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39results about How to "Doping effective" patented technology

Preparation method of large single crystal lithium ion battery nickel cobalt lithium manganate cathode material

The invention relates to a preparation method of a single crystal lithium ion battery nickel cobalt lithium manganate cathode material. The method comprises the following steps of: (1) taking a small-grain crystal spherical NCM ternary precursor, a lithium salt and an A element-containing nano fluxing agent as raw materials, uniformly mixing the raw materials by adopting a dry-method high-speed mixing mode, and performing primary sintering under an oxygen-enriched atmosphere condition; (2) subjecting the sintered material to jaw breaking, roller pairing, crushing and sieving so as to obtain asingle-crystal once-sintered base material; and (3) mixing the primary sintering base material with a B element-containing nano coating agent, sintering again under an oxygen-enriched atmosphere condition, and then performing jaw breaking, roller pairing, crushing and sieving to obtain the large single crystal lithium nickel cobalt manganate cathode material. The cathode material prepared by the invention has the characteristics of the large particle size, the good dispersity, the moderate specific surface area, the high compaction density, the high voltage, the good high-temperature cycle performance and the like.
Owner:ZHEJIANG MEIDU HITRANS LITHIUM BATTERY TECHNOLOGY CO LTD

Preparation method of nitrogen-doped silicon-aluminum immobilized TiO2 porous ceramic

The invention provides a preparation method of nitrogen-doped silicon-aluminum immobilized TiO2 porous ceramic. The preparation method comprises the steps of: carrying out reaction with water-soluble inorganic silicon salt as a silicon source, water-soluble inorganic titanium salt as a titanium source, water-soluble inorganic aluminum salt as an aluminum source, urea as a nitrogen source and cetyl trimethyl ammonium bromide as a template agent to obtain a suspension D, transferring the suspension to a hydrothermal kettle, carrying out hydrothermal reaction, after hydrothermal reaction is finished, washing, carrying out suction filtering to obtain filter mud, granulating and shaping the filter mud, then drying to obtain nitrogen-doped silicon-aluminum immobilized TiO2 precursor, and sintering the nitrogen-doped silicon-aluminum immobilized TiO2 precursor to obtain the nitrogen-doped silicon-aluminum immobilized TiO2 porous ceramic. According to the invention, urea is used as the nitrogen source, under hydrothermal high-temperature and high-pressure conditions, N-H bond in urea can replace oxygen in Ti-O to firmly bond in a chemical bond form, thus effective doping is achieved; and in addition, lattice distortion generated due to nitrogen entering TiO2 lattice can broaden photoresponse range of TiO2 and increase photocatalysis activity under visible light.
Owner:SHAANXI UNIV OF SCI & TECH

Near-infrared visible-light OPV iodine-doped photovoltaic organic detector

The invention relates to the field of photoelectronic techniques, in particular to a photoconductive organic semiconductor detector. The invention discloses a near-infrared visible-light OPV iodine-doped photovoltaic organic detector, which comprises a substrate, wherein functional layers are arranged on the substrate. The organic detector comprises the substrate (1), a metal or transparent conductive pole (3), a hole transmission layer (4), an organic photosensitive layer (2) and the like, and is characterized in that the organic photosensitive layer (2) is made of an OPV material, after acceptor-doping of iodine and has photoelectric response to near-infrared light, of a solar cell. The organic photosensitive layer is a common OPV material of a typical solar cell, is subjected to effective acceptor-doping of iodine in order to achieve response to near-infrared bands. The near-infrared visible-light OPV iodine-doped photovoltaic organic detector has the advantages of being easy to achieve large area and large array, having controllable resistance of photosensitive layer material, being able to achieve flexible processing and the like, and has important application value in military, civil use and some specific fields.
Owner:KUNMING INST OF PHYSICS

Polycrystalline silicon ingot and polycrystalline silicon rod prepared from silicon materials purified according to physical method, and methods thereof

The invention discloses a polycrystalline silicon ingot and a polycrystalline silicon rod prepared from silicon materials purified according to a physical method, and corresponding methods thereof. The silicon materials are prepared into the polycrystalline silicon ingot according to a directional solidification method; a first-type element and a second-type element are doped in the preparation process to control the resistivity of the polycrystalline silicon ingot within a preset range, wherein the first-type element controls the resistivity increase of the polycrystalline silicon ingot, andthe second-type element controls the resistivity reduction of the polycrystalline silicon ingot. According to the technical scheme, the polycrystalline silicon ingot is prepared by the directional solidification method to remove metal impurities, and accordingly, the metal impurities in the polycrystalline silicon ingot and the polycrystalline silicon rod can be removed effectively; through dopingof the first-type element and the second-type element, the doping balance in the polycrystalline silicon ingot and the polycrystalline silicon rod can be realized to control the resistivity within the preset range, so that the performance of silicon wafers prepared from the polycrystalline silicon ingot or the polycrystalline silicon rod is improved, and the cost of semiconductor structural devices is effectively reduced.
Owner:ZHEJIANG JINKO SOLAR CO LTD +1

