This invention discloses a method for preparing highly stable gyromagnetic ferrites, belonging to the field of magnetic material preparation technology. The method includes formulation preparation, multi-stage sand milling and
granulation, molding and
sintering,
composite structure preparation, and precision
machining steps. The formulation consists of VIII-series, IIIB-series,
lanthanide-series, IVB-series, and VIIB-series
metal oxides in a specific
molar ratio, with
rare earth nano-additives added to enhance lattice stability. Uniform
slurry particle size is achieved through two-stage sand milling and
spray granulation. A curved
sintering process is used to control the temperature rise and
oxygen content to obtain a high-density
green body. A
yttrium iron garnet or
dysprosium iron garnet functional layer is formed on the surface of the
green body by magnetron
sputtering, constructing a multi-layer
composite structure. Finally, a conductive modification layer is formed on the surface through integrated
laser cutting and chemical mechanical
polishing. The gyromagnetic ferrite material prepared by this method exhibits
high saturation magnetization, low high-frequency loss, and excellent
thermal stability, making it suitable for 5G communication,
radar, and high-frequency
microwave devices.