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79results about How to "Increase service temperature" patented technology

Method for achieving electronic building brick high-temperature packaging by filling Sn-based solder with micro-nano metallic particles

The invention provides a method for achieving electronic building brick high-temperature packaging by filling Sn-based solder with micro-nano metallic particles. The method comprises the steps that the micro-nano metallic particles are prepared and mixed with a dispersing agent, a caking agent, diluent and scaling powder; a micro-nano metallic particle mixture is evenly mixed with pure Sn or Sn-based soldering paste; the Sn-based soldering paste is filled with the micro-nano metallic particles and placed on a base plate, alignment process of a part to be welded is completed, and pressure is exerted on the Sn-based soldering paste; the Sn-based soldering paste is put back in a reflow oven and experiences a preheating stage, an insulation stage, a reflowing stage and a cooling stage. According to the method for achieving electronic building brick high-temperature packaging by filling the Sn-based solder with the micro-nano metallic particles, the Sn-based solder is filled with the micro-nano metallic particles, connection and assembly of high-power devices or components can be achieved under the process condition of being compatible with traditional reflow soldering, when the devices serve at high temperature, metallic particles are formed inside a connector, excellent conductivity property and heat-conducting property are achieved, and the heat dissipation index and the electrical performance index of the electronic building brick can be significantly improved.
Owner:HARBIN INST OF TECH

Interconnection brazing material and interconnection forming method thereof

ActiveCN106271177ASolve the problem of long time consumption of phase methodLow Young's modulusWelding/cutting media/materialsMetal working apparatusAmount of substanceThird phase
The invention provides an interconnection brazing material and an interconnection forming method thereof. The heating technological temperature of a product applied by the interconnection brazing material is T, the interconnection brazing material contains a component A with the melting point larger than T, a component B with the melting point smaller than T and a third-phase component C with the melting point larger than T; the third-phase component C accounts 0-30% the total mass of the component A, the component B and the third-phase component C. A compound AxBy is formed through a reaction between the component A and the component B at the heating technological temperature; the ratio of amounts of substances of the component A to the component B is larger than x/y, the third-phase component C does not react with the component A or the component B, the hardness of the third-phase component C is smaller than those of the component A, the component B and the compound AxBy. According to the technical scheme, a high-melting-point welding joint is obtained, and the Young modulus and the thermal expansion coefficient of a joint can be adjusted by adjusting the proportion of the components inside the brazing material.
Owner:HARBIN INST OF TECH SHENZHEN GRADUATE SCHOOL

Wide temperature region viscosity corrosion resisting solid self-lubricating coating and preparation method thereof

The invention discloses a wide temperature region viscosity corrosion resisting solid self-lubricating coating and a preparation method thereof. The coating comprises nano nickel Ni, tungsten selenide WSe2, sliver Ag, yttrium Y, eutectic calcium fluoride fluoride barium CaF2.BaF2 and boron nitride hBN, the raw materials are subjected to mixing with a polyving akohol solution, sintering and breaking and screening, the atmospheric plasma spraying technology is adopted, then the coating is prepared. The solid self-lubricating coating prepared by the method does not contain the chrome Cr element, the working environment of the solid self-lubricating coating is improved, compared with technologies of the same field, the wide temperature region viscosity corrosion resisting solid self-lubricating coating has the advantages that the low friction coefficient is low and stable, the metal melting-drop viscosity corrosion resistance ability is strong, the fluctuation range in the wide temperature region range is smaller, the coating can be used at the temperature ranging from 25 DEG C to 800 DEG C, the service temperature of the coating is improved, and the important engineering application value is achieved.
Owner:PLA SECOND ARTILLERY ENGINEERING UNIVERSITY

Thermal barrier coating with two bonding layers and preparation method of thermal barrier coating

