The invention discloses a preparation method of micro-nano holes in the surface of a
nickel-containing iron-
chromium alloy. The method comprises the following steps that firstly, the
alloy is pretreated to remove surface impurities; the surface of the
alloy is subjected to first-time
anodic oxidation treatment, the alloy serves as an
anode, a
graphite sheet serves as a
cathode, first-time
anodic oxidation is conducted, and then the alloy is cleaned with ethyl
alcohol and dried for use; and then, secondary
anodic oxidation treatment is conducted on the surface of the alloy subjected to primary anodic oxidation treatment, the alloy serves as an
anode, a
graphite flake serves as a
cathode, secondary anodic oxidation is conducted in a
sodium dihydrogen
phosphate dihydrate solution, then ethyl
alcohol is used for cleaning, and the flexible
alloy surface with obvious micro-nano holes is obtained after
drying. According to the method, the
alloy surface is subjected to flexible treatment by adopting a two-time anodic oxidation method, the universality of the anodic oxidation alloy is higher, micro-nano holes in the surface of the
nickel-iron-
chromium-containing alloy are ideally arranged through two-time anodic oxidation, and application of the
nickel-iron-
chromium-containing alloy in the fields of 3C,
electronics and the like is promoted.