One lt; 100 gt; the preparation method of the
crystal orientation high-purity
germanium single crystal comprises the following steps: S1,
crystal pulling: S11, loading a
germanium ingot raw material into a
crucible, 1t; 111gt, 111gt; the method comprises the following steps: S11, fixing a
crystal orientation
seed crystal on a
seed crystal chuck, S12, blowing a pulling furnace, S13, melting a
germanium ingot raw material to form a melt, S14, sequentially performing seeding,
necking,
necking, shouldering,
diameter equalizing and
diameter equalizing until a small amount of melt is left in a
crucible, S15, re-melting the crystal to a seeding end of the
seed crystal, S16, repeating the sub-steps S14 and S17, ending until the melt is completely pulled, S18, cooling, opening the pulling furnace, and
cutting off the crystal; s2, performing a
cutting test perpendicular to the axial direction of the crystal, and screening out a part of which the carrier concentration at two ends is less than 2E10cm <-3 > and the
dislocation density meets 6000-10000 / cm < 2 > as a first qualified section; s3, as lt; 111gt, 111gt; the
crystal orientation is used as the standard, 54.74 degrees are used as the steering included angle, and the 1t is
cut from the first qualified section; 100 gt; a second qualified section of
crystal orientation; and S4, rechecking the head and the
tail of the second qualified section.