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218 results about "Acidum Nicotinicum" patented technology

Acidum Nicotinicum. Acidum Nicotinicum may be available in the countries listed below. Ingredient matches for Acidum Nicotinicum Nicotinic Acid. Nicotinic Acid is reported as an ingredient of Acidum Nicotinicum in the following countries:. Hungary

Photosynthetic bacterium with high yield nano-selenium and preparation method of nano-selenium living bacterium preparation thereof

The invention discloses a photosynthetic bacterium with high yield nano-selenium and a preparation method of a nano-selenium living bacterium preparation thereof. The invention particularly disclosesthiocapsa roseopersicina capable of tolerating high-concentration (25g/L) sodium selenite. Nicotinic acid is creatively used for modifying high-concentration biological nano-selenium, so that the storage stability of the nano-selenium in the liquid is greatly improved. Meanwhile, the conversion rate of the nano-selenium is over 90 and thus nano-selenium fermentation liquid can be not subjected tocentrifugal purification, so that a liquid nano-selenium preparation which is relatively high in nano-selenium content, contains viable bacteria and is long in preservation time can be directly obtained. Problems that high-concentration biological nano-selenium prepared by the microorganisms in the prior art can not be stored in a liquid mode and easy transformation to black elemental selenium occurs frequently are solved and defects of high energy consumption and serious pollution are overcome. The nano-selenium living bacterium preparation has advantages of simple production process, low cost, low equipment requirement, no emission of three wastes, and environmental friendliness has the great market popularization value.
Owner:FOSHAN YANHUI BIOTECH CO LTD

Preparation method of 4-trifluoromethyl nicotinic acid

The invention relates to a synthetic method of 4-trifluoromethyl nicotinic acid. The method is characterized by comprising the following steps: (1) in a solvent A, enabling methyl acrylate to react for 30-60 minutes at 25-90 DEG C under the action of a catalyst and an oxidizing agent, with the molar ratio of methyl acrylate to the catalyst to the oxidizing agent being 1:(0.01-0.05):(1-1.5), so asto prepare methyl 3-oxopropionate; (2) in a solvent B, controlling the mole ratio of the methyl 3-oxopropionate to 4-amino-1,1,1-trifluoro-3-buten-2-one to be (1-1.5):1, reacting at 25-90 DEG C for 30-60 min to prepare N-(2-methoxycarbonyl vinyl)-4,4,4-trifluoro-3-one-1-butenylamine, then adding an alkali, with the mole ratio of the N-(2-methoxycarbonyl vinyl)-4,4,4-trifluoro-3-one-1-butenylamineto the alkali being 1:1-5, performing ring closing hydrolysis at 25-90 DEG C under the action of the alkali for 30-60 min, subjecting the reaction product to rectification separation after the reaction is finished to obtain a 4-trifluoromethyl nicotinic acid finished product. The method has the advantages that the adopted raw materials are cheap and easy to obtain, the synthesis method is simple to operate, reaction conditions are mild, requirements on equipment are low, and the method is suitable for industrial large-scale production.
Owner:ANHUI JINGHE IND

Gas-phase SO3 sulfonation process and production system

The invention belongs to the technical field of fine chemical engineering. The invention aims to provide a gas-phase SO3 sulfonation process and a production system thereof. The sulfonation system basically has no exhaust emission and good environmental effect, and meanwhile, dangerous solid wastes such as electrostatic acid and the like are not generated any more. According to a technical schemein the invention, the gas-phase SO3 sulfonation process comprises the following steps: 1) mixing tail gas having undergone gas-liquid separation after sulfonation with a certain flow of oxygen, conveying the obtained mixture into a sulfur burning furnace from a gas-phase inlet of the sulfur burning furnace through a Roots blower, and enabling liquid sulfur to enter the sulfur burning furnace froma liquid sulfur inlet of the sulfur burning furnace, and carrying out contact combustion in the sulfur burning furnace to generate SO2 gas; 2) subjecting the SO2 gas to conversion by a conversion tower, cooling by a cooler and filtering by an SO3 filter to remove a trace amount of nicotinic acid so as to obtain SO3 gas, and allowing the SO3 gas to enter a sulfonator and to contact with an organicmaterial input into the sulfonator from another inlet for a sulfonation reaction; and 3) subjecting a sulfonation product to gas-liquid separation, and recycling a gas phase to the step 1).
Owner:ZANYU TECH GRP CO LTD +1

Production device and production process of EL-grade sulfuric acid

The invention relates to a production device of EL-grade sulfuric acid. The production device comprises a first condenser, a second condenser, a first gasifier and a second gasifier which are connected in sequence. The first condenser is communicated with a falling film evaporator in the nicotinic acid evaporation process and is used for receiving evaporated sulfur trioxide gas; the second gasifier is connected with an EL-grade sulfuric acid absorption tower, the EL-grade sulfuric acid absorption tower is tower-tank integrated equipment and comprises an absorption tower body and an acid tank,the acid tank is connected with a circulating acid cooler through a circulating acid pump, and the outlet of the circulating acid cooler is divided into three paths which are respectively communicatedwith the acid tank, the absorption tower body and a diluter; the diluter is communicated with the water treatment device and is used for receiving high-purity water; the diluter is communicated withthe finished product acid cooler and is used for cooling to prepare finished product acid. The production device has the advantages of low energy consumption and no pollution. The invention also provides a production process of EL-grade sulfuric acid.
Owner:上海六谦工程科技股份有限公司

