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203results about How to "Continuous industrial production" patented technology

Lithium ion battery cathode material with variable slope concentration gradient doping structure and preparation thereof

InactiveCN108649205AThe rate of change of concentration increasesGood element doping distributionElectrode thermal treatmentSecondary cellsSurface layerSynthesis methods
The invention discloses a lithium ion battery cathode material with a variable slope concentration gradient doping structure and a synthesis method thereof. For solving the problems of capacity fadingand rate performance degradation which are brought by the conventional doping method, an element with a variable slope concentration gradient structure is doped, thereby obtaining the lithium ion battery cathode material with the concentration of a doping element continuously changed from the center of a material particle to the surface of the material particle; and change rate is gradually increased from inside to outside, so that the concentration of the doped element inside the material is slowly changed, the concentration of the doped element on the surface of the material is rapidly changed, and change of the concentration of the doped element is mainly concentrated on a surface layer. The method improves stability of the internal structure and the surface of the material while sideeffect is not introduced, the problems such as phase change of the material, volume change and dissolution of transition metal elements in a charge-discharge cycle process are reduced, cycle life of the material is greatly prolonged, and safety performance of the material is greatly improved.
Owner:HARBIN INST OF TECH

Method for continuously refining L-lactide from crude L-lactide

The invention discloses a method for continuously refining L-lactide from crude L-lactide, which comprises the following steps of: firstly, performing at least once lightness removal to the crude L-lactide by using a lightness-removing column, sending melted crude L-lactide into the middle of the lightness-removing column, refluxing and separating as well as distilling the crude L-lactide in the lightness-removing column, condensing vapor distillate at the upper end of the lightness-removing column for removing water, L-lactate and meso-lactide; secondly, enabling column bottom liquid to enter a reboiler for vaporization and then enter into the column, performing at least once rectification to the left column bottom liquid through a treating column after cooling, wherein the lower end of the lightness-removing column mainly has high-boiling point distillate liquid comprising the L-lactide and lactate oligomer; and when in rectification, refluxing and separating the column bottom liquid of the lightness-removing column to obtain a refined L-lactide; refining column bottom flow to obtain concentrated lactate oligomer. The L-lactide purified by the method can be directly used in the polymerization of poly L-lactate, thereby lowering the purifying cost of the L-lactide, increasing the yield, and being environmental friendly without organic solvents.
Owner:南京冠创生物科技有限公司

Preparation method of long-fiber reinforced polypropylene microcellular foam material

The invention discloses a preparation method of a long-fiber reinforced polypropylene microcellular foam material. The method includes the following steps of adding 45-80 parts of raw material into an extruder, wherein the raw material is polypropylene resin; adding 10-45 parts of long fiber and 2-12 parts of supercritical fluid into the middle section of the extruder respectively to be sufficiently mixed to obtain a melt mixture; making the melt mixture pass through a die head of the extruder to be subjected to depressurization foaming to obtain the long-fiber reinforced polypropylene microcellular foam material, wherein the extruder is formed by connecting a twin-screw extruder with a single-screw extruder in series, the temperature of the first region of the single-screw extruder is 120-140 DEG C, the temperature of the die head is 150-175 DEG C, and the pressure of melt in the die head is 6-20 MPa. Compared with a material where fiber is not added or ordinary short-cut fiber is added, the strength and modulus of the long-fiber reinforced polypropylene microcellular foam material can be remarkably improved; the material is formed, extruded and prepared through one step, continuous industrial production can be achieved, and production efficiency is greatly improved. The material is safe, free of toxin, green and environmentally friendly.
Owner:GUANGZHOU HKUST FOK YING TUNG RES INST

Method for processing high-performance modified polyethylene monofilaments for manufacturing fishing net

The invention discloses a method for processing high-performance modified polyethylene monofilaments for manufacturing a fishing net, relates to a method for processing polyethylene monofilaments for manufacturing a fishing net and aims to provide a method for processing the high-performance modified polyethylene monofilaments for manufacturing the fishing net. In the technical scheme of the invention, a stirring machine, a single-screw extruder, a twice-drafting electrical heating drafting machine, a filament winding machine and a filament separating machine are adopted. The method is characterized by comprising the following steps of: mixing a sieved spinning-grade dry HDPE resin, a dry VERSIFYTM 6002 elastomer, white oil or a turpentine aid; uniformly mixing the materials to obtain an HDPE / VERSIFYTM 6002 elastomer blend and fusing and extruding the blend by using the single-screw extruder; cooling and pre-drafting fused and extruded primary filaments, thermally drafting the pre-drafted filaments twice, rapidly cooling the thermally-drafted filaments from which oil is removed with high-pressure air current and winding modified PE monofilaments by using the winding machine; and separating the modified PE monofilaments into the high-performance modified polyethylene monofilaments for manufacturing the fishing net by using the filament separating machine.
Owner:EAST CHINA SEA FISHERIES RES INST CHINESE ACAD OF FISHERY SCI

Electrostatic spinning submicron fiber and sliver composite blended yarn preparation device and method

