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162results about How to "Many gaps" patented technology

Preparation method for gamma-AlON transparent ceramic powder

The invention relates to a method for preparing pure-phase gamma-AlON transparent ceramic powder by carbothermal reduction of gamma-Al2O3, and belongs to the field of preparation of transparent ceramic materials. According to the preparation method, nano-alpha-Al2O3 and activated carbon are taken as raw materials; powder is filled in a graphite crucible loosely, wherein an aluminum oxide plate is paved at the bottom of the graphite crucible; an air hole which penetrates through the powder is preformed at the aluminum oxide plate; a graphite cover provided with fine and dense air holes is used for covering the hole; the pure-phase gamma-AlON transparent ceramic powder is prepared by adopting a two-step heating process in a flowing nitrogen environment with a micro positive pressure. By the adoption of the preparation method, the vacuumizing difficulty can be effectively reduced, powder is prevented from scattering in a vacuumizing stage, the time required for discharging adsorbed gas can be greatly shortened, the vacuumizing speed is high, and the preparation efficiency of the gamma-AlON powder is greatly improved; the obtained gamma-AlON powder phase has stable and reliable compositions and can be used for pressure-less sintering preparation of AlON transparent ceramics with high transmittance; the process is simple and is easy to operate, and is suitable for industrial production.
Owner:DALIAN MARITIME UNIVERSITY

Electric core used for secondary lithium battery and preparation

The invention relates to an electric core of a secondary lithium battery and a preparation method thereof. The preparation method comprises the following steps: electrode mixed materials which are used in the secondary lithium battery are prepared, and the electrode mixed materials comprise the following materials by weight percentages: a. 30-97.9% of anode/cathode active materials; b. 1-40% of a solvent; c. 1-10% of a binding agent; and d. the rest of conductive additive; and the materials are mixed evenly; a produced current collector needed by the anode/cathode and the electrode combined materials of the anode/cathode are put in a mould, the electrode combined materials are evenly pressed on a surface of the anode/cathode current collector, or evenly pressed on two surfaces of the anode/cathode current collector, or evenly pressed on the periphery of the anode/cathode current collector by an extrusion process, and the electrode of the secondary lithium battery having an inner lining or simultaneously having an inner lining and an outer lining is obtained by heating and drying treatment. The method provides electrode shapes required by batteries with various shapes, and the thickness and the density of a pole piece can be made according to the design by a compaction process, therefore the energy density of the battery is improved.
Owner:董兴国

Preparation method of porous graphene and applications of finished product thereof

The invention relates to a preparation method of porous graphene and applications of finished product thereof. The preparation method comprises following steps: (1) ultrasonically dispersing graphene oxide in deionized water; (2) dissolving a certain amount of water-soluble transition metal salts in deionized water, dropwise adding the solution into the graphene oxide solution, and stirring at the same time; (3) subjecting the mixed solution to treatments of centrifugation and washing to extract products, drying the products for 1 to 20 hours; (4) putting the obtained materials into a tube-type furnace, heating, burning the materials at a constant temperature of 500 to 1050 DEG C for 1 to 20 hours, while controlling the flow speed of inert gas in the range of 10 to 300 mL/min, cooling, and collecting the solid products; (5) processing the solid products with dilute hydrochloric acid to remove the transition metal oxides in the solid products so as to obtain the porous graphene material. The porous graphene material prepared by the method has the advantages of few layers and controllable hole size, and solves the problems of non-conductivity of electrons in the vertical direction to the horizontal surface of the graphite material multi-layer graphene and obstructed route of Li. Furthermore, the construction of nano micro-hole structure is beneficial for storage, diffusion, and transportation of charges.
Owner:上海一广新能源科技有限公司

Closed mesoporous silicon oxide and preparation method of same

The invention discloses closed mesoporous silicon oxide and a preparation method of same. The preparation method comprises the steps of treating dry mesoporous silicon oxide with polychlorinated silane to prepare mesoporous silicon oxide containing chlorine groups on the surface; reacting the mesoporous silicon oxide containing the chlorine groups on the surface with polyhedral silsesquioxanes and polychlorinated silane to obtain a crude product; and after washing and drying, conducting calcination at the temperature of 230-300 DEG C, thereby obtaining the closed mesoporous silicon oxide. A coating layer is formed at the outer surface and the mesopores of the mesoporous silicon oxide by polyhedron silsesquioxane and mutual connection is realized through a Si-O bond or Si-N bond. The inner pores of the mesoporous silicon oxide are kept; besides, the mesopores of the mesoporous silicon oxide are closed by polyhedron silsesquioxane, and a larger specific surface area and more pores are obtained, so that the dielectric constant of the materials is lowered and the adsorptive property of the mesoporous silicon oxide is improved and the method provided by the invention ensures that the advantages of the mesoporous silicon oxide in preparing materials with low dielectric constant are brought into full play.
Owner:SUZHOU UNIV