Synthetic medium for Staphylococcus carnosus, and preparation method and application of Staphylococcus carnosus fermentation broth

The invention discloses a synthetic medium for Staphylococcus carnosus, and a preparation method and application of Staphylococcus carnosus fermentation broth. The synthetic medium for Staphylococcus carnosus comprises the following raw materials by weight: on the basis of a volume of 1 L, 10 to 50 g of anhydrous glucose, 0.1 to 1.5 g of lysine, 1.0 to 5.0 g of valine, 0.1 to 1.5 g of glycine, 1.0 to 5.0 g of arginine, 1.0 to 5.0 g of proline, 5 to 10.0 g of glutamic acid, 0.1 to 0.5 g of tryptophan, 0.1 to 1.5 g if cystine, 1.0 to 3.0 mg of thiamine hydrochloride, 1.0 to 3.0 mg of calcium pantothenate, 1.0 to 3.0 mg of nicotinic acid, 1.0 to 3.0 mg of manganese sulfate, 0.1 to 1.0 g of potassium dihydrogen phosphate, 0.1 to 0.8 g of magnesium sulfate heptahydrate, 0.005 to 0.010 g of ferrous sulfate heptahydrate, 1.0 to 5.0 g of dipotassium hydrogen phosphate trihydrate and 6 to 10 g of 3-(N-morpholino)propanesulfonic acid, with the balance being water. The invention also discloses a preparation method for the Staphylococcus aureus fermentation broth. The synthetic medium for Staphylococcus carnosus is reasonable in composition, rich in nutrients and capable of meeting the growth demands of Staphylococcus carnosus. The growth amount of Staphylococcus carnosus obtained through the synthetic medium provided by the invention is increased by 5% compared with the growth amount of Staphylococcus carnosus obtained through frequently used LB (Luria-Bertani) mediums.
Owner:TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY

Method for detecting vitamins in formula food for special medical purposes

The invention discloses a method for detecting vitamins in formula food for special medical purposes, and relates to the technical field of vitamin detection, and the method comprises the following steps: preparing standard solutions: preparing 1 mg/mL of vitamin B6 standard stock solution, 1 mg/mL of vitamin B1 standard stock solution, 1 mg/mL of vitamin B2 standard stock solution, 1 mg/mL of nicotinic acid nicotinamide standard stock solution, and leaf standard stock solution; preparing mixed standard work solutions: accurately sucking the standard stock solutions, and fixing the volumes bya mobile phase so as to obtain a series of curve solutions, wherein the concentrations of the curve solutions are 1 microgram/mL, 2 micrograms/mL, 5 micrograms/mL, 10 micrograms/mL and 20 micrograms/mL respectively; preparing a sample: firstly preparing a sample solution, and then preparing a to-be-detected solution by using the sample solution; and analyzing the result: injecting the sample solution into a high performance liquid chromatograph to obtain the corresponding peak area of each component, and obtaining the concentration of each vitamin component in the to-be-tested sample solutionaccording to a standard curve, wherein the content of each vitamin component in the sample is calculated according to the following formula: Xi=([rho]*V)/m*100/1000.
Owner:特康药业集团有限公司

Method for preparing manganese nicotinate and application of manganese nicotinate to animal feed

The invention discloses a method for preparing manganese nicotinate. The method includes steps of adding nicotinic acid into water; adding manganese sources into the water and carrying out stirring reaction; carrying out cooling after the reaction is sufficiently completely carried out; separating solid from liquid; washing and drying obtained solid products to obtain the manganese nicotinate. ThepH (potential of hydrogen) values of reaction systems are controlled in whole procedures during stirring reaction, so that the reaction systems are weakly acidic. The invention further discloses application of the manganese nicotinate to animal feed. The method and the application have the advantages that the method is simple, is short in reaction time, low in cost and high in production efficiency and only has low requirements on equipment, the manganese nicotinate which is a product prepared by the aid of the method is high in yield and purity, the yield can reach 95% at least on the basisof manganese, and the purity of the product can reach 98% at least; excellent growth promoting effects can be realized for poultry animals when the manganese nicotinate is used in poultry feed, and the quality of carcasses can be improved; the reproductive performance of reproductive sow can be particularly greatly improved when the manganese nicotinate is used in pig feed; effects of obviously improving the growth performance and reducing the death rates can be realized when the manganese nicotinate is used in aquatic feed; effects of increasing the milk quantities of ruminant animals and reducing the mastitis incidence can be realized when the manganese nicotinate is used in ruminant feed.
Owner:XINGJIA BIO ENG CO LTD
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