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46results about How to "Improve hydrophilicity and hydrophobicity" patented technology

Fabricating method of fiber powder modified polymer microporous film

The invention relates to a macromolecule separation microporous membrane and a preparation method thereof, in particular to a preparation method of modified fiber powder / polymer mixed microporous membrane. The method provided by the invention includes the following steps: the surface of the fiber powder is cleaned and carved; the surface-carved fiber powders, polymer, various additives and solutions are combined to prepare membrane casting liquid, and then the membrane casting liquid is put onto a glass plate for membrane-shaving or spanning and then the liquid membrane is gelatinized into membrane in the coagulation bath process, and finally the membrane is dipped in membrane-dipping liquid and then is dried. The invention can prepare the polymer microporous membrane which has low cost, high strength and better capability through adding various fiber powders into the membrane preparation liquid and changing process conditions.
Owner:WUHAN TEXTILE UNIV

Polyester composite fiber with intelligent surface, and preparation method and application thereof

The invention discloses a polyester composite fiber with an intelligent surface, and a preparation method and application thereof. The polyester composite fiber comprises a polyester fiber matrix andparticles covering the polyester fiber matrix, wherein the particles and the polyester fiber matrix are chemically bonded; preferably, the particles are polymer particles; more preferably, the particles are polymer particles with environmental response; thus, covering of the surface of the polyester fiber matrix with the particles can improve the hydrophilicity and hydrophobicity of the fiber andendows the fiber with certain environmental response. The preparation method comprises the following steps: preparing the polyester fiber matrix having reactive groups on the surface at first; then preparing the particles having reactive functional groups; and finally, mixing the polyester fiber matrix and the particles for a reaction so as to obtain the polyester composite fiber. The polyester composite fiber of the invention can be used for smart textiles, non-woven fabrics, porous films, composite materials and oil-water separators, preferably for smart textiles and oil-water separators.
Owner:BEIJING INSTITUTE OF CLOTHING TECHNOLOGY

Membrane electrode of direct carbinol full cell fed by liquid state and its prepn. tech

Proton exchange membrane is adopted in membrane electrode. There is catalyst supported by carbon paper treated by Teflon latex on two sides of the membrane. Carbon carried platinum-ruthenium catalyst is as anode, and Carbon carried platinum catalyst is as cathode. The preparing procedure includes: preparation of membrane and pretreatment, preparation of catalyst and paste, preparation of anode and cathode, and hot pressing procedure. Advantages are: new type proton exchange membrane of blocking alcohol raises fuel utilization and voltage discharged at low current of DMFC, improves transferring fuel, oxidant, CO2 and water inside membrane electrode.
Owner:TIANJIN UNIV

Rice-dedicated slow release fertilizer and preparation method thereof

The invention relates to the technical field of slow release fertilizer, in particular to a rice-dedicated slow release fertilizer and a preparation method thereof. Raw materials include organic fertilizer, monopotassium phosphate, sulfate, urea and medical stone powder and can also include chitosan sodium glycero-phosphate temperature-sensitive gel. The rice-dedicated slow release fertilizer is comprehensive and balanced in nutrition; through reasonable arrangement of a coating structure, nutrient release is matched with rice required fertilizer, and therefore the nutrient resource utilization rate is raised; physiological disease resistance of rice is enhanced, the lodging-resistance capability is enhanced, the demand of rice in the maximum absorption period can be met, therefore, the yield of rice is increased, and the quality of rice is improved.
Owner:GUIYANG KAILIN FERTILIZER CO LTD

Antibacterial-plant-pigment-added biodegradable packaging material and preparation method thereof

The invention discloses an antibacterial-plant-pigment-added biodegradable packaging material and a preparation method thereof, belonging to the technical field of packaging material production. The biodegradable packaging material comprises the following components in parts by mass: 70-90 parts of material body, 5-30 parts of modified vinasse fiber, 0.1-5 parts of coupling agent, 0.2-3 parts of heat stabilizer, 0.3-1.5 parts of antioxidant and 0.5-15 parts of plant-derived pigment. The packaging material has the advantages of favorable biodegradability, favorable antibacterial property, favorable thermodynamic stability, high tensile strength, favorable hydrophilicity and high degradation rate. The preparation method of the antibacterial-plant-pigment-added biodegradable packaging material comprises the following steps: banburying and blending the raw materials, carrying out melt extrusion at 100-120 DEG C, and carrying out blow molding forming. The preparation method has the advantages of simple technical operation, low facility request and environment friendliness, and is suitable for industrial large-scale production.
Owner:陕西鼎夏生物科技有限公司

