The invention provides a method for simply and stably preparing micro-nano hollow
copper, and belongs to method for preparing hollow
copper. The method includes the steps that firstly,
copper sulfate is dissolved in water and placed in a water bath kettle to be heated; secondly,
polyvinylpyrrolidone is added to the solution and stirred; thirdly, water is added to
sodium hydroxide, and a water solution of
sodium hydroxide is prepared, added to the solution in the second step and stirred; fourthly, a pre-mixed hydrazine
hydrate solution is added to the solution in the third step and stirred; fifthly, the water bath kettle is adjusted to the proper temperature, sepia Cu particles are generated,
solid-liquid two phases containing the Cu particles are centrifuged at a high speed, Cu
solid particles are acquired and washed multiple times with
anhydrous alcohol and deionized water in a cross mode, and other impurities generated in the reaction process are removed; sixthly, Cu
powder containing water or
alcohol is placed in a
vacuum drying oven to be dried, and then the high-purity Cu micro-nano particles can be acquired. The method has the advantages of being low in cost, simple in preparation process, high in purity, good in
repeatability and high in
surface chemical activity.