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51results about How to "Synthetic even" patented technology

Process for producing lithium ion battery anode material ferrtilithium phosphate

A method for preparing lithium iron orthophosphate being used as material of lithium cell positive electrode includes mixing iron orthophosphate with lithium phosphate and cane sugar according to designed ratio , grinding mixture by dry method in grinder for 12 ¿C 36 hours , putting ground power into heat ¿C treatment oven for carbonization , forming plate by pressing , placing plate in container and placing container into microwave oven for synthesizing reaction , grinding reacted matter to be powder being able to pass through 400 micron screen for being used as final product .
Owner:GUIZHOU NEW MATERIAL MINING DEV

Reservoir forming and developing simulated experiment system and method for submarine natural gas hydrate

The invention relates to a reservoir forming and developing simulated experiment system and method for submarine natural gas hydrate. The reservoir forming and developing simulated experiment system and method for submarine natural gas hydrate consists of a fluid injection part, a hydrate synthesis/decomposition part and a withdrawal fluid metering part, wherein the fluid injection part comprisesa high-pressure displacement pump, a natural gas cylinder, a middle container and a seawater storage tank; the hydrate synthesis/decomposition part comprises a high-low-temperature test box, a high-pressure reaction kettle, a simulating straight well pipeline, a simulating horizontal well pipeline, a temperature sensor, a pressure sensor and a computer, wherein the high-pressure reaction kettle ispositioned in the high-low-temperature test box; fluid injection and withdrawal interfaces are uniformly distributed in the end cover and the wall surfaces of a kettle body; the pressure sensor and the temperature sensor are connected to the computer through guide-out wires; and the withdrawal fluid metering part comprises a back-pressure valve, a gas-liquid separator, a measuring barrel and a gas meter. The system can be utilized to perform experiments such as submarine natural gas hydrate synthesis simulation or submarine natural gas hydrate exploitation, is simple and convenient in operation, and can provide important support for submarine natural gas hydrate reservoir development technical evaluation and establishment.
Owner:SOUTHWEST PETROLEUM UNIV

Preparation method for aluminum-doped zinc oxide (AZO) nano array

The invention provides a preparation method for an aluminum-doped zinc oxide (AZO) nano array. The method is performed as follows: precisely controlling the concentration of chemical reaction solution by continuously injecting growing sources and doping sources at a constant speed to controllably prepare an aluminum-doped zinc oxide (AZO) array with high carrier concentration; compounding the aluminum-doped zinc oxide (AZO) array and a nickel oxide material to obtain a capacitor electrode material with high electricity capacity. The capacitor electrode material with high electricity capacity is attained in such a way that an aluminum-doped zinc oxide (AZO) array with high conductivity prepared by a continuous flow injecting method and a nickelnanosheet material with poor conductivity but high electricity capacity are combined. In comparison to a conventional hydrothermal method, the carrier concentration obtained from the preparation method provided in the invention increases three orders of magnitude. In the method, an aluminum-doped zinc oxide (AZO) material with high carrier concentration and a nickel oxide with poor conductivity are combined such that the advantages of the two materials are brought into full play and the electricity capacity of a capacitor is substantially increased. Beyond that, the continuous flow injecting and doping method provides a new idea for controllable precise doping. The method is simple in operation, cost-effective and enjoys great application prospects.
Owner:UNIV OF SCI & TECH BEIJING

Double-layer temperature control system for hydrate sediment long core composition and decomposition

ActiveCN103105876ASynthetic evenSolve the difficulty of synthesisTemperatue controlTemperature controlDecomposition
The invention discloses a double-layer temperature control system for hydrate sediment long core composition and decomposition. The double-layer temperature control system for hydrate sediment long core composition and decomposition comprises a pressure chamber and a cooling system, a spacer layer is arranged inside the pressure chamber, a sediment layer and a composition temperature control layer are arranged inside the pressure chamber, an inlet end and an outlet end are respectively arranged on two sides of the sediment layer, the composition temperature control layer is placed outside the sediment layer and is tightly contacted with the sediment layer, and the composition temperature control layer comprises an inner temperature control layer and an outer temperature control layer. The cooling system comprises a first cooling system and a second cooling system, wherein the first cooling system is connected with the inner temperature control layer, the second cooling system is connected with the outer temperature control, the flow direction of cooling liquid in the inner temperature control layer is opposite to the flow direction of air in the sediment layer, and the flow direction of cooling liquid in the outer temperature control layer is the same with the flow direction of air in the sediment layer. According to the double-layer temperature control system for hydrate sediment long core composition and decomposition, the hydrate sediment long core can be fast and evenly composited in composition process, and constant environment temperature is provided for decomposition.
Owner:北京中科力森科技有限公司

Ratio type quantum dot ECL aptamer sensor and manufacturing method thereof

The invention belongs to the technical field of new materials and analysis sensing, and particularly relates to a ratio type quantum dot ECL aptamer sensor and a manufacturing method thereof, the ratio type quantum dot ECL aptamer sensor comprises a cathode electrode and an anode electrode, the ratio type quantum dot ECL aptamer sensor is characterized in that: the cathode electrode is cadmium selenide quantum dots, and the anode electrode is modified ruthenium silicon particles (RuSi@Ru(bpy)32+); the constructed ratio type electrochemiluminescence aptamer sensor is applied to the detection ofthe antibiotic kanamycin, and has certain practical significance; ECL signals are generated by ruthenium-silicon particles and a co-reactant n-propylamine at an anode, and ECL signals are generated by cadmium selenide quantum dots and a co-reactant potassium persulfate at a cathode, so that a ratio type ECL sensor is designed, false negative existing in an experiment is eliminated, experimental data is more reliable, the selectivity of the sensor can be greatly improved by introducing an aptamer, and the sensitivity of the sensor is improved. The sensor can be applied to biological analysis or ion detection, and the designed sensor is applied to antibiotic detection of environmental analysis pollutants.
Owner:安徽理工大学环境友好材料与职业健康研究院(芜湖) +1