Polyetheretherketone composite implant as well as preparation method and application thereof

The invention discloses a polyetheretherketone composite implant as well as a preparation method and application thereof. The composite implant comprises a polyetheretherketone substrate, a degradable polymer coating wrapping the surface of the polyetheretherketone substrate, and a functional substance loaded and / or grafted by the degradable polymer coating; the functional substance comprises a substance with an immune regulation function and / or a substance with an osteogenesis regulation function. The preparation method comprises the following steps: constructing the degradable polymer coating loaded with the functional substance on the surface of the polyetheretherketone substrate; modifying and activating the surface of the degradable polymer coating loaded with the functional substances, and introducing active groups to the surface of the degradable polymer coating loaded with the functional substances; and then the functional substances are grafted through active groups. The polyetheretherketone composite implant is applied to preparation of a medicine for treating bone defects. According to the polyetheretherketone composite implant prepared by the invention, the excellent mechanical property of the substrate polyetheretherketone is maintained, and the immunocompetence and the osteogenic activity of the surface are also increased.
Owner:SHENZHEN INST OF ADVANCED TECH

Cerebral cancer suppressing phycocyanin-polylactic acid-adriamycin micelle and preparation method and application thereof

The invention discloses a cerebral cancer suppressing phycocyanin-polylactic acid-adriamycin micelle. Phycocyanin and PLA-PEG-PLA are utilized as raw materials, and a phycocyanin-polylactic acid no-load micelle is formed according to addition reaction of carboxyl and self-assembly principle based on hydrophilia and hydrophobicity. According to the self-assembly principle, adriamycin is coated in the no-load micelle to assemble by itself to form the micelle. The phycocyanin-polylactic acid-adriamycin micelle is a novel nano medicine capable of directly acting on tumor through blood-brain barrier to suppress cerebral cancer cells and capable of releasing slowly to retain in blood for a long time, thereby overcoming influence and limit of the blood-brain barrier to drug treatment effect. Besides, the micelle is prepared from natural or degradable components which are not involved with organic solvents during synthesis, has the advantages such as good biocompatibility, biodegradability, hypotoxicity, high loading capacity, and accordingly has high application potential in treating cerebral cancer.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Preparation method of nanometer porous carbon material

InactiveCN108706583APreserve nanoporous structureChange hydrophilicityCarbon compoundsRoom temperatureNanoporous carbon
The invention relates to a preparation method of a nanometer porous carbon material. The preparation method comprises the following steps: dissolving a template agent in a water solution, and uniformly stirring, thus obtaining a template agent water solution; adding phloroglucin and melamine into the template agent water solution, adding formaldehyde after completely dissolving, then adding a sodium bicarbonate solution, and uniformly stirring, thus forming sol; sealing and putting the sol in a baking oven for carrying out thermal treatment, thus forming gel; cooling to room temperature, thusobtaining organic wet gel; repeatedly washing the organic wet gel in a deionized water solution of sorbitan oleate, and then drying at normal pressure, thus obtaining an organic dry gel block. The nanometer porous carbon material prepared by the preparation method has the characteristics of adjustable density, low cost, high specific surface area and the like, and plays a critical role in the field of electrochemistry.
Owner:TONGJI UNIV

Preparation method and application of vertically-oriented magnetic nanosheet/sodium alginate composite membrane

The invention discloses a preparation method of a vertical orientation magnetic nanosheet / sodium alginate composite membrane. By means of the magnetic field responsiveness of a magnetic nanosheet, a vertical orientation structure is formed in a magnetic field so as to prepare a high-performance pervaporation composite membrane; wherein the magnetic nanosheets comprise nanosheets with intrinsic magnetic responsiveness or other nanosheets which generate magnetic responsiveness by loading magnetic response particles. The preparation method specifically comprises the following steps: uniformly dispersing magnetic nanosheets, physically blending the dispersion with sodium alginate to form a membrane casting solution, carrying out standing treatment for defoaming, spin-coating the membrane casting solution on a polyacrylonitrile ultrafiltration membrane, drying the composite membrane in a magnetic field at room temperature, and carrying out crosslinking treatment to obtain the magnetic nanosheet / sodium alginate composite membrane with vertical orientation. The preparation method is simple and controllable, and the raw materials are cheap and easily available. The composite membrane is suitable for pervaporation ethanol dehydration, has high permeation flux and high selectivity to water molecules, and has good operation stability at high temperature.
Owner:TIANJIN UNIV