N-type boron nitride film/p-type monocrystalline silicon heterogeneous pn junction prototype device and preparation method thereof

The invention provides an n-type boron nitride film / p-type monocrystalline silicon heterogeneous pn junction prototype device and a preparation method thereof, and belongs to the field of semiconductor materials. The preparation method comprises the following steps: preparing a boron nitride film on a p-type (100) surface monocrystalline silicon substrate by adopting a magnetron sputtering method; carrying out in-situ carbon doping by using a co-sputtering means to obtain an n-type boron nitride film; and respectively manufacturing silver electrodes on one side of the n-type boron nitride film and one side of the p-type monocrystalline silicon to obtain the n-type boron nitride film / p-type monocrystalline silicon heterogeneous pn junction prototype device. According to the invention, the n-type conductive layer with excellent electrical properties is obtained by performing in-situ carbon doping on the boron nitride film, and the electrical properties of the n-type conductive layer are remarkably improved compared with those of non-doped and silicon-doped boron nitride films; and a pn junction prototype device with good rectification characteristics is obtained.
Owner:JILIN UNIV

Preparation method of nitrogen oxide green fluorescent powder material

The invention discloses a nitrogen oxide green fluorescent powder material; and the chemical general formula of the nitrogen oxide green fluorescent powder material is (Ba,A)(2-x)Siy(O,B)zN2+4y-2z:xEu, wherein 0<=x<1.0, 0<y<=1, 1<z<=2.0, A is Ca or Sr element, and B is F or Cl element. In the preparation method, two-step synthesis is adopted to prepare the nitrogen oxide green fluorescent powder and the method comprises the following steps: 1) synthesizing A2SiO4 which is the precursor of the nitrogen oxide green fluorescent powder; and 2) doping elements in the matrix structure provided by the precursor A2SiO4 to synthesize the nitrogen oxide green fluorescent powder material (Ba,A)(2-x)Siy(O,B)zN(2+4y-2z):xEu. By adopting the method, the brightness of the nitrogen oxide green fluorescent powder can be increased and the emission wavelength of the nitrogen oxide green fluorescent powder can be modulated; by adjusting the doping amount of each element, the color gamut of the nitrogen oxide green fluorescent powder can be broadened effectively; and the fluorescent powder can be used to satisfy the lighting demand and used in the white LED backlight with high color rendering index. The method is simple and practical, and is suitable for the large-scale industrial production.
Owner:IRICO

Preparation method of nitrogen-doped silicon-aluminum immobilized TiO2 porous ceramic

The invention provides a preparation method of nitrogen-doped silicon-aluminum immobilized TiO2 porous ceramic. The preparation method comprises the steps of: carrying out reaction with water-soluble inorganic silicon salt as a silicon source, water-soluble inorganic titanium salt as a titanium source, water-soluble inorganic aluminum salt as an aluminum source, urea as a nitrogen source and cetyl trimethyl ammonium bromide as a template agent to obtain a suspension D, transferring the suspension to a hydrothermal kettle, carrying out hydrothermal reaction, after hydrothermal reaction is finished, washing, carrying out suction filtering to obtain filter mud, granulating and shaping the filter mud, then drying to obtain nitrogen-doped silicon-aluminum immobilized TiO2 precursor, and sintering the nitrogen-doped silicon-aluminum immobilized TiO2 precursor to obtain the nitrogen-doped silicon-aluminum immobilized TiO2 porous ceramic. According to the invention, urea is used as the nitrogen source, under hydrothermal high-temperature and high-pressure conditions, N-H bond in urea can replace oxygen in Ti-O to firmly bond in a chemical bond form, thus effective doping is achieved; and in addition, lattice distortion generated due to nitrogen entering TiO2 lattice can broaden photoresponse range of TiO2 and increase photocatalysis activity under visible light.
Owner:SHAANXI UNIV OF SCI & TECH

Organic field effect transistor semiconductor layer P-type doping method and prepared organic field effect transistor

The invention discloses a P-type doping method for a semiconductor layer of an organic field effect transistor and the prepared organic field effect transistor, and the method comprises the steps: dissolving 2, 3, 5, 6-tetrafluoro-7, 7 ', 8, 8'-tetracyanodimethyl p-benzoquinone (F4-TCNQ) in an orthogonal solvent of the organic semiconductor layer to serve as a P-type doping agent; the method comprises the following steps of: preparing an organic semiconductor layer film, spin-coating the organic semiconductor layer film on the spin-coated organic semiconductor layer film in an air atmosphere, and activating doping through rapid thermal annealing, so that the problems caused by jump transmission and coulomb traps in charge transport are solved, the threshold voltage is reduced, and the switch ratio is increased. For the P-type field effect transistor, the P-type doping enhances the hole transport, effectively improves the saturation current, and inhibits the electron transport, so that the power consumption is reduced when the transistor is closed. The doping method is operated based on a solution method, is simple in process and low in preparation cost, can be suitable for large-scale production, and has a very good prospect in application of flexible and portable electronic equipment.
Owner:NANJING UNIV OF POSTS & TELECOMM
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