ActiveCN106119760AReduce vertical stressRelieve high temperature thermal expansionMolten spray coatingPorous layerSand blasting
The invention discloses a thermal barrier coating with two bonding layers. The thermal barrier coating comprises a high-temperature alloy matrix, wherein a first bonding layer, a second bonding layer and a surface ceramic layer are deposited above the matrix in sequence; and the first bonding layer is of a multiporous laminated structure, and the second bonding layer is of a compact structure. A preparation method of the thermal barrier coating comprises the following steps: (1) grinding and performing sand blasting treatment on the surface of the high-temperature alloy matrix; (2) depositing a porous layer, which is the first bonding layer, with the porosity of 10 to 30 percent on the surface of the matrix by adopting gas shield protection plasma spraying; (3) depositing a compact layer, which is the second bonding layer, on the surface of the porous layer by adopting hypersonic flame spraying, low-pressure plasma spraying or cold spraying; and (4) depositing the surface ceramic layer on the surface of the second bonding layer by adopting atmospheric plasma spraying. The thermal barrier coating with the two bonding layers can both ensure that alpha-Al2O3 is continuously generated on the surfaces of the bonding layers and further relieve thermal expansion mismatch between the matrix and the ceramic layer, so that the service life of the thermal barrier coating is prolonged.
Owner:XI'AN PETROLEUM UNIVERSITY

Aluminum silicate fiber reinforced oxide ceramic containing interface phase and preparation method thereof

The invention relates to aluminum silicate fiber reinforced oxide ceramic containing an interface phase. The aluminum silicate fiber reinforced oxide ceramic adopts one or a mixture of more of mullite, aluminum silicate and aluminum oxide as a ceramic substrate and adopts aluminum silicate fiber as a reinforcing phase, and a sacrifice carbon interface phase is formed between the substrate and the reinforced phase. The preparation method of the aluminum silicate fiber reinforced oxide ceramic comprises the following steps: preparing a three-dimensional aluminum silicate fiber fabric, and preparing a pyrolytic carbon coating on the surface of the fiber fabric by utilizing a chemical vapor phase deposition process; taking oxide sol as a precursor, vacuum impregnating the fiber fabric, carrying out the gelatization, then carrying out the high-temperature ceramization, and completing the primary compacting process; repeating compacting for at least 10 times; finally carrying out oxidative cracking on carbon interface phase coating, forming a gap between the aluminum silicate fiber and the substrate, and preparing the product. The product is excellent in mechanical property both at the room temperature and high temperature and has the advantages of short preparation period, low cost, wide applicability and the like.
Owner:NAT UNIV OF DEFENSE TECH

Nickel-cobalt-based high-temperature alloy welding wire

The invention belongs to the field of welding materials, and particularly relates to a precipitation strengthening type nickel-cobalt-based high-temperature alloy welding wire for welding a high-temperature part of an 800-DEG C ultra-supercritical power station. The welding wire is mainly characterized in that Ti/Al is more than or equal to 1.5 and less than or equal to 2, and C/Nb is more than orequal to 0.03. The yield strength of the welding wire at 800 DEG C is not less than 600 MPa. An alloy comprises, by mass percent, 25-30% of Co, 20-23% of Cr, 1.4-1.8% of Al, 2.1-3.6% of Ti, 1.5-2.0%of Nb, 0.5-1.0% of Mo, less than or equal to 0.1% of Si, less than or equal to 0.3% of Mn, less than or equal to 0.01% of Cu, less than or equal to 0.04% of C, less than or equal to 0.003% of B, and the balance of Ni, and no rare earth element is contained. A deposited metal matrix of the welding wire is an austenite (gamma) phase of a disordered face-centered structure, precipitation strengthening phases are a Ni3 (Al, Ti) gamma'phase and a primary carbide NbC, and carbide phases are distributed between crystals. The welding wire fills up the blank in the prior art, has excellent high-temperature performance, can be widely applied to homogeneous and heterogeneous welding of high-temperature alloy parts under the condition of ultra-supercritical water vapor at the temperature of 750-800 DEG C, and can also replace an existing nickel-based/nickel-cobalt-based high-temperature alloy welding wire.
Owner:CHINA HUANENG GRP CO LTD +1

