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80results about How to "Increase the spread distance" patented technology

Rare earth hydride surface coating treating agent, application thereof and method for forming rare earth hydride surface coating

The invention discloses a rare earth hydride surface coating treating agent, a method for forming a rare earth hydride surface coating and application of the rare earth hydride surface coating treating agent, which are used for improving the coercive force of a sintering NdFeB magnet and belong to the technical field of magnetic materials. The coating treating agent is a colloid solution formed by dispersing rare earth hydride into a methanol or ethanol solvent. The method for forming the rare earth hydride surface coating comprises the following steps of: injecting the treating agent into glassware and soaking a magnet into a solution; carrying out ultrasonic processing on the treating agent containing the magnet so that rare earth hydride in the treating agent is uniformly coated on the surface of the magnet to form a surface coating with even thickness; taking the magnet provided with the rare earth hydride surface coating out of the solution and volatilizing the solvent in the magnet surface coating in an air drying way to form a coating; and placing the air dried magnet into a vacuum heat treatment furnace and carrying out heat treatment for 0.5-2 hours in a temperature range of 500-950 DEG C. The invention can obviously improve the magnetic performance of the magnet, especially the coercive force of the magnet.
Owner:BEIJING UNIV OF TECH

Calcium vanadate mesoporous nanowire and preparation method and application thereof

The invention relates to a calcium vanadate mesoporous nanowire material and a preparation method thereof. The material can be used as a sodium-ion battery anode active material. The calcium vanadate mesoporous nanowire is obtained in combination with post heat treatment by using a hydrothermal process, the molecular formula of calcium vanadate is CaV4O9, the diameter of the nanowire is 100-200 nm, the length of the nanowire is 5-10 microns, a large number of mesopores are uniformly formed in the surface of the nanowire, and the pore diameters of the mesopores are 20-50 nm. The calcium vanadate mesoporous nanowire material has the beneficial effects that the calcium vanadate mesoporous nanowire material has relatively high specific capacity, good cycling stability and extremely excellent rate capacity when being used as the sodium-ion battery anode active material, and is a potential high-performance sodium-ion battery anode material; and moreover, the preparation method is simple in technology, and the calcium vanadate mesoporous nanowire can be obtained through the simple hydrothermal process and subsequent heat treatment, so that the method is green and environmentally-friendly and relatively low in energy consumption.
Owner:WUHAN UNIV OF TECH

Method for connecting skutterudite thermoelectric material and electrode by using high-thermal-stability alloy composite intermediate layer

The invention relates to a method for connecting a skutterudite thermoelectric material and an electrode by using a high-thermal-stability alloy composite intermediate layer, in particular to the method for connecting the skutterudite thermoelectric material and the electrode. The method aims to solve the problems of poor thermal stability and large contact resistance of a joint obtained by the existing skutterudite thermoelectric material welding method. The method comprises the following steps of 1, cleaning the skutterudite thermoelectric material and the electrode; and 2, preparing the intermediate connecting layer and a diffusion barrier layer by using an electroplating or physical vapor deposition method, and carrying out diffusion welding, wherein the intermediate connecting layer is made of Co, Fe or Ni, and the diffusion barrier layer is made of CoMo, CoW, FeMo or FeW. According to the method, the joint obtained by utilizing the intermediate connecting layer and the diffusionbarrier layer has low contact resistivity, and the thermal stability of the joint is high. The method is suitable for connecting the skutterudite thermoelectric material and the electrode.
Owner:HARBIN INST OF TECH

Semiconductor structure and forming method thereof

The invention discloses a semiconductor structure and a forming method thereof. The method comprises the steps of forming a substrate, wherein the substrate comprises a substrate, a gate structure located on the substrate, source-drain doped regions located in the substrate at two sides of the gate structure, and a dielectric layer located on the substrate from which the gate structure is exposed;forming contact openings for exposing the source-drain doped regions in two sides of the gate structure, wherein each contact opening comprises a through hole penetrating through the substrate with the thickness of the dielectric layer, and a groove penetrating through the substrate with the thickness of the part corresponding to each source-drain doped region, and the bottom size of each grooveis smaller than the top size in the direction vertical to the extension direction of the gate structure; covering the surfaces of the grooves with a metal silicide layer in a conformal manner; and forming the metal silicide layer and then forming contact hole plugs in the contact openings. The bottom size of each groove is smaller than the top size, so that, compared with a scheme that side wallsof the grooves are vertical to the substrate, the semiconductor structure has the advantages that the diffusion distance from metal atoms to a channel region in the process of forming the metal silicide layer can be increased, and the possibility that the metal atoms are diffused to a bulk region of the substrate is reduced, thereby reducing bulk leakage current.
Owner:SEMICON MFG INT (SHANGHAI) CORP +1

Hot galvanized high-strength steel plate with high surface quality and excellent corrosion resistance and manufacturing method thereof

