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122 results about "O methylglucose" patented technology

Facial mask with rhus chinensis leaf extract and method for preparing facial mask

The invention provides a facial mask with rhus chinensis leaf extract and a method for preparing the facial mask. The facial mask comprises facial mask base cloth and facial mask essence. The facial mask essence comprises allantoin, methylparaben, EDTA (ethylene diamine tetraacetic acid) disodium, glycerin, betaine, xanthan gum, polyacrylate cross-linked polymers-6, methyl glucitol polyether-10, panthenol, PEG-40 (polyethylene glycol-40) hydrogenated castor oil, beta-glucan, ceramide 3, chitosan oligosaccharide, hyaluronic acid, caprylyl hydroximic acid, polypeptides, the rhus chinensis leaf extract and water. The method for preparing the facial mask includes steps of 1), preparing the rhus chinensis leaf extract by the aid of steps of repeated extraction, micro-filtration and ultra-filtration, reduced-pressure distillation and concentration, spray drying and the like; 2), preparing the facial mask with the rhus chinensis leaf extract. The facial mask and the method have the advantages that a main active component of the facial mask is the natural plant extract, and accordingly obvious tightening, anti-wrinkle, moisturizing and skin whitening effects can be realized by the facial mask; raw materials for the facial mask can come from wide sources, and the method is simple.
Owner:张家界久瑞健康产业发展有限公司

Composite microbial multi-element film coating synergistic fertilizer and preparation method thereof

The invention discloses composite microbial multi-element film coating synergistic fertilizer and a preparation method thereof. The composite microbial multi-element film coating synergistic fertilizer is prepared from the following raw materials in parts by weight: 100 parts of particle fertilizer cores, 2 to 3 parts of film coating agents and 1 to 3 parts of composite microbial bacterial agents.The particle fertilizer cores are prepare from urea, ammonium sulphate, monoammonium phosphate, triple superphosphate, potassium chloride, monopotassium phosphate, ammonium molybdate, magnesium sulfate, fermentation fertilizer, bentonite, gamma-polyglutamic acid/chitooligosaccharide hydrogel; the film coating agents are prepared from urea, formaldehyde, alpha-methyl glucoside and diethylenetriamine pentaacetic acid; the composite microbial bacterial agents are prepared from bacillus subtilis, bacillus lateraporus and trichoderma viride. The composite microbial multi-element film coating synergistic fertilizer has the excellent performance that the nutrition is comprehensive; the fertilizer effect is good; the soil microenvironment is obviously improved; the soil quality is improved; the hardened soil is loosened. The fertilizer belongs to the fertilizer meeting the requirements of fertilizer reduction, effect enhancement and green and environmentally friendly effects.
Owner:河北百禾丰化肥有限公司

Preparation method of polyether polyol cross-coupling agent

The invention relates to a preparation method of a polyether polyol cross-coupling agent, which is mainly used for solving the problems that the reaction procedure of preparing the polyether polyol is complicated, post treatment is necessary for removing metal ions after a polymerization reaction and the prepared polyether polyol has low activity and poor mechanical property and size stability when used for preparing polyurethane foam plastics. The polyether polyol cross-coupling agent is prepared by using urea and polyol as a co-initializing agent and epoxypropane as a polymerization monomer through carrying out catalytic reaction on reaction raw materials and a catalyst under the conditions that the mol ratio of the urea to the polyol to the epoxypropane is (1-20):1:(1-40), the reaction temperature is 60-180 DEG C and the reaction pressure is less than 0.6MPa, wherein the polyol is selected from at least one of cane sugar, sorbierite, alpha-methyl glucoside or mannitol, the catalyst is selected from at least one of trimethylamine, dimethylamine, triethylamine, dimethylethanolamine, dimethylisopropanolamine or N,N'-dimethyl-1,3-propanediamine, and the consumption of the catalyst accounts for 0.1-5 percent by weight of the raw materials. The technical scheme provided by the invention better solves the problems and can be used in the industrial production of the polyether polyol cross-coupling agent.
Owner:CHINA PETROCHEMICAL CORP

