The invention discloses an oxidation-reduction preparation method for
graphene. The oxidation-reduction preparation method comprises the following steps: soaking a certain amount of natural
flake graphite powder into concentrated acid; transferring a vessel to a low-temperature environment, adding
phosphoric acid, stirring, and then adding strong oxidant and controlling the temperature of a
reaction system to be below 5 DEG C; transferring the vessel to a room-temperature environment and then stirring; heating and increasing the temperature, reacting for 6-12h while stirring, diluting by water, and then adding
hydrogen peroxide and
hydrochloric acid; performing ultrasonic treatment, thereby acquiring a
graphene oxide acid solution; adding
aluminum foil chippings of the
lithium battery
current collector into the
graphene oxide acid solution, heating and starting the reduction reaction, stirring, removing impurities, and performing
vacuum drying, thereby acquiring the graphene. According to the oxidation-reduction preparation method for graphene, the graphene is acquired after the graphene
oxide acid solution is directly reduced by the
aluminum foil chippings of the
lithium battery
current collector, so that the experiment technique is simplified, the experimental period is shortened, the
impurity introduction is reduced, the adoption of the high-risk and environment-unfriendly raw materials is avoided, the safe and environment-friendly purposes are achieved, the waste of resources is avoided by recycling and reusing and the cost of laboratory is reduced.