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96results about How to "The process is green and environmentally friendly" patented technology

Technique for preparing high purity ultra-fine magnesium hydroxide by sodium hydroxide method

InactiveCN101234769ASpeed ​​up the distribution balance stateHigh purityMagnesium hydroxideDecompositionSlurry
The invention discloses a process for preparing high-purity ultrafine magnesium hydroxide by a sodium hydroxide method; by using a crystal seed decomposition method, purified brine and crystal seed of the magnesium hydroxide are added to a reaction pool to be mixed and temperature is kept at 60-80 DEG C; then solution of the sodium hydroxide is added to the reaction pool to carry out the precipitation reaction, crystallization and aging; after the reaction is finished, slurry of the magnesium hydroxide is filtered and washed; cake after filter is dried and crashed, the crystal product of the magnesium hydroxide is obtained. Compared with the prior art, the process for preparing the high-purity ultrafine magnesium hydroxide accelerates agglomeration and growth of the magnesium hydroxide crystal by adding the crystal seed, solves the problem of the difficulty for filtering and washing the filter cake by using the prior sodium hydroxide method to produce the magnesium hydroxide, and directly utilizes the slurry of the magnesium hydroxide generated by the reaction as the crystal seed to carry out cyclic decomposition. The process flow is simple and the process parameter can be easily controlled. The production process is pro-environment without producing pollutant. At the same time, the purity of the magnesium hydroxide obtained by the process and the recovery rate of the magnesium are very high; furthermore, the purity of the by-product sodium chloride is high. The process for producing the magnesium hydroxide has great development prospect.
Owner:GUIZHOU UNIV

Technique for extraction separation of quadravalence cerium, thorium and cerium less tervalence rare earth from sulphuric acid rare earth solution

The invention relates to a technological method for extracting and separating quadrivalent cerium, thorium, and less-cerium trivalent rare-earth from rare earth sulfate solution. The rare earth sulfate solution, which is obtained through processing the rare-earth ores and contains the thorium and high-valence cerium, is used as raw material; synergistic extraction agent basing on P507 and P204 is adopted for extracting and separating; the cerium (4) and the thorium are extracted into an organic phase, then selective washing and back extraction are performed step by step to obtain the products including pure cerium and pure thorium, the trivalent rare-earth is left in a water phase, and then unsaponifiable P507 or the synergistic extraction agent basing on P507 is adopted to perform multistage fractional extraction to separate single rare earth elements after impurity removal. The technological methodn has the characteristics that the synergistic extraction agent basing on P507 and P204 is adopted, the thorium is easy to perform the back extraction, and extraction capacity is large, and the emulsification is not generated during the extraction process; the cerium (4), the thorium and trivalent rare-earth are extracted and separated in the same extraction system; both extraction and the separation adopt unsaponifiable extraction agent, and ammonia-nitrogen wastewater is not generated; in addition, the thorium is recovered as products, and the pollutions caused by thorium-containing waste residue and the ammonia-nitrogen containing wastewater are eliminated from headstream. Therefore, the technological method has the advantages of simple procedures, green environmental protection, and low manufacturing cost.
Owner:GRIREM ADVANCED MATERIALS CO LTD

Liquid rare earth calcium zinc stabilizer and preparation method thereof

The present invention provides liquid rare-earth calcium-zinc stabilizer and the preparation method. The liquid rare-earth calcium-zinc stabilizer is compound made of rare-earth calcium-zinc compound and effectively cooperative material. The beneficial effects of the liquid rare-earth calcium-zinc stabilizer and the preparation method provided by the present invention is mainly shown in that (1) the liquid rare-earth calcium-zinc stabilizer has the advantages of high product quality, no toxin, environmental protection, no toxic heavy metal component in recipe, strong practicability and wide application range, which is particularly applicable to the transparent packaging material of food, candy and medicine, as well as the advantages of good processing performance, no precipitation, excellent lubricating performance, superior transparency, thermal stability and oxidation resistance; (2) the process condition is stable and easy to control, thus being applicable to industrialized mass production; the process flow has the advantages of simplicity, environment friendliness, easy access to raw materials and less energy consumption, thus greatly decreasing the production cost; in addition, the whole production process has anhydrous operation, safety and convenience, no discharge of three wastes and less environmental pollution.
Owner:高春福

Method for extracting lithium from electrolytic aluminum waste residues

The invention discloses a method for extracting lithium from electrolytic aluminum waste residues. The method comprises the following steps: (1) reacting the electrolytic aluminum waste residues withconcentrated sulfuric acid to obtain a mixture A; (2) adding water to dissolve the mixture A, filtering the obtained solution to obtain a filtrate B, slowly adding calcium oxide to the filtrate B, andfiltering the obtained solution to obtain a filter residue C and a filtrate D; (3) heating the filtrate D, carrying out evaporative concentrating, filtering the obtained concentrate, further carryingout evaporative concentrating on the obtained filtrate to obtain a filtrate E, and maintaining the filtrate E in a heated state; and 4) adding a saturated sodium carbonate solution to the filtrate Ein order to obtain a suspension F, filtering the suspension F to obtain a filter cake, and washing and drying the filter cake to obtain a lithium carbonate product. The method adopts the waste residueof the electrolytic aluminum industry as raw material, the raw material has a wide source, and has a lower cost than a lithium ore raw material, the method has the characteristics of easiness in extraction and high yield, other raw materials used in the extraction method have a low price and low cost, and obtained byproducts can be recycled.
Owner:台州闪能科技有限公司

