134results about How to "Reduce the difficulty of process control" patented technology

The invention relates to a method and device for refinery sludge carbonization treatment and carbon recovery. The method comprises the following steps: pre-treatment: heating oil-containing sludge to 160-180 DEG C in an external heating manner while isolating air, and ensuring that the water content of the oil-containing sludge is controlled at 20% or below; carbonization: carbonizing the oil-containing sludge at 600-650 DEG C for 30-45 minutes, and recovering the solid residue generated by carbonization; condensation and oil-water separation: collecting gas-phase products generated by pre-treatment and carbonization, condensing in a water spray manner to obtain carbonization liquid and non-condensable gas, and performing oil-water separation on the carbonization liquid to obtain carbonization oil; utilization of combustible gas: performing combustion treatment on the non-condensable gas, enabling high temperature generated by combustion to provide heat energy for pre-treatment and carbonization, and performing purification treatment on the tail gas before discharging. The invention also provides a device for realizing the method. According to the invention, the advantages of high oil content recovery rate and stable and reliable process operation are achieved.

The invention discloses a titanium alloy and a preparing method thereof, the titanium alloy comprises chemical components in percent by weight: 33wt%-40wt% of Nb, 0.3wt%-0.5wt% of O and the balance of Ti; or the alloy comprises the components in percentage by weight: 33wt%-40wt% of Nb, 0.3wt%-0.5wt% of O, one or more of following element groups: 0-3wt% of V, 0-1wt% of Mo, 0-3wt