Thin film transistor for ultralow-limit detection of C-reactive protein and preparation method thereof

The invention belongs to the technical field of biosensors, and relates to a thin film transistor for ultralow-limit detection of C-reactive protein and a preparation method thereof. Comprising a substrate, a grid electrode, an insulating layer, a P3HT active layer, a source electrode and a drain electrode, wherein the source electrode and the drain electrode are arranged on the active layer; the insulating layer comprises a PVA (Polyvinyl Alcohol) insulating layer arranged on the grid electrode and a PMMA (Polymethyl Methacrylate) insulating layer arranged on the PVA insulating layer; an anti-CRP is fixed on the P3HT active layer channel; the biosensor is prepared by combining a double-dielectric-layer structure and a 3D printing technology; high-selectivity detection of CRP as low as a pM level is realized through physical adsorption of the anti-CRP modified active layer, the anti-CRP does not need to be fixed by a complex modification method, the thin film transistor prepared by the invention is used for detecting C-reactive protein, and the detection limit is as low as 1.8 pmol / L.
Owner:TAIYUAN UNIV OF TECH

Vaccine preparation as well as production method and use of vaccine preparation

The invention provides a vaccine preparation as well as a production method and the use of the vaccine preparation. The vaccine preparation comprises a vaccine carrier and an antigen component, wherein the vaccine carrier is obtained by performing hydrothermal conversion on microorganisms. The vaccine preparation is obtained by compounding the vaccine carrier obtained by performing hydrothermal conversion on microorganisms with the antigen component. According to the vaccine preparation, the vaccine carrier material prepared by virtue of the hydrothermal reaction is optimized in properties such as porosity, hydrophilcity and hydrophobicity and surface immune related ligand density, and therefore, when the vaccine carrier material is compounded with the antigen component, the antigen loading efficiency is improved, the vaccine preparation is enabled to have a strong immune activation effect, the immunogenicity of the loaded antigen is effectively enhanced, and the immunotherapy and prevention of a specific disease are realized by virtue of specific immune response of an organism to the antigen. Besides, the vaccine preparation is wide in raw material source, and has universality in vaccine construction; and as a result, a plurality of vaccine preparations to different diseases can be constructed.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Composite spiral fiber spinning apparatus and spinning method thereof

ActiveCN106555234AHas the characteristics of helical electrospun fibersMeet Biomedical Engineering ApplicationsFilament/thread formingEngineeringHigh pressure
The invention discloses a composite spiral fiber spinning apparatus and a spinning method thereof. The apparatus comprises an insulation liquid storage chamber, high-voltage power sources, a motor and a collector electrode, wherein the upper end of the insulation liquid storage chamber is connected with an output shaft of the motor, the insulation liquid storage chamber is at least provided with two chambers, a stainless steel nozzle is inserted in the bottom of each chamber, the insulation liquid storage chamber is provided with vents in the same quantity as the chambers, each vent communicates with the corresponding chamber, the insulation liquid storage chamber is sleeved by annular brushes in the same quantity as the chamber, each annular brush is connected with the corresponding chamber through a lead wire, each annular brush is connected with the anode of its respective high-voltage power source, and the cathodes of all the high-voltage power sources are connected with the collector electrode. According to the invention, the apparatus has features of electrospun fibers of multiple different materials, effectively improves the mechanical strength and the surface form through an intertwining effect, and has potential application prospect in such aspects as preparation of multifunctional biological supports, composite non-woven fabrics, materials for drug delivery and the like.
Owner:ZHEJIANG UNIV

Preparation method of printable high-strength body temperature release drug hydrogel