Graphene nano steam generation device and cosmetic instrument

The invention provides a graphene nano steam generation device and a cosmetic instrument. The steam generation device comprises a coarse steam channel and a nano steam channel, wherein the coarse steam channel is respectively connected with a coarse steam manufacturing device and the nano steam channel, a steam screening and filtering device is arranged in the coarse steam channel, and a first electrode and a second electrode are arranged in the tail end of the coarse steam channel. The steam generation device further comprises a high voltage power supply device, wherein the high voltage powersupply device is connected with the first electrode and the second electrode, the high voltage power supply device can load high voltage power on the first electrode and the second electrode and canform high voltage arc discharge between the two electrodes, flowing-through coarse steam molecular groups are broken by high voltage arc to generate a lot of active steam with the nano particle size,and the active steam flows out of the nano steam channel. The graphene nano steam generation device and the cosmetic instrument disclosed by the invention can continuously and stably manufacture a lotof nano steam and have the advantages of simple manufacturing technology, low manufacturing cost and convenience in large-scale industrial production.
Owner:HANGZHOU QINGKE ENERGY SAVING ENVIRONMENTAL PROTECTION TECH CO LTD

Preparation method for antibacterial melt-blown non-woven fabric

The invention relates to the technical field of non-woven fabrics, and provides a preparation method for an antibacterial melt-blown non-woven fabric. The preparation method comprises the following steps of (1) carrying out oxygen plasma treatment on a polypropylene non-woven fabric, and carrying out graft modification on the polypropylene non-woven fabric to prepare a modified polypropylene non-woven fabric; (2) polymerizing an amino-terminated hyperbranched polymer with propylene diamine and methyl methacrylate as raw materials, and preparing a modified hyperbranched polymer through polycondensation of carboxymethyl chitosan and the amino-terminated hyperbranched polymer; and (3) adding a copper chloride solution into a modified hyperbranched polymer aqueous solution, dropwise adding a sodium borohydride solution under nitrogen protection and ice bath conditions, carrying out impregnation treatment on the modified polypropylene non-woven fabric in the modified hyperbranched polymer aqueous solution after the reaction is finished, and drying to obtain the antibacterial melt-blown non-woven fabric. The preparation method solves a problem that the melt-blown non-woven fabric in theprior art only has an efficient filtering effect and does not have antibacterial property.
Owner:FUJIAN HENGAN HLDG CO LTD +2

Super absorbent dust-free wiping cloth and manufacturing method thereof

The invention discloses a super absorbent dust-free wiping cloth and a manufacturing method thereof. The wiping cloth is formed by interweaving warps and wefts and is characterized in that the dust-free wiping cloth is formed by circularly arranging square concave weave repeat units formed by interweaving the warps and the wefts along the warp direction and the weft direction respectively; at least one of the warp and the weft is formed by superfine fiber filaments; and in one weave repeat unit, the warps and the wefts are respectively arranged stepwise and upward in sequence from the central lowest point, and the floating length of the adjacent warps and the adjacent wefts on the steps increases in sequence to form concavo-convex patterns which are piled up alternately from low to high and have four high sides and low middle. The manufacturing method comprises the steps of beaming, drafting and reeding, weaving, weight reducing, tenter setting, laser cutting and packaging, thereby obtaining the super absorbent dust-free wiping cloth. The super absorbent dust-free wiping cloth has soft handfeel, good wiping effect and super absorbency and can be used in a dust-free room with a higher cleanliness requirement. The manufacturing method is simple and can be used for manufacturing the high-quality dust-free wiping cloth.
Owner:SHENZHEN SELEN SCI & TECH CO LTD

High-silicon porzite in gramineous plant structure biomorph and preparation method of high-silicon porzite in gramineous plant structure biomorph

The invention relates to a high-silicon porzite in gramineous plant structure biomorph and a preparation method of the high-silicon porzite in gramineous plant structure biomorph. According to the technical scheme, the preparation method comprises the following steps of impregnating for 3-24 hours under the condition of normal pressure or the pressure of 10<3>-10<4> Pa by taking 10%-70% by weight of a gramineous plant as a template and 30%-90wt% of aluminum sol as an impregnant, and uniformly stirring; baking the gramineous plant impregnated with the aluminum sol under the condition of 60-200 DEG C for 24-48 hours, and then preserving heat under the condition of 1100-1400 DEG C for 2-12 hours to obtain the high-silicon porzite in the gramineous plant structure biomorph. The preparation method disclosed by the invention is not only capable of integrally retaining the intrinsic structures of natural plants, but also capable of forming porzite nanoparticles on the surfaces of the hole walls of the natural plants, thereby thinning the hole structure and enhancing the frame strength, the high-temperature volume stability and the acid-proof and alkali-proof corrosivity; the porous morphological intrinsic structure has large specific area and has high potential in the fields of high-temperature insulation, catalyst carriers and the like.
Owner:WUHAN UNIV OF SCI & TECH