The invention discloses a hot galvanized high-strength steel plate with high surface quality and excellent corrosion resistance and a manufacturing method thereof. The hot galvanized high-strength steel plate sequentially comprises a substrate, a pre-metallization layer and Fe-Al barrier layer and a galvanized layer from bottom to top, wherein the chemical composition of the substrate comprises the following chemical components of, in percentage by weight, 0.15 wt% to 0.25wt% of C, 1.00 wt% to 2.00 wt% of Si, 1.50 wt% to 3.00 wt% of Mn, less than or equal to 0. 015 wt% of P, less than or equalto 0.012 wt% of S, 0.03 wt% to 0.06 wt% of Al and the balance Fe and inevitable impurities, and the pre-metallization layer is a metal Ni layer. The hot galvanized high-strength steel plate is good in surface quality, uniform and complete in plating layer, and better in corrosion resistance compared with a conventional hot galvanized product; and the yield strength of the hot galvanized steel plate is 600-900 MPa, the tensile strength is 980 MPa or above, the elongation is 15-22%, the surface quality and corrosion resistance are superior to those of conventional hot galvanized high-strength steel, and the hot galvanized teel plate is suitable for automobile structural parts and outer plates with higher requirements on surface quality, corrosion resistance and formability.
Owner:BAOSHAN IRON & STEEL CO LTD

Preparation method of polyhedral nano oxide for catalyzing

The invention relates to a preparation method of polyhedral nano oxide for catalyzing. The preparation method comprises the following steps: preparing nano polyhedral copper oxide powder by a salt melting method taking a potassium source and a sodium source as melted salt; dissolving copper salt into water to prepare a solution; dropping an alkali source into the solution until the pH of the solution is 6-8; putting the solution into a constant-temperature magnetic stirrer to be stirred at constant temperature of 60 DEG C; filtering and washing for two to three times after sediment is generated and putting the product into a drying oven to be dried; putting a dried precursor, sodium salt and potassium salt into a ball milling tank to be milled; drying the milled mixed solution and transferring the solution into a crucible to be calcined; then cooling in the air to room temperature; and filtering, washing and drying to prepare the nano polyhedral copper oxide powder. The preparation method has the advantages of low synthesis temperature, simplicity in operation, uniform chemical components of the synthesized powder, good crystal appearance and the like; and a Rhodamine B degrading experiment shows that compared with commodity nano copper oxide, the catalyzing performance is greatly improved.
Owner:上海泛翌新材料有限公司

Rare earth hydride surface coating treating agent, application thereof and method for forming rare earth hydride surface coating

The invention discloses a rare earth hydride surface coating treating agent, a method for forming a rare earth hydride surface coating and application of the rare earth hydride surface coating treating agent, which are used for improving the coercive force of a sintering NdFeB magnet and belong to the technical field of magnetic materials. The coating treating agent is a colloid solution formed by dispersing rare earth hydride into a methanol or ethanol solvent. The method for forming the rare earth hydride surface coating comprises the following steps of: injecting the treating agent into glassware and soaking a magnet into a solution; carrying out ultrasonic processing on the treating agent containing the magnet so that rare earth hydride in the treating agent is uniformly coated on thesurface of the magnet to form a surface coating with even thickness; taking the magnet provided with the rare earth hydride surface coating out of the solution and volatilizing the solvent in the magnet surface coating in an air drying way to form a coating; and placing the air dried magnet into a vacuum heat treatment furnace and carrying out heat treatment for 0.5-2 hours in a temperature rangeof 500-950 DEG C. The invention can obviously improve the magnetic performance of the magnet, especially the coercive force of the magnet.
Owner:BEIJING UNIV OF TECH

Color adjustable perovskite LED based on micro-nano structure and preparation method thereof

The invention discloses a color adjustable perovskite LED based on a micro-nano structure and a preparation method thereof. The overall device structure, from the bottom up, sequentially includes a tin indium oxide layer, a titanium dioxide layer, a styrene sulfonate layer, a perovskite layer, a 1,3,5-tris(1-phenyl-1H-benzimidazol-2-yl) benzene layer and a lithium/aluminum fluoride layer; the titanium dioxide layer is taken as a scattering body and includes a plurality of single-layer and periodically-arranged titanium dioxide micro-nano structures; a longitudinal section of each titanium dioxide micro-nano structure is of a trapezoid having an upper edge shorter than a lower edge; cross sections of upper and lower surfaces of each titanium dioxide micro-nano structure are of a square respectively; and the titanium dioxide micro-nano structures are arranged orderly and are formed into a clear edge. The invention further discloses a preparation method. Compared with the prior art, thestructure is simple, the preparation method is greatly simplified, the conversion efficiency is high, the energy consumption is low and thus the color adjustable perovskite LED is a novel color adjustable perovskite LED with high brightness, high sensitivity and large color adjustment range.
Owner:HARBIN INST OF TECH SHENZHEN GRADUATE SCHOOL

Circulating pressure-maintaining multi-turn grouting method for dam seepage-proofing reinforcement