The invention discloses a preparation method of a printable high-strength body temperature release drug hydrogel. The preparation method comprises the following steps: preparing chemically crosslinkedPNaAMPS hydrogel, grinding the chemically crosslinked PNaAMPS hydrogel into powder, adding the PNaAMPS powder into a solution containing NIPAM, AAm monomers, an initiator and a crosslinking agent, directly pouring the solution into a glass mold, and carrying out polymerization molding under the illumination of ultraviolet light. The obtained hydrogel has a unique double-network structure, excellent mechanical strength, good toughness and good environmental responsiveness, and can efficiently load and release small molecular drugs in a body temperature environment to achieve an antibacterial effect. The preparation process is simple and easy to implement, the product performance is excellent, and the hydrogel has wide application prospects in the fields of bioengineering, drug controlled release, and the like.
Owner:HUBEI UNIV OF TECH

Circulating cooling system preparation method based on nanometer limited water pressure thermal effect

The invention discloses a circulating cooling system preparation method based on a nanometer limited water pressure thermal effect, and the method comprises the steps: firstly enabling an electronic chip needing to be cooled to be integrated on a silicon wafer, and enabling the silicon wafer to be provided with a groove; depositing a limited layer in the groove; secondly, preparing a rigid nano-pillar array on the surface of the silicon wafer, and enabling the nano-pillar array to be located in the groove of the silicon wafer and to be in contact with the limited layer; casting an epoxy resin film in the groove, cooling, separating the silicon wafer and the silicon wafer, and filling the obtained nano micropore array with a liquid refrigerant through vapor pressure; and finally, depositing a piezoelectric film on the silicon wafer. The piezoelectric film drives the nano-columns to move, so that pressurization and decompression of the refrigerating medium are achieved, water limited in the nano-micropores is induced to generate phase change, and then refrigeration is achieved. The refrigerating system has the advantages of large adiabatic temperature change, wide working temperature range, clean and pollution-free refrigerating medium and the like.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Preparation method of elemental sulfur based ammonium phosphate slow release fertilizer

The invention relates to the technical field of fertilizer processing, in particular to a preparation method of an elemental sulfur based ammonium phosphate slow release fertilizer. The preparation method comprises the following steps of preparation of sulfur sol, mixing, pelleting, coating and cleaning. The preparation method provided by the invention is simple in technology and safe to operate;a prepared coated elemental sulfur based ammonium phosphate product well controls the release rate of nitrogen, phosphorus and sulfur, realizes long-acting release of nutrient elements; and in addition, the contained sulfur and silicon components can promote absorption of other nutrient elements and improve the stress resistance growth of crops.
Owner:GUIYANG KAILIN FERTILIZER CO LTD +2

Polyamide composite fibers with intelligent surfaces and preparation method and application of polyamide composite fibers

The invention discloses polyamide composite fibers with intelligent surfaces and a preparation method and application of the polyamide composite fibers. The polyamide composite fibers comprise a polyamide fiber matrix and particles which cover the polyamide fiber matrix, so that the roughness of the fibers can be improved by covering the surface of the fiber matrix with the particles, the hydrophobicity of the fibers is further improved, and the condition of poor dimensional stability caused by strong hygroscopicity of the polyamide fibers is improved. The preparation is carried out as follows: firstly, obtaining a polyamide fiber matrix with reactive groups on the surface; secondly, obtaining particles with reactive functional groups; and finally, mixing and reacting the polyamide fiber matrix and the particles to obtain the polyamide composite fibers. The polyamide composite fibers can be used for intelligent textiles, non-woven fabrics, porous films, composite materials and oil-water separators, and is preferably used for intelligent textiles and oil-water separators.
Owner:BEIJING INSTITUTE OF CLOTHING TECHNOLOGY

Polyolefin composite material with intelligent surface, and preparation method and application thereof

The invention discloses a polyolefin composite material with an intelligent surface, and a preparation method and application thereof. The polyolefin composite material comprises a polyolefin matrix and particles covering the polyolefin matrix, wherein the particles and the polyolefin matrix are chemically bonded; preferably, the particles are polymer particles; more preferably, the particles arepolymer particles with environmental response; thus, covering of the surface of the polyolefin matrix with the particles can improve the hydrophilicity and hydrophobicity of the material and endows the material with certain environmental response. The preparation method comprises the following steps: preparing the polyolefin matrix having reactive groups on the surface at first; then preparing theparticles having reactive functional groups; and finally, mixing the polyolefin matrix and the particles for a reaction so as to obtain the polyolefin composite material. The polyolefin composite material of the invention can be used for smart textiles, non-woven fabrics, porous films, waterproof gas-permeable membranes, battery diaphragms, composite materials, and switch films.
Owner:BEIJING INSTITUTE OF CLOTHING TECHNOLOGY

