and product quality are ensured, and a cloth surface has a certain color-deepening effect and softening effect, so that customer satisfaction is achieved.
Owner:佛山市顺德金纺集团有限公司

Comprehensive utilization method of hydrargillite-produced 4A zeolite waste residue

The invention provides a comprehensive utilization method of hydrargillite-produced 4A zeolite waste residue. The method comprises the steps of: separating the ferrosilicoaluminum component in the hydrargillite-produced 4A zeolite waste residue by means of acid leaching and filtering, wherein the obtained mixed liquor of filter liquor and filter residue washing liquor is used for preparing a polymeric aluminum ferric chloride water purifying agent; and removing iron from the wet slag obtained by washing the filter residue by means of alkali fusing, roasting and activating, and synthesizing the 4A zeolite by a hydrothermal method by means of adjusting and assembling. Triethanolamine is taken as a complexing agent of the microelement iron in the liquor during synthesizing the 4A zeolite, so that the produce of an iron precipitate is overcome, and the whiteness of a 4A zeolite product is guaranteed; sodium sulfide is reacted with a triethanolamine iron complex in the zeolite-synthesized mother liquor to reduce the triethanolamine and obtain an iron sulfide precipitate; and removing the mother liquor of the iron sulfide precipitate to realize the cycle utilization. The synthesis method of the 4A zeolite adopts a sealed cycle technology, thereby being stable in operation, and free of the generation of new waste liquor and new waste slag.
Owner:HEBEI UNIV OF TECH

Energy-saving and environment-friendly solid waste smashing and incinerating device

The invention discloses an energy-saving and environment-friendly solid waste smashing and incinerating device and relates to the technical field of solid waste treatment. The energy-saving and environment-friendly solid waste smashing and incinerating device comprises a solid waste smashing device and a high-temperature incinerating device. The solid waste smashing device comprises a feeding box, a smashing mechanism and a discharging port. The discharging port is connected with the high-temperature incinerating device through a solid waste conveying pipeline. The high-temperature incinerating device comprises an incinerating cylinder. A clean water storage tank, an electrolyzing tank, a solar power generation device and a hydrogen recycling device are further included. The clean water storage tank is connected with the electrolyzing tank through a clean water conveying pipeline. A pressurizing pump is arranged on the clean water conveying pipeline. A hydrogen outlet pipeline is arranged on a cathode of the electrolyzing tank. The hydrogen outlet pipeline is connected with the hydrogen recycling device. An anode of the electrolyzing tank is provided with an oxygen outlet pipeline. One end of the oxygen outlet pipeline stretches in the bottom of the incinerating cylinder, a nozzle is arranged at the end portion of the oxygen outlet pipeline, and a power device of the electrolyzing tank is connected with the solar power generation device. The energy-saving and environment-friendly solid waste smashing and incinerating device is simple in structure, clean, capable of saving energy and environment-friendly, and the purpose of effectively recycling clean resources is achieved.
Owner:弘毅天承知识产权股份有限公司

Preparation technology of chicken Eimeria tenella egg yolk antibody targeted sustained release preparation

ActiveCN103349782AImproved pharmacokinetic profileProlongs the duration of the effective concentrationAntibody ingredientsPharmaceutical non-active ingredientsCoccidiosisMass ratio
The invention relates to a chicken coccidiosis prevention and treatment preparation, in particular to a preparation technology of a chicken Eimeria tenella egg yolk antibody targeted sustained release preparation so as to solve the prevention and treatment problems of chicken coccidiosis. The preparation technology of the chicken Eimeria tenella egg yolk antibody targeted sustained release preparation includes the steps of: preparation, separation and purification of a highly immunized egg yolk antibody (IgY), and preparation of a microcapsule. Preparation of the microcapsule has the reaction conditions that: the chitosan concentration is 0.05-0.8% (w/v), the concentration of CaCl2 is 0.5-1.5% (w/v), the concentration of sodium alginate is 1.0-3.0% (w/v), and the IgY and the sodium alginate are in a mass ratio of 1-4:8. The IgY microcapsule prepared by the technical scheme involved in the invention is a preventive medicine, and is also a therapeutic drug. The microcapsule prepared by the invention provides a very good example for antibiotic substitution therapy. And the determined technology can also be used to prepare IgY or IgG microcapsules of other pathogenic microorganisms, thus having promotional value, and being beneficial to sound development of the green and organic chicken raising industry.
Owner:SHANXI AGRI UNIV

Method for directly preparing mesoporous silicon-magnesium composite oxide fiber by electrospinning