Method for preparing high-purity cadmium telluride

The invention discloses a method for preparing high-purity cadmium telluride. The reaction process is carried out in a closed quartz tube with melting point above cadmium and tellurium and after carbon coating treatment, wherein the mass ratio of a 5N cadmium material to a 5N tellurium material is 1: 1.1-1.15. The method comprises the following steps: dividing the weighed tellurium material into N parts according to the charging times N, dividing the weighed cadmium material into N-1 parts, alternately adding each part of tellurium material and each part of cadmium material into the quartz tube and adding the tellurium material into the quartz tube firstly and lastly, removing oxygen after charging, sintering and sealing the tube by using a sealed bulb, and slowly performing high-temperature and high-pressure synthetic reaction. The method has the advantages that the contact area of the raw materials is larger in a molten state, the reaction speed is more sufficient compared with the solid raw material, the micro-sized crushing treatment for the raw materials is avoided, the shape requirement of the raw materials is relaxed, the preparation cost is greatly reduced, the purity of the raw material is ensured, the method is suitable for large-scale production, the synthetic conversion rate of the cadmium telluride can reach 98 to 99.5 percent, and the single-tube yield of 800 to 1,000 grams can be ensured by using the quartz tube with the inside diameter of 32 millimeters under the premise of safety.
Owner:中国东方电气集团有限公司

Aluminum antimonide polycrystalline material synthesizing process device and synthesis method

The invention relates to an aluminum antimonide polycrystalline material synthesizing process device and a synthesis method. High-purity antimony and high-purity aluminum are put into a silicon nitride ceramic crucible, a graphite gasket is covered and nested in a quartz crucible, an air gap exists between the graphite gasket and the upper surface of the silicon nitride ceramic crucible, and highvacuum in the silicon nitride ceramic crucible is not influenced during vacuumizing; after vacuumizing, a quartz plug and the quartz crucible are welded, and finally the quartz plug and the quartz crucible are synthesized in an inclinable rotating tubular furnace in a rotating mode, so that synthesis of single-phase aluminum antimonide in a small-cavity crucible without additional compensation isachieved, and elements are not lost in the synthesis process. According to the process device, the silicon nitride ceramic crucible does not react with an aluminum antimonide melt at high temperature,antimony evaporation is inhibited, the effect of cracking of the reaction that the outer quartz crucible adsorbs the aluminum element is prevented, it is guaranteed that melt components are not lostin the synthesis process, and the graphite gasket has the effect of adsorbing residual oxygen at high temperature. The synthesized aluminum antimonide polycrystalline material has the characteristic of uniform single-phase components.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Nanometer flaky MFI molecular sieve and preparation method thereof

The invention provides a nanosheet-shaped MFI molecular sieve and a preparation method thereof, and relates to the technical field of molecular sieves. The preparation method comprises the following steps: mixing a silicon source, tetrapropylammonium hydroxide and water, carrying out microwave heat treatment, and dialyzing and purifying to obtain an MFI crystallite solution; and carrying out hydrothermal treatment on the MFI crystallite solution to obtain the nanosheet-shaped MFI molecular sieve. The microwave heating assisted synthesis method has the advantages of fast reaction and uniform heating, and can efficiently synthesize the MFI zeolite crystallite with a uniform structure; the MFI crystallite molecular sieve with high purity and uniform structure is obtained through dialysis and purification, the MFI crystallite molecular sieve is used as a raw material to facilitate the generation of the nanosheet-shaped MFI molecular sieve with stable morphology, and the nanosheet-shaped MFI molecular sieve with uniform particle size, high purity and uniform structure is obtained. Moreover, the preparation method provided by the invention is simple to operate and simple in process, and the nanosheet zeolite material with the size required by practical application can be efficiently customized.
Owner:FUDAN UNIV

Marine Gas Hydrate Accumulation-Development Simulation Experiment System and Method

The invention relates to a marine natural gas hydrate accumulation-development simulation experiment system, which consists of a fluid injection part, a hydrate synthesis / decomposition part and a produced fluid metering part, and the fluid injection part includes a high-pressure displacement pump, a natural gas bottle, an intermediate container and seawater Storage tank; Hydrate synthesis / decomposition part includes high and low temperature test chamber, high pressure reactor, simulated vertical well pipeline, simulated horizontal well pipeline, temperature sensor, pressure sensor, computer, high pressure reactor is located in the high and low temperature test chamber, at the end of the kettle body The lid and the wall are arranged with fluid injection and extraction interfaces, and the pressure sensor and temperature sensor are connected to the computer through lead wires; the produced fluid metering part includes a back pressure valve, a gas-liquid separator, a graduated cylinder, and a gas meter. The system can be used for experiments such as synthesis simulation of marine gas hydrate reservoirs or exploitation of marine gas hydrates. The invention is easy to operate, and can provide important support for the evaluation and establishment of marine natural gas hydrate reservoir development technology.
Owner:SOUTHWEST PETROLEUM UNIV
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