Composite fiber with intelligent surface and preparation method and application of composite fiber

The invention discloses a composite fiber with an intelligent surface and a preparation method and application of the composite fiber. The composite fiber comprises a fiber matrix and conductive particles covering the fiber matrix, and the surface of the fiber matrix covered with the conductive particles can improve the specific conductance of the fiber and further improve the electrical conductivity of the fiber. The preparation method comprises the following steps: firstly obtaining a fiber matrix with reactive groups on the surface, then obtaining conductive particles with reactive functional groups, and finally mixing the fiber matrix with the conductive particles for reaction to obtain the composite fiber. The composite fiber can be used for conductive fibers, antistatic fibers or fabrics, electronic circuits, sensors, smart textiles and the like, and is preferably used for conductive fibers and sensing and antistatic fiber fabrics.
Owner:BEIJING INSTITUTE OF CLOTHING TECHNOLOGY

Preparation method of silane modified attapulgite clay and application thereof in removing pesticide residues from Chinese herbal medicines

The invention discloses a preparation method of silane modified attapulgite clay and application thereof in removing pesticide residues from Chinese herbal medicines. The preparation method of the silane modified attapulgite clay includes purification of attapulgite, acidification and silane modification of the attapulgite clay. The application steps of the silane modified attapulgite clay in removing the pesticide residues from Chinese herbal medicines include weighing Chinese herbal medicine extracts, and placing the silane modified attapulgite clay in a mixed pesticide aqueous solution; performing shock adsorption at the constant temperature of 15-25 DEG C for 1-2 hours; centrifuging with the rotating speed of 11000 r / min<-1> for 5-10 minutes; adopting GC-MS / MS to analyze the pesticidecontent of supernatant liquid; and adopting the GC-MS / MS to analyze the pesticide content of raw materials in the traditional Chinese medicine extracts. The method of the invention has the advantagesof simple process, convenient operation and no potential safety hazard; the pesticide residues in the traditional Chinese medicine extracts meet the maximum pesticide residue limit standards of countries and regions such as China, the European Union, the United States and the like after being removed; and moreover, the attapulgite clay is abundant in storage and low in price in China.
Owner:HUAIYIN INSTITUTE OF TECHNOLOGY

Gas diffusion layer structure of electrochemical oxygen generator membrane electrode and preparation method

The invention discloses a gas diffusion layer structure of an electrochemical oxygenerator membrane electrode and a preparation method, the gas diffusion layer structure comprises a cathode gas diffusion layer and an anode gas diffusion layer, the cathode gas diffusion layer comprises a cathode conductive porous substrate layer and a cathode microporous layer arranged at the inner side of the cathode conductive porous substrate layer; the anode gas diffusion layer comprises an anode conductive porous substrate layer and an anode microporous layer arranged on the inner side of the anode conductive porous substrate layer, the anode microporous layer comprises carbon particles and a binder, and the cathode microporous layer comprises carbon particles, a binder, a water absorbent and an adsorption material. Compared with the prior art, the electrochemical oxygen generator has the advantages that the conductivity is good, the hydrophilic and hydrophobic properties of the cathode gas diffusion layer and the anode gas diffusion layer are different, the gas diffusion performance and the water management performance of the electrochemical oxygen generator are improved, the water-gas distribution performance of the cathode gas diffusion layer and the anode gas diffusion layer is optimized, the electrolysis rate of the anode side water is further improved, and the electrochemical oxygen generator is more stable. And oxygen can be stably produced under the condition of low humidity.
Owner:江西德合医疗器械有限公司

Preparation method of sewage treatment agent and application of sewage treatment agent in ozonized water treatment