Water-purifying process and water-purifying equipment thereof

InactiveCN104098218ARealize integrated processingRealize water conservation and environmental protectionMultistage water/sewage treatmentWater savingTap water
The invention relates to a water-purifying process and water-purifying equipment thereof. Tap water is treated into flushing water, clean water and direct drinking water in a grading and classifying manner as required through a first-stage purification treatment device, a second-stage purification treatment device and a third-stage purification treatment device which are connected in sequence from bottom to top. By adopting the water-purifying process and the water-purifying equipment, water resources are utilized more optionally and reasonably, the problems of secondary pollution and the like since heavy metal pollutants in tap water cannot be removed in an efficient and environment-friendly way in the prior art are solved effectively, heavy metal ions, residual chlorine and other harmful particles in tap water are removed efficiently, bacteria are killed, the water quality is improved, sewage is disposed automatically, and the water yield and the utilization ratio of water are increased greatly; the health of a user is ensured; tap water is classified and treated effectively and is utilized in a shunting way according to the water quality, water amount and water pressure requirements of household water, and water is saved; energy is saved efficiently, space is saved, and remarkable energy-saving and environmental protection effects are achieved. The water-purifying process and the water-purifying equipment are suitable to be popularized and applied in relevant tap water treatment field.
Owner:合肥一言科技发展有限公司

Waste gas recovery processing system and recovery processing technique used in chemical car loading

The invention relates to a waste gas recovery processing system and recovery processing technique used in chemical car loading. The system comprises a storage tank, a tank car, a pipeline, a condensation separation device and an adsorptive separation device, wherein chemicals are delivered from the storage tank to the tank car through the pipeline; the condensation separation device and the adsorptive separation device are connected with each other; the condensation separation device comprises a refrigerating unit, a condenser and a gas-liquid separator which are connected with each other; the adsorptive separation device an adsorption device and a desorption device which are connected with each other; the adsorption device is connected with the gas-liquid separator; and the desorption device is connected with the condenser. By using the system, the adsorption / condensation combined circular recovery processing technique is implemented. The invention can sufficiently implement classified recovery processing of organic chemical products and other components in waste gas, and effectively avoid pollution in the chemical storage tank region and the surrounding environment of the chemical storage tank region due to exhaust emission in the chemical car loading; and the invention is applicable to various chemical storage tank regions and related fields.
Owner:BAY ENVIRONMENTAL TECH BEIJING +1

Distillation extraction process of Chinese fir oil

The invention relates to a distillation extraction process of Chinese fir oil, particularly comprising the steps of: 1) placing Chinese fir wood chip being less than 0.1 cm in diameter into a distillation tank, and at the same time, uniformly adding a quick penetrating agent by 0.8-1.2 kg per 1.6 ton of the Chinese fir wood chip, stirring the Chinese fir wood chip, and when the distillation tank is full, sealing the distillation tank; and 2) performing distillation, wherein the production time of the distillation tank is 16 h and is divided into four steps: a) a first step, wherein vapor temperature is 80 DEG C, pressure is 0.5 kg and distillation time is 4 h; b) a second step, wherein the pressure is gradually increased to 8 kg, temperature is increased to 170 DEG C, and a water-soluble weak-alkaline penetrating agent is added through a pressure-reduced valve, and distillation time is 3 h; c) a third step: the pressure is gradually reduced to 3 kg, temperature is 132 DEG C and distillation time is 6 h; and d) a fourth step: quickly increasing the pressure to 10 kg, the temperature is 180 DEG C, and a water-soluble high-temperature penetrating agent is added through the pressure-reduced valve, and distillation time is 3 h. The Chinese fir oil is a colorless or slight-yellow transparent liquid, has good fragrance quality and can be directly used for flavor blending.
Owner:福建省建瓯市金路实业有限公司

