The invention discloses a preparation method of a
water treatment defluorination agent. The preparation method is characterized by comprising the following steps: step 1, preparing a
sodium silicate solution, and adding a diluted
hydrochloric acid solution for activation to obtain a solution A; step 2, weighing a first fixed amount of aluminum
chloride hexahydrate
solid, adding the aluminum
chloride hexahydrate
solid into the solution A, stirring for 10-30 minutes, continuously weighing a second fixed amount of
ferric chloride hexahydrate
solid, slowly adding the
ferric chloride hexahydrate solid into the solution until the color of the solution becomes dark and turbid, continuously stirring, gradually clarifying the solution, and finally turning into a reddish brown transparent solution, so as to obtain a solution B; step 3, preparing a
sodium carboxymethyl cellulose solution, namely a solution C; and step 4, placing the prepared solution B and the solution C in a constant-temperature water bath kettle according to the proportion, fully mixing and reacting in a high-speed stirring and heating state, and after the reaction is finished, obtaining the final defluorination agent solution. The
fluorine removal rate of the deep defluorination agent can reach 95% or above, the
fluorine removal rate is high, the
fluorine removal effect is obvious, and deep fluorine removal of fluorine-containing
wastewater can be achieved.