Composite and efficient oil-water-separation filter paper for hydraulic filter

The invention discloses composite and efficient oil-water-separation filter paper for a hydraulic filter. The composite and efficient oil-water-separation filter paper is prepared by, by weight, 50-55 parts of 3-5mm alkali-free superfine glass fiber, 55-60 parts of bleached softwood pulp, an appropriate amount of distilled water, 0.8-1 part of anionic polyacrylamide, an appropriate amount of concentrated sulfuric acid with the concentration being 98wt%, 10-12 parts of nano titanium dioxide, 20-25 parts of ferroferric oxide colloidal solution with the solid content being 30%, an appropriate amount of anhydrous ethanol, 60-65 parts of fluoro-silicon emulsion with the solid content being 40wt%, 1-1.2 parts of alkenyl succinic anhydride, 7-8 parts of sisal fiber, 3-4 parts of waste rubber powder, 0.9-1.1 parts of silane coupling agent kh550, 1.5-2 parts of organic silicon emulsion and 2-3 parts of urea. By the scientific and reasonable component proportion, the composite and efficient oil-water-separation filter paper is good in absorbability, good in hydrophobic and oleophylic performance and capable of efficiently separating oil and water. When the filter paper is applied to the hydraulic filter, hydraulic equipment can be well protected.
Owner:ANHUI PHOENIX INT CO LTD

Novel aluminum alloy anodic oxidation process

The invention discloses a novel aluminum alloy anodic oxidation process. The novel aluminum alloy anodic oxidation process comprises the following steps: (S01) mechanical polishing is performed; (S02)pretreatment: a polished aluminum alloy is put in circular flowing degreasing liquid for degreasing; (S03) cleaning: after degreasing is finished, water of 50-55 DEG C is used for spraying the surface of the aluminum alloy until no residue is on the surface; (S04) anodic oxidation: the cleaned aluminum alloy is immediately put in anodic oxidation liquid for anodic oxidation; (S05) coloring: the aluminum alloy treated in the step (S04) is cleaned until no residue is on the surface, and is dried; and screen printing of color paste is performed on an anodic oxidation film of the aluminum alloy;and (S06) the hole sealing treatment is performed by 10-12 min. The anodic oxidation process adopts a sulfuric acid anodic oxidation method; and through assistance by mated methods, the prepared anodic oxidation film of the aluminum alloy has natural fragrance to improve additional value. Further, the anodic oxidation film prepared by the anodic oxidation process is high in hardness, more in air gaps and high in absorption force, facilitates dyeing, and achieves higher corrosion resistance after closing treatment.
Owner:FOSHAN CITY GAOMING GAOSHENG ALUMINUM CO LTD

Preparation process of novel aluminum alloy anodic oxidation film

The invention discloses a preparation process of a novel aluminum alloy anodic oxidation film. The preparation process comprises the steps that S01, degreasing treatment is conducted; S02, chemical polishing treatment is conducted; S03, corrosive wash is conducted, specifically, an aluminum profile after being subjected to degreasing is placed in circularly flowing corrosive wash liquid for corrosive wash; S04, washing is conducted; S05, anodic oxidation treatment is conducted; S06, coloring is conducted, specifically, an aluminum alloy treated through the S04 step is washed until the surfacehas no residue, drying is conducted, and color paste is screen-printed on the anodic oxidation film of the aluminum alloy; and S07, hole sealing is conducted, specifically, the surface of the aluminumalloy is rinsed by using 50-55 DEG C of water, and hole sealing treatment is conducted in 100-102 DEG C of water steam. The preparation process of the novel aluminum alloy anodic oxidation film adopts a sulfuric acid anode oxidation method, supplemented with matched components and methods, the prepared aluminum alloy anodic oxidation film has natural fragrance, and added value of the aluminum alloy anodic oxidation film is promoted. Further, the anodic oxidation film prepared through the anodic oxidation process has high hardness, many gaps and high adsorption capability, is beneficial for dyeing, and has high corrosion resistance after being subjected to sealing treatment.
Owner:FOSHAN CITY GAOMING GAOSHENG ALUMINUM CO LTD

Preparation method of copper cobaltate porous microrod and nickel foam composite electrode material

The invention belongs to the field of preparation of inorganic nonmetallic materials, and particularly relates to a preparation method of a copper cobaltate porous microrod and nickel foam composite electrode material. The preparation method comprises the steps that clean nickel foam is soaked in an oxalic acid aqueous solution, and a mixed aqueous solution of soluble copper salt and soluble cobalt salt is dropwise added into the oxalic acid aqueous solution under the condition of stirring at room temperature; stirring reaction is conducted till micron-structure precursors grow out on the surface of the nickel foam, the nickel foam is taken out, cleaning, drying and calcining are sequentially conducted, and the copper cobaltate porous microrod and nickel foam composite electrode material is obtained. According to the preparation method of the copper cobaltate porous microrod and nickel foam composite electrode material, the technology is simple and easy to carry out, the product purity is high, the preparation cost is low, the diameter of a copper cobaltate microrod ranges from 0.5 micrometer to 2 micrometers, the length of the copper cobaltate microrod is about 5-10 micrometers, the size of a nano pore channel ranges from 10 nm to 50 nm, the uniformity and the dispersity of the product are both good, the copper cobaltate porous microrod and nickel foam composite electrode material can be directly applied to electrode materials of supercapacitors, the production technology is simple, and the preparation method is prone to be applied to practical large-scale production.
Owner:BOHAI UNIV
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