A method for environmentally friendly recycle and reusing waste pow battery

ActiveCN109244586ASolve the safety problem of being volatile and easily decomposed into toxic and harmful gasesHarm reductionWaste accumulators reclaimingBattery recyclingFiltrationHazardous substance
A method for recycling and reusing waste power battery belongs to that field of recycling waste battery. The battery is completely discharged and placed under a sealed and protective gas atmosphere, and the battery pole head, the shell and the battery cell are collected by cold cutting; the obtained cell is immersed and cleaned in the replacement solution. And the positive electrode, the negativeelectrode and the diaphragm are separated by unwinding; The positive and negative electrode pieces are respectively soaked in distilled water and ultrasonicated to obtain positive and negative electrode materials, aluminum foil and copper foil; The electrolyte volatile in the process of cell disassembly is absorbed by absorption tower. Distillation, condensation, filtration and drying are used forrecycling of the replacement liquid used in the cell immersion process, and the harmful substances are recovered through a neutralization sedimentation tank and a tail gas absorption tank. The ultrasonic liquid is recycled after being precipitated by adding demulsifier, filtered and treated by biological contact oxidation. The invention realizes the recovery and regeneration of the waste lithiumion battery, the process is safe, harmless, the automation degree is high, the treatment is efficient and convenient, and the secondary pollution to the environment is not generated.
Owner:BEIJING UNIV OF TECH

Environment-friendly 1, 5-diamido-naphthlamine production technique

The invention discloses an environment-friendly 1, 5-diamido-naphthlamine production technique. The environment-friendly 1, 5-diamido-naphthlamine production technique sequentially includes (A), adding raw materials including 1,5-dinitronaphthalene, reaction solvent N, N-dimethylformamide (DMF) and a Pd / C (palladium / carbon) catalyst into a reaction kettle, and performing catalytic hydrogenation reaction at the reaction temperature of 25-50 DEG C and under the reaction pressure of 0.1-0.5 MPa; (B), after reaction, recycling a solid catalyst in reaction liquor by a nitrogen filter pressing method, obtaining a solid crude product after distilling of filter liquor, and obtaining a high-purity 1, 5-diamido-naphthlamine product after washing and filtering of the crude product; (C), mixing distillation cut obtained by distillation and washing liquor after washing, recycling DMF and water by a vacuum rectification method. The 1, 5-diamido-naphthlamine production technique is mild in reaction condition, high in reaction yield, high in purity of the obtained 1, 5-diamido-naphthlamine product, low in production energy consumption and simple and efficient in recycling process of catalyst and solvent; recycled catalyst, solvent and water can be utilized cyclically, so that the production technique is environment friendly.
Owner:XIANGTAN UNIV

Nickel-containing electroplating wastewater treatment method

The invention discloses a nickel-containing electroplating wastewater treatment method which comprises the following steps: putting nickel-containing electroplating wastewater into a stirring tank, and stirring with an electric stirring machine; putting a precipitator into the stirring tank; further putting a settling agent into the stirring tank; further putting a composite water purifier into the stirring tank, and increasing a stirring speed for a certain time; further putting a polymeric flocculant into the stirring tank, and reducing the stirring speed for a certain time; introducing obtained wastewater into the settling tank, and performing precipitation so as to obtain precipitated sludge; filtering and drying the precipitated sludge; dissolving the dried sludge into dilute sulfuric acid so as to obtain a primary solution; extracting the primary solution so as to obtain an extract; performing reverse extraction on the extract so as to obtain a reverse extract; electrolyzing the reverse extract, thereby obtaining metal nickel. The method is environmentally friendly in process procedure, low in energy consumption, high in heavy metal recycling rate, low in overall production cost and easy in industrial on-scale production.
Owner:长沙埃比林环保科技有限公司

Technique for extraction separation of quadravalence cerium, thorium, fluorine and cerium less tervalence rare earth from sulphuric acid rare earth solution

The invention relates to a technological method for extracting and separating quadrivalent cerium, thorium, fluorine and less-cerium trivalent rare-earth from rare earth sulfate solution. The rare earth sulfate solution, which is obtained through processing the rare-earth ores and contains high-valence cerium, the fluorine, the thorium and ferrum, is used as raw material; synergistic extraction agent basing on P507 and P204 is adopted for extracting and separating; the cerium (1V), the thorium, the fluorine, and the ferrum are extracted into an organic phase, then selective washing and back extraction are performed step by step to obtain three products that are the cerium, the fluorine, and the thorium, the trivalent rare-earth is left in a water phase, and then unsaponifiable P507 or thesynergistic extraction agent basing on P507 is adopted to perform multistage fractional extraction to separate single rare earth elements. The technological method has the characteristics that the synergistic extraction agent basing on P507 and P204 is adopted, the thorium is easy to perform the back extraction, and extraction capacity is large, and the emulsification is not generated during the extraction process; the cerium (1V), the thorium, the fluorine, the ferrum and the trivalent rare-earth are extracted and separated in the same extraction system; both extraction and the separation adopt unsaponifiable extraction agent, and ammonia-nitrogen wastewater is not generated; in addition, the thorium and the fluorine are recovered as products, and the pollutions caused by thorium-containing waste residue, fluoride-containing wastewater and the ammonia-nitrogen wastewater are eliminated from headstream. Therefore, the technological method has the advantages of simple procedures, greenenvironmental protection, and low manufacturing cost.
Owner:GRIREM ADVANCED MATERIALS CO LTD
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