Method for continuously synthesizing benzyl-substituted glucolactone by adopting microchannel reaction device

ActiveCN112961135ADoes not reduce consumptionReduce consumptionOrganic chemistryGluconic acidBenzyl chloride
The invention discloses a method for continuously synthesizing benzyl-substituted glucolactone by adopting a microchannel reaction device. The method comprises the following steps: taking methyl-alpha-D-mannopyranoside as an initial raw material, preparing the methyl-alpha-D-mannopyranoside into an old organic solvent solution, and reacting the old organic solvent solution with an organic solvent solution of benzyl chloride in a first microreactor to generate methyl glucose with hydroxyl protected by benzyl; reacting a homogeneous solution formed by mixing a reaction solution of benzyl-substituted gluconic acid and a small amount of hydrochloric acid solution in a second microreactor for demethylation to generate hydroxyl benzyl-substituted glucose; and finally, reacting the reaction solution with an aqueous solution of hydrogen peroxide and sodium hydroxide and an organic solvent solution of tetramethylpiperidine nitrogen oxide in a third microreactor to generate the high-purity hypoglycemic drug Dapagliflozin intermediate benzyl substituted glucolactone. The method disclosed by the invention is higher in heat and mass transfer efficiency and easier to industrially amplify, the initial materials are simple, cheap and easily available, the process is simple, the obtained intermediate is high in purity and high in yield, the production cost can be effectively reduced, and the method is suitable for industrial production.
Owner:安庆奇创药业有限公司

Preparation method of composite sandwiched biomass foam partition wall material

InactiveCN105462163AHigh reactivityAccelerate the liquefaction conversion rateLayered product treatmentLaminationPolyethylene glycolPhosphoric acid
The invention discloses a preparation method of a composite sandwiched biomass foam partition wall material. The method comprises the technological steps of preparing a sandwiched biomass foam material, and gluing the sandwiched biomass foam material and a panel. A multiphase composite liquefying agent containing phenol, polyethylene glycol and cyclic carbonates and a mixed catalyst containing concentrated sulfuric acid and phosphoric acid are adopted, so that not only is the liquefying conversion rate increased, but also flame-retardant phosphorus-containing groups are introduced; in the resinification process, solid paraformaldehyde is used for substituting a formaldehyde solution, and methyl glucoside is added to form a multi-phase tool system, so that the reaction activity is further improved, the release amount of formaldehyde is reduced, the flexibility of resin is further improved, the hard brittleness and scaling-off defects of the foam material are improved, and the solid content of the resin is also enabled to reach 75 percent or more suitable for foaming; and in the foaming process, methyl benzenesulfonic acid is selected to be compounded with N-hydroxymethyl acrylamide, so that not only can the curing efficiency be increased, but also the flame-retardant effect can be improved.
Owner:NANJING FORESTRY UNIV

Metal surface coating process

The invention relates to the technical field of metal surface treatment, and particularly discloses a metal surface coating process. The metal surface coating process specifically comprises the following steps: (1) polishing treatment: polishing the surface of a metal workpiece through sand blasting and shot blasting; (2) etching treatment: carrying out etching treatment on the surface of the metal workpiece through an etching solution, wherein the etching solution is prepared from the following components in parts by weight: 5 to 10 parts of a sulfuric acid solution, 0.1 to 0.3 part of benzotriazole, 0.3 to 0.5 part of methyl glucose polyoxyethylene ether and 0.3 to 0.5 part of a surfactant; (3) silane treatment: adopting silane treatment liquid for conducting silane spraying conversion on the surface of the metal workpiece; (4) drying: drying the metal workpiece subjected to silane conversion; and (5) coating: conducting primer coating and finish coating on the surface of the dried metal workpiece. According to the metal surface coating process provided by the invention, the surface of the workpiece is subjected to etching treatment before silane treatment, so that a uniform rough surface is formed, the binding force of subsequent film layers is greatly improved, and the overall adhesive force and the overall compactness of the coated film layers are improved.
Owner:上海阿尔斯通交通电气有限公司
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