The invention discloses a preparation method of a sewage treatment agent and application of the sewage treatment agent in ozonized water treatment, and belongs to the technical field of sewage treatment materials. The method comprises the steps: adding the dispersion liquid 2 in the step 2 into the dispersion liquid 1 in the step 1, continuously stirring to obtain a dispersion liquid 3, and adjusting the pH value of the dispersion liquid 3 to 9-11 through a sodium hydroxide solution to obtain a dispersion liquid 4; transferring the dispersion liquid 4 in the step 3 into a polytetrafluoroethylene-lined stainless steel high-pressure reaction kettle for hydrothermal reaction; after the reaction is finished, cooling to room temperature, absorbing the supernate, and repeatedly washing with deionized water and ethanol pentahydrate for a plurality of times; after standing and layering, sucking away supernatant liquid containing unreacted impurities again; and freeze-drying the Co3O4 / GO compound with low water content in the lower layer to finally obtain the sewage treatment agent. The cobaltosic oxide composite aerogel with different hydrophilicity and hydrophobicity is synthesized by adopting a simple method, and the cobaltosic oxide composite aerogel shows excellent performance on ozonization degradation of hydrophilic / lipophilic pollutants.
Owner:邹金宏

Anti-condensation method in dry carbide slag recycling process

ActiveCN112916594AImprove moisture absorption and condensation performanceOptimizing short-range resource utilization technologyCalcium/strontium/barium carbonatesSolid waste disposalSlagCorrosion
The invention provides an anti-condensation method in a dry carbide slag recycling process. The method comprises the following steps of adding a dehumidizer in an impurity removal process in the dry carbide slag recycling process, and mixing dry carbide slag and the dehumidizer, wherein the content of particles with the particle diameter smaller than 50 microns in the dehumidifier is greater than or equal to 80wt%, and the content of particles with the particle diameter smaller than 20 microns in the dehumidifier is larger than or equal to 40wt%. According to the method, the moisture absorption condensation performance of the dry carbide slag is avoided, the resource short-distance utilization technology of the dry carbide slag is optimized, the risks of bag pasting and corrosion of the surface of a bag type dust collector are reduced, the equipment maintenance frequency is reduced, the method is simple in process, product performance is not affected, the difficulty in the dry carbide slag recycling process is effectively solved, and good economic and social value is achieved.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Amphipathic random copolymer with disulfide bond and preparation method and application of amphipathic random copolymer

The invention discloses an amphipathic random copolymer with a disulfide bond and a preparation method and application of the amphipathic random copolymer. The preparation method comprises the following steps: firstly, synthesizing monomers with a disulfide bond and an aldehyde group respectively, performing a double-bond addition reaction of the monomers, and performing RAFT (reversible additionfragmentation chain) polymerization so as to synthesize the amphipathic random copolymer. Because of existence of the disulfide bond, the amphipathic random copolymer disclosed by the invention has good chelation with a nano crystal, and in addition, because of hydrophilic / hydrophobic monomers, the amphipathic random copolymer has amphipathicity, thus has good biocompatibility and has potential application in biological medical application.
Owner:XIAMEN UNIV

Drying agent with heavy metal removal function and preparation method thereof

The invention discloses a drying agent with a heavy metal removal function and a preparation method thereof. The preparation method comprises the following steps: 1, preparing bentonite filtered powder; 2, uniformly mixing the bentonite filtered powder, silicon dioxide nano powder and plant starch, adding water, and preparing a suspension; 3, adding an organic modifier and an auxiliary modifier into the suspension, adjusting the pH with a sodium hydroxide solution and then heating to prepare modifiedbentonite; 4, soaking the modified bentonite in a hydrochloric acid solution, washing the modified bentonite to be neutral with deionized water, granulating, and drying to obtain the spherical drying agent with the particle size of 1-3 mm. The prepared drying agent has a good adsorption effect on heavy metal ions, especially for heavy metal ions such as copper, chromium, nickel, lead, iron and zinc, the lead ion adsorption rate can reach 75% or above, and the chromium ion adsorption rate can reach 80% or above.
Owner:ANQING XINXIANGRUI CHEM CO LTD

Intelligent layered nano foam stabilizer, preparation method thereof and application of intelligent layered nano foam stabilizer in foam flooding