ActiveCN109825899AOvercoming the problem of easy magnesium silicate precipitationGood fiber shapeInorganic material artificial filamentsFiberEnvironmental resistance
The invention relates to a method for directly preparing a mesoporous silicon-magnesium composite oxide fiber by electrospinning. In the method, a stable aqueous silicon-magnesium sol spinning solution is provided, and the silicon-magnesium composite oxide fiber can be directly obtained by electrospinning and subsequent heat treatment. The method solves the problem that silicon and magnesium easily generate magnesium silicate precipitation in a water solution, an aqueous solvent is used, acid is used for catalyzing the hydrolysis of common silane, an inorganic magnesium salt is added, the solution pH value and the alcohol content are controlled, and the stable silicon-magnesium sol spinning solution is obtained. The adopted solvent is an aqueous solution of water or alcohol, the heat treatment mode is simple, and the fiber manufacturing process can reduce the cost and meet the environmental protection requirement. The obtained silicon-magnesium composite oxide fiber has a good fiber morphology, a good mesoporous structure and a high specific surface area and is also good in flexibility. The method is simple in process and suitable for mass preparation, and the fiber does not contain impurity metallic elements, does not have potential harm to the human body or the environment and has great potential application value.
Owner:SHANDONG UNIV

Method for synthesizing mesalazine

A method for synthesizing mesalazine is disclosed. The method comprises the following steps: 1) adding p-nitrophenol, p-toluenesulfonic acid, absolute ethyl alcohol and hexamethylenetetramine, stopping heating after the reaction is finished, heating to room temperature while stirring with ice water, separating out solids, filtering, washing and drying to obtain 5-nitrosalicylaldehyde; 2) adding the 5-nitrosalicylaldehyde, potassium tert-butoxide, copper salt and acetonitrile, adding tert-butyl hydroperoxide while stirring, after the reaction is finished, performing vacuum concentration to remove the solvent, pouring cold water into residues, stirring, performing suction filtration, adjusting the pH value of the filtrate with hydrochloric acid, performing suction filtration, and drying to obtain 5-nitrosalicylic acid; and 3) adding stannous chloride dihydrate, concentrated hydrochloric acid, the 5-nitrosalicylic acid and ethanol, carrying out vacuum concentration after the reaction is finished, dissolving residues in water, adjusting the pH value with a concentrated hydrochloric acid solution, standing for crystallization, carrying out suction filtration, washing filter cake with water, and drying to obtain mesalazine. No isomer is generated, and the yield is high; the method does not need high-temperature and high-pressure conditions; the reaction cost is low; and raw materialsand auxiliary materials with high toxicity and heavy environmental pollution are not used.
Owner:CHANGZHOU VOCATIONAL INST OF ENG

Method for producing phosphorus oxychloride with purity of 99.99999 percent

The invention discloses a method for producing phosphorus oxychloride with the purity of 99.99999 percent. The method comprises the following steps of: adding 1-4 percent by mass of composite complexing agent A into industrial grade phosphorus oxychloride with the concentration of 99.5 percent and collected heavy components produced by primary distillation at the temperatures of lower than 100 DEG C and higher than 107 DEG C, controlling the temperature between 20 DEG C and 50 DEG C, fully stirring for reaction of 40-60 minutes, distilling and extracting a fraction with the temperature of between 100 DEG C and 107 DEG C to obtain a primary distillation product; adding 5.1-11 parts of collected low-boiling-point substance produced by secondary distillation at the temperature of lower than 100 DEG C, 5.1-11 parts of collected heavy component produced by secondary distillation at the temperature of lower than 100 DEG C and 78-89 parts of primary distillation product into an enamel reaction kettle, adding a composite complexing agent B of which the mass is 1-5 percent of that of phosphorus oxychloride, controlling the temperature between 25 DEG C and 50 DEG C, fully stirring for reaction of 40-100 minutes, depositing, delaminating, filtering supernate, distilling filtrate and extracting a fraction with the temperature of between 100 DEG C and 107 DEG C to obtain a secondary distillation product; and rectifying the secondary distillation product to obtain electronic grade phosphorus oxychloride with the purity of 99.99999 percent. The method has the advantages of simple process, high product yield, environmental-friendly production technology and high product purity.
Owner:贵州威顿晶磷电子材料股份有限公司

Full-quantitative treatment method of kitchen biogas slurry

The invention discloses a full-quantitative treatment method for kitchen biogas slurry. The full-quantitative treatment method is based on a UASB treatment unit, a primary A / O treatment unit, a secondary A / O treatment unit, an MBR and an electrocatalytic oxidation treatment unit which are connected in sequence. According to the method, full-quantitative treatment of the kitchen biogas slurry is realized, and on the basis of a common treatment method, an A / O process is adopted, so that the removal efficiency of ammonia nitrogen in the kitchen wastewater is enhanced; an MBR treatment process isadded, and mud-water separation is performed through a physical interception effect, so that the solid-liquid separation efficiency is greatly improved; and the biochemical tail end adopts an electrocatalytic oxidation technology to replace the traditional membrane treatment technology used at the biochemical tail end, so that the membrane concentrated solution generated in the membrane advanced treatment process is overcome, the full-quantitative treatment of the kitchen biogas slurry wastewater is realized, and the kitchen biogas slurry wastewater completely reaches the discharge standard specified by the state.
Owner:NANJING WONDUX ENVIRONMENTAL PROTECTION TECH CO LTD