The invention belongs to the technical field of seepage-proofing reinforcement of water conservancy foundations, and particularly relates to a circulating pressure-maintaining multi-turn grouting method for dam seepage-proofing reinforcement. The method comprises the following steps that the position of a permeable layer needing to be disposed is determined; holes are distributed in the position,close to the upstream face, of the top of a dam, and then a grouting hole is drilled through a drilling machine; a grouting pipe is arranged in the grouting hole, a hole sealing pipe is shorter than the grouting pipe, and an isolation block is arranged below the hole sealing pipe; an expansion material is injected into the hole sealing grouting pipe for hole sealing and pressure maintaining; and acirculating pressure-maintaining multi-turn grouting method is used for grouting of permeable high polymers, and the grouting pressure is 0.5-2Mpa. According to the method, construction is convenientand fast, the construction period is short, disturbance to the dam is small, the seepage-proofing effect is good, durability is high, full permeation and diffusion of grout are facilitated, subjectivity and experience of the grouting process can be effectively reduced, and grouting construction can be guided.
Owner:SUN YAT SEN UNIV +1

Strip-shaped brazing filler metal for lap joint brazing of copper plate and aluminum plate and preparation method thereof

The invention belongs to the field of welding materials, and relates to strip-shaped brazing filler metal for lap joint brazing of a copper plate and an aluminum plate and a preparation method thereof. The strip-shaped brazing filler metal comprises a brazing filler metal body, a coating I and a coating II, the brazing filler metal body comprises the chemical components of 3.2%-4.5% of nano-zinc oxide, 6.8%-8.2% of selenium, 2.6%-4.2% of aluminum and the balance zinc, the coating I is composed of 90%-92% of surface modified nano-copper and the balance of polyvinyl alcohol, the coating II is composed of 90%-92% of surface modified nano-aluminum and the balance of polyvinyl alcohol, and the molecular weight of the polyvinyl alcohol is 8000 to 12000. According to the strip-shaped brazing filler metal for lap joint brazing of the copper plate and the aluminum plate and the preparation method thereof, the melting point of the brazing filler metal is 330 DEG C +/-10 DEG C, the wettability of the brazing filler metal is good, and due to the existence of the nano-zinc oxide, the nano-copper coating and the nano-aluminum coating, the shear strength of a copper plate and aluminum plate brazed joint is effectively improved and reaches 121 MPa or above. The preparation method is an innovation in the aspect of the strip-shaped brazing filler metal for lap joint brazing of the copper plate and the aluminum plate.
Owner:ZHENGZHOU UNIV

Multi-layer alloy diffusion barrier layer for Cu interconnection integrated circuit and preparation method of multi-layer alloy diffusion barrier layer

The invention belongs to the technical field of semiconductor integrated circuits, and particularly relates to a multi-layer alloy diffusion barrier layer for a Cu interconnection integrated circuit and a preparation method thereof, and the multi-layer alloy diffusion barrier layer sequentially comprises a Si substrate layer, a high-entropy alloy middle barrier layer and a Cu film from bottom to top; the high-entropy alloy middle barrier layer sequentially comprises a first coating, a second coating, a third coating, a fourth coating and a fifth coating from top to bottom; according to the preparation method, NbMoTaW and VCrTiZr high-entropy alloy is used as a target material, a direct-current magnetron sputtering method is adopted, and a coating is sputtered on a Si base body layer to obtain the high-entropy alloy diffusion impervious layer of a Si-VCrTiZr-NbMoTaW-VCrTiZr-NbMoTaW-VCrTiZr-Cu composite structure. The obtained Cu interconnection integrated circuit high-entropy alloy diffusion impervious layer can still keep excellent thermal stability and diffusion impervious performance after being annealed at the high temperature of 400-750 DEG C for 30 min, and has wide application prospects in Cu interconnection integrated circuits.
Owner:亚芯半导体材料(江苏)有限公司 +1

Method for preparing rare-earth magnetic ferrite through in-situ polymerization cracking process

InactiveCN103964833AEvenly dispersedHigh degree of nanometerizationIonIn situ polymerization
The invention discloses a method for preparing rare-earth magnetic ferrite through an in-situ polymerization cracking process. Before a reaction begins, a stable solution is formed by dispersing metal ions in the stoichiometric ratio in an acrylic aqueous solution, various reactant metal ions are thoroughly mixed, and an initiator is added so that a polymerization reaction is aroused quickly. Lots of heat is released in the reaction, and the volume of the reactants expands sharply due to water vapor, so that a honeycombed solid-state polymer is formed. Due to volume expansion, the metal ions are dispersed more evenly, the nanocrystallization degree is high, the reaction activity among nanoparticles is increased, the diffusion distance of ions in a solid-phase reaction is reduced, the diffusibility is improved, and the nucleation and growth speed of a crystalline-state material is accelerated, and then a material uniform in dimension can be obtained through subsequent relative low heat treatment. The prepared material is good in crystallinity and few in crystal defects, and the nanoparticles are dispersed evenly. The method for preparing the rare-earth magnetic ferrite is simple in process, low in preparation temperature, short in heat-preserving time and advantageous for industrial production.
Owner:HUBEI ENG UNIV
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