This invention discloses a method for preparing and applying a high
fluorine-to-carbon ratio fluorinated carbon material, belonging to the field of fluorinated carbon material preparation. The method for preparing a high
fluorine-to-carbon ratio fluorinated carbon material includes the following steps: S1: Crush tea stems and filter to separate the tea stem fragments; S2: Stir the dried tea stem fragments with an acid solution at 100℃-130℃ for 2-4 hours, and wash the tea stem fragments until the pH of the
aqueous solution is 6-8; S3: Heat the tea stem fragments to 140℃-160℃ under an
inert gas
atmosphere. The mixture is heated to ℃ and maintained at that temperature for 1.5-2.5 hours, then carbonized at 1100℃-1400℃ for 2-4 hours. After cooling,
pyrolytic carbon material is obtained. S4: The
pyrolytic carbon material is washed with water until neutral, dried, and ground into
powder. S5: The
powder is placed in a container and evacuated.
Fluorine-containing gas is introduced, maintaining a pressure of 0.3-0.7 MPa, and reacted at 280℃-360℃ for 12-72 hours. After the reaction, the temperature is lowered to
room temperature to obtain a high
fluorine-to-carbon ratio fluorinated carbon material. This invention uses tea stems as
raw material and utilizes a high-pressure, low-temperature fluorination process to obtain a high fluorine-to-carbon ratio fluorinated carbon material with a fluorine-to-carbon ratio ≥1.0.