ActiveCN107904732AEquipment modification is simpleWide range of applicationsFilament/thread formingYarnElectrospinningSolvent
The invention discloses an electrostatic spinning submicron fiber and sliver composite blended yarn preparation device and method. The preparation device comprises a drawing frame and an electrostaticspinning device, the electrostatic spinning device comprises needle-free electrostatic spinning spray heads located on the two sides of a sliver respectively and a receiving pole plate, and the needle-free electrostatic spinning spray heads are connected with a high voltage generator; a liquid storage bottle is communicated with the needle-free electrostatic spinning spray heads. The preparationmethod comprises the steps that a control valve and a liquid supply pump are opened, and a spinning solution in the liquid storage bottle flows into the needle-free electrostatic spinning spray heads;the drawing frame is started, the high voltage generator is connected with the needle-free electrostatic spinning spray heads, the high voltage generator is started, multiple jet flows are sprayed out from the needle-free electrostatic spinning spray heads, in the process that the jet flows fly to the receiving pole plate, solvent is volatilized, high polymer is stretched and cured, and submicronfibers are formed and deposited on the sliver. Accordingly, blending of electrostatic spinning submicron fibers and fibers for traditional textile can be achieved, and the functional characteristicsof the submicron fibers are applied to the traditional textile.
Owner:DONGHUA UNIV

Method for producing inonotus obliquus exopolysaccharides through submerged fermentation

The invention belongs to the technical field of microorganisms, and relates to a method for producing inonotus obliquus exopolysaccharides through submerged fermentation, particularly to a method for industrial-scale production of the inonotus obliquus exopolysaccharides. The method comprises the steps as follows: activated inonotus obliquus strains are inoculated into a seed tank for propagation, then propagated liquid seeds are inoculated into a specially-made polysaccharide-producing liquid culture medium for fermentation, and a fermentation liquid is separated to extract the exopolysaccharides. According to the method, research is conducted to overcome defects in the prior art, on the premises that a fermentation culture medium (especially a carbon source) is continuously optimized through small and medium tests and the biomass and the exopolysaccharides are increased, the problems of fermentation process parameter control, extracting equipment model selection, optimization and the like in the process of enlargement from the small tests to industrial production are solved, the strains are successfully inoculated into fermentation tanks of 10-20 t finally for industrial production, the high-quality inonotus obliquus polysaccharides are produced smoothly, and the continuous, automatic and industrial production is actually realized.
Owner:JIANGSU SHENHUA PHARMA

Method for extracting silver from silver-containing crude tin alloy

The invention provides a method for extracting silver from silver-containing crude tin alloy. The method comprises the following steps of: heating the silver-containing crude tin alloy to reach the temperature of 430 to 500 DEG C for melting; feeding a zinc ingot into the molten silver-containing crude tin alloy, and agitating to dissolve; cooling the dissolved mixture to reach the temperature of 390 to 400 DEG C; and centrifugally separating at a rotating speed of 200-700rpm until the surface of the liquid at the upper layer has no floating slags, so as to obtain the tin liquid at the upper layer and the sliver-zinc slags at the lower layer; naturally cooling and condensing the tin layer to obtain the tin alloy without silver; and distilling the silver-zinc slags under the vacuum to obtain the silver and the crude zinc, wherein the silver in the tin alloy subjected to silver extracting is less than 10g / t. According to the method, the whole process is safe and controllable; the method is convenient to operate, and has no exhaustion of three wastes; and the method has high universality to the raw materials; the tin alloys with different silver contents can be effectively processed; the continuous industrial production can be achieved; and high recovery rate of the tin and the silver can be ensured; the silver in the silver-containing tin alloy can be efficiently extracted; with adoption of the method, the quality of the tin can be improved, and large amounts of silver can be recovered for the enterprises.
Owner:KUNMING UNIV OF SCI & TECH

Household waste incineration fly ash cyclic utilization method

The invention relates to a household waste incineration fly ash cyclic utilization method. A flow distributing device is installed at the lower end of a dust remover of a waste incineration smoke treatment system and controls the amount of fly ash circularly entering a non-medium grinding machine, and therefore the phenomenon that since the fly ash agglomerates at a grinding medium or adheres to the inner wall of the grinding machine, the grinding effect is influenced is avoided. After the fly ash is smashed in a grinding bin, a high-pressure centrifugal fan brings the grinded powder materialsinto a powder selecting machine, fine powder meeting the fineness requirement enters a circulatory system along with airflow, and coarse particle materials incapable of meeting the fineness requirement return to the grinding bin to continue to be grinded. It is guaranteed that the particle sizes of the grinded fine powder are uniform and kept within a certain range, unreacted calcium hydroxide isfully exposed, the specific surface area of the fly ash is increased, the utilization rate of the calcium hydroxide in the fly ash can be improved to be 80% or over, and continuous industrial production can be achieved. Meanwhile, phosphate is fed into the non-medium grinding machine so as to pre-stabilize heavy metal and reduce the application amount of follow-up deacidification agents, and thephosphate also has the grinding assistance function. A strong oxidant is added and achieves the desulfurization and denitration function and the function of promoting dioxin to decompose.
Owner:TIANJIN YIMING ENVIRONMENTAL TECH CO LTD
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