The invention discloses an intelligent layered nano foam stabilizer and a preparation method and application thereof in foam flooding, the formula comprises MXene, inorganic matter, an alkali source and a cross-linking agent, and the preparation method comprises the following steps: step 1, weighing raw materials; 2, preparing a mixed solution A; step 3, preparing a mixed solution B; and step 4, obtaining a finished product. The intelligent layered nano foam stabilizer is obtained by performing in-situ crosslinking on the surface and between layers of MXene, depositing magnetic nano particles and improving the hydrophilic and hydrophobic properties of the MXene, and the intelligent layered nano foam stabilizer has the characteristics of prolonging the service life of foam and improving the comprehensive performance of the foam, so that the acting time of the foam in a formation pore throat is prolonged, and the foam is prevented from being damaged. Temporary plugging of large hole channels of the stratum is achieved, and the crude oil recovery rate is increased; and after the foam is broken when meeting oil, the intelligent layered nano foam stabilizer can be quickly recycled and reused through an external magnetic field, and the intelligent layered nano foam stabilizer has important significance on improvement of the foam oil displacement effect and further popularization and application.
Owner:XI'AN PETROLEUM UNIVERSITY +1

A phycocyanin-polylactic acid-doxorubicin micelle for inhibiting brain cancer and its preparation method and application

The invention discloses a cerebral cancer suppressing phycocyanin-polylactic acid-adriamycin micelle. Phycocyanin and PLA-PEG-PLA are utilized as raw materials, and a phycocyanin-polylactic acid no-load micelle is formed according to addition reaction of carboxyl and self-assembly principle based on hydrophilia and hydrophobicity. According to the self-assembly principle, adriamycin is coated in the no-load micelle to assemble by itself to form the micelle. The phycocyanin-polylactic acid-adriamycin micelle is a novel nano medicine capable of directly acting on tumor through blood-brain barrier to suppress cerebral cancer cells and capable of releasing slowly to retain in blood for a long time, thereby overcoming influence and limit of the blood-brain barrier to drug treatment effect. Besides, the micelle is prepared from natural or degradable components which are not involved with organic solvents during synthesis, has the advantages such as good biocompatibility, biodegradability, hypotoxicity, high loading capacity, and accordingly has high application potential in treating cerebral cancer.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Electrolytic manganese slag source decrement method

The invention discloses an electrolytic manganese slag source decrement method. The method is characterized by comprising the following steps that ore slurry is prepared according to a certain solid-liquid ratio of rhodochrosite powder, the ore slurry is fed into a reactor, the proper reaction temperature and the mineral acid ratio are controlled, and after the ore slurry is stirred and mixed, a surfactant with a certain concentration range is added, the pH of the ore slurry is adjusted by adopting an alkaline agent after the reaction is finished, and solid-liquid separation is performed. Compared with a traditional non-surfactant process, the manganese leaching rate is increased by 7-14%, and the water content of manganese slag is reduced by 2-5%. According to the method, by adding the surfactant, the manganese slag particle size in the manganese ore leaching process can be regulated and controlled, the dispersion of manganese slag particles is strengthened, the utilization rate of manganese ore resources is improved, and valuable resources and pollutants entrained in the manganese slag are reduced. Compared with the prior art, the method has the advantages of being simple in process, low in cost and high in operability.
Owner:SOUTHWEAT UNIV OF SCI & TECH

A kind of ionic liquid composite material and its preparation method for separating ephedrine in pinellia

The invention relates to an ionic liquid composite material for separating ephedrine in pinellia ternata and a preparation method thereof and belongs to the technical field of separation of natural products. The ionic liquid composite material and the preparation method thereof provided by the invention have the beneficial effects that the ionic liquid composite material takes a silica gel material as a substrate and is prepared by firstly performing functional group modification on the surface of the silica gel material through ionic liquid and then compounding a molecularly-imprinted polymerlayer on a functional group of the silica gel material; the ionic liquid silica gel-imprinted polymer composite material takes the silica gel material as the substrate and has good acid resistance and mechanical strength; then the group modification is performed on the surface through the ionic liquid, and the adsorption efficiency can be improved by utilizing the excellent solubility, the hydrophobicity and various chemical forces of the ionic liquid; finally, not only is the surface area of the compounded imprinted polymer material increased, but also the adsorption selectivity is greatly improved. The composite material is applied to the separation of a pinellia ternata extract, and the ephedrine can be subjected to highly-selective adsorption separation.
Owner:YANGTZE UNIVERSITY
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