Ultrasonic nondestructive testing device for pipeline defects

The invention provides an ultrasonic nondestructive detection device for pipeline defects, which comprises a detection frame and four Mecanum wheels mounted at the bottom of the detection frame and controlled by an independent motor, an ultrasonic nondestructive detection box is fixedly mounted in the middle of the detection frame, and a filter cabin is communicated with a liquid supply cabin through a transition pipeline. A circulating pump is arranged on the transition pipeline, a liquid return channel is formed in the detection probe on the side, away from the driven liquid supply pipe, of the arc-shaped ultrasonic detection area, and the liquid return channel is communicated with the filtering cabin through a flexible pipe and a liquid return pipeline; the detection frame is firmly limited on the surface of the pipeline by applying strong airflow thrust to one side far away from the pipeline through the reverse thrust fan blades, and liquid water is used as a coupling medium to replace a coupling agent in the prior art, so that the defects that the liquid water is easy to air in a long-term detection process due to high flowability on the surface of the arc-shaped pipeline are overcome; bubbles are effectively eliminated in the detection process, and the accuracy of ultrasonic bubble detection is ensured.
Owner:蚌埠市特种设备监督检验中心

Baffle type evaporation ammonia-process desulfurization technique and device

The invention discloses jet deflection evaporation-type ammonia process desulphurization technology and a device for implementing the same. The technology comprises a technical proposal: using ammonia as desulfurizing agent; preheating flue gas discharged by the ammonia to between 80 DEG C and 90 DEG C through a boiler; vaporizing the flue gas into steam through an ammonia evaporator so as to contact flue gas flowing from bottom to top for realizing desulphurization; carrying out demisting through a jet deflection demister, and changing the direction of demisted flue gas so as to carry out adsorption desulphurization from top to bottom through a desulphurization ring; directly discharging the flue gas after adsorption desulphurization; respectively washing the air distribution bed and the demister through an air distribution bed wash pipe and a demister wash pipe every 3 to 8 hours, so as to ensure cleanness and smoothness of an air distribution bed and the demister during desulphurization. The device mainly relates to a jet deflection evaporation-type ammonia process desulphurization tower which consists of a base, a tower body, the air distribution bed, the air distribution bed wash pipe, the ammonia evaporator, the demister, the demister wash pipe, the desulphurization ring, a flue gas inlet and a flue gas outlet. The technology and the device not only have excellent desulphurization effect, but also have an exhaust temperature as high as 80 DEG C; therefore, flue gas discharged from the device has excellent diffusibility and less smoke plume; especially importantly, because flue gas does not contain ammonium bisulphite and aerosol after adsorption desulphurization, the device can also prevent erosion in a flue and a chimney caused by wet flue gas; wash water adopted by the invention can be recycled, thereby ensuring remarkable energy-saving effect; moreover, the device has the advantages of simple structure, low operation cost and convenient maintenance.
Owner:QINGDAO HONGYU ENVIRONMENTAL PROTECTION AIR CONDITIONING EQUIP

Ternary positive electrode material complex precursor for lithium battery and preparation method of ternary positive electrode material complex precursor

The invention provides a ternary positive electrode material complex precursor for a lithium battery and a preparation method of the ternary positive electrode material complex precursor. The method comprises the steps of adding a nickel-cobalt-manganese ion water solution prepared at a stoichiometric ratio to a water solution containing lactic acid bacteria and coenzyme, adding sugars, sealing and then standing in a thermotank of 45 DEG C for 12h; taking out a product and adjusting the pH to an appropriate range through adding a precipitant and slowly stirring under nitrogen protection to form a precipitate; and filtering and drying the precipitate to obtain the ternary positive electrode material precursor. According to the ternary positive electrode material complex precursor, the defects that ammonia or oxalic acid is directly added as a complexing agent, is difficult to evenly combine with metal particles and is harmful to the human body and the environment in existing high-nickelternary material preparation are overcome; the sugars are decomposed into lactic acid through slow fermentation of the lactic acid bacteria to form a slow release effect; and the prepared ternary positive electrode material precursor is uniform and controllable in granularity, the preparation process is environment-friendly and pollution-free, raw materials are simple and available and the preparation method is suitable for large-scale industrial production.
Owner:CHENDU NEW KELI CHEM SCI CO LTD
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