Method for rapidly wetting carbon fibers in ceramic matrix composite material by taking Fe as active element

The invention discloses a method for rapidly wetting carbon fibers in a ceramic matrix composite material by taking Fe as an active element, namely, Fe-based or alloy type brazing filler metal containing enough Fe is taken as high-temperature active brazing filler metal, and rapid and compact wetting of the carbon fibers is realized in a manner that the active element Fe and the carbon fibers aresubjected to eutectic reaction. The method has the advantages that rapid wetting of the carbon fibers and densification of original pores and brazing seams in the composite material base material in the near-seam area are achieved through eutectic reaction, and a continuous interface reaction phase formed by interface reaction is avoided; the dissolved carbon in the brazing seams is fully graphitized, so that the thermal stress can be reduced; the brazing temperature reaches 1154 DEG C or above, and the service temperature of a brazed joint can be increased; long-time heat preservation is notneeded, and the surface of the composite material does not need to be modified before welding; no or a small amount of precious metal is contained. The problems that when traditional Ag-based active brazing filler metal and Ni-based brazing filler metal are used for brazing ceramic-based composite materials, the joint heat-resisting temperature is low, and the heat preservation time is long are solved.
Owner:咸阳瞪羚谷新材料科技有限公司

Nano silver copper wrapped welding flux preparing method based on phonochemistry

The invention provides a nano silver copper wrapped welding flux preparing method based on phonochemistry. The preparing method comprises the following steps that a copper salt organic solvent solution and a sodium phosphite and protective agent organic solvent solution are mixed, horn type pulse ultrasonic waves straight downwards are applied into the solution, copper nano particle dispersion liquid is obtained through the heating reaction, and Cu nano particles are obtained through cooling, centrifuging and washing; the Cu nano particles and a reducing agent are added in deionized water to be evenly mixed, a silver salt solution is added for the reaction at 30-50 DEG C, silver copper wrapped nano particle dispersion liquid is obtained, the silver copper wrapped nano particle dispersion liquid is centrifuged and washed, and silver copper wrapped nano particles are obtained; and the silver copper wrapped nano particles and a welding paste organic solvent are evenly mixed, and silver copper wrapped nano particle welding paste is obtained. The silver copper wrapped nano particle welding flux prepared through the technical scheme is high in reliability and has the characteristics of low-temperature connection and high-temperature service, protective gas is not needed in the preparing process, the technology is simple, and green and environment protection are achieved.
Owner:HARBIN INSTITUTE OF TECHNOLOGY SHENZHEN (INSTITUTE OF SCIENCE AND TECHNOLOGY INNOVATION HARBIN INSTITUTE OF TECHNOLOGY SHENZHEN)

High-temperature and high-emissivity hafnium oxide base infrared radiating coating and preparing method thereof

InactiveCN109355613ARadiantStrong ionic polarityMolten spray coatingSpray GranulationEmissivity
The invention discloses a high-temperature and high-emissivity hafnium oxide base infrared radiating coating. According to the high-temperature and high-emissivity hafnium oxide base infrared radiating coating, HfO2 powder and rare earth oxide powder serve as main raw materials, water and a binding agent are added in the HfO2 powder and the rare earth oxide powder to prepare uniform slurry, and then the high-temperature and high-emissivity hafnium oxide base infrared radiating coating is formed sequentially through spray granulation, high-temperature roasting and heat spraying. According to the high-temperature and high-emissivity hafnium oxide base infrared radiating coating, compounding of HfO2 powder and Gd2O3 or Sm2O3 and other rare earth oxide is provided for the first time, the heatspraying technology is combined, the full-wave band normal integral emissivity of the obtained high infrared radiating coating at the normal temperature can reach 0.85 or above, the slow ascending tendency is achieved along with increasing of the high temperature, and good high temperature resisting performance and full-wave band infrared radiation performance can be combined; and the related preparing technology is simple, the synthesis time is short, energy consumption is low, and important study and popularization value is achieved.
Owner:WUHAN UNIV OF TECH

Contact reaction brazing process for connecting TZM alloy and graphite through pure zirconium layer

The invention relates to the technical field of brazing, and discloses a contact reaction brazing process for connecting TZM alloy and graphite through a pure zirconium layer, which comprises the following steps: step 1, taking TZM alloy, graphite and Zr foil to be welded, polishing the surfaces to be welded by using abrasive paper, and ultrasonically cleaning the sample in an organic solution for 30 minutes; and 2, grooving the surface of the graphite in the step 1, and then sequentially putting Zr foil and TZM alloy into the grooves in the surface of the graphite so as to prevent the sample from being misplaced and prevent brazing filler metal from flowing out. And (3) the workpiece assembled in the step (2) is put into a furnace cavity of a vacuum air pressure sintering furnace, the furnace cavity is vacuumized to be lower than 1 * 10 <-3 > Pa, then argon is filled into the furnace cavity to reach the set pressure, and the temperature is increased to 1000 DEG C from 20 DEG C at the speed of 50 DEG C/min. According to the method, the requirement for the smoothness of the welding surface can be lowered by adding the zirconium middle layer, and the welding surface can be subjected to various treatments such as polishing, sand blasting and machining according to the requirements so as to increase the mechanical occlusal force.
Owner:HEFEI UNIV OF TECH

Refractory metal surface in-situ reaction self-generation high-temperature diffusion barrier and preparing method thereof

ActiveCN110373628AGuaranteed high temperature oxidation resistanceImprove high temperature service lifeSolid state diffusion coatingSlurryOxidation resistant
The invention discloses a refractory metal surface in-situ reaction self-generation high-temperature diffusion barrier. The refractory metal surface in-situ reaction self-generation high-temperature diffusion barrier is located between refractory metal and sintered silicide high-temperature protection coating coated on the surface of the refractory metal, and SiC serves as the main phase. The invention further discloses a preparing method of the refractory metal surface in-situ reaction self-generation high-temperature diffusion barrier. According to the method, graphene slurry or graphene oxide slurry and silicide composite suspension slurry are sequentially preset on the pre-treated refractory metal matrix surface, through sintering, the in-situ reaction self-generation high-temperaturediffusion barrier is obtained, the in-situ reaction self-generation high-temperature diffusion barrier reduces the high-temperature mutual diffusion rate between the high-temperature protection coating and the refractory metal matrix, the high-temperature oxidation resistance of the high-temperature protection coating is ensured, the high-temperature service life is prolonged, due to the in-situ reaction self-generation high-temperature diffusion barrier, the interfacial compatibility is improved, and the refractory metal-diffusion barrier-high-temperature protection coating has the good heatcycle resistance and thermal shock resistance.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Method for obtaining ferritic heat-resisting steel with the characteristic of austenite structure

The invention relates to a method for obtaining ferritic heat-resisting steel with the characteristics of an austenite structure, and belongs to the technical field of heat-resisting steels. A large deformation+heat treatment process is adopted, and the technical parameters controlled in process steps are as follows: heating 9%-12% Cr steel to 1100-1200 DEG C at 20 DEG C / s, and keeping temperature for 30-120 minutes; then cooling to 500-800 DEG C at 10 DEG C / s, keeping the temperature for 3-15 seconds, deforming at the deformation rate of 1s<-1> and the deformation amount of 70%-90%, immediately quenching to room temperature after the deformation is completed; then tempering at 650-800 DEG C for 1-5 hours, and air-cooling to room temperature. The method disclosed by the invention is used for preparing the 9%-12% Cr steel and a large-caliber boiler pipe thereof. According to the invention, the initial size of a precipitated phase is obviously thinner than the initial size of a precipitated phase treated through the traditional heat treatment mechanism, a ferrite structure has characteristics similar to the characteristics of the austenite structure, belongs to an equilibrium state and is small in interface quantity and less in diffusion channel; a base body has good structure stability in a long-time service process.
Owner:CENT IRON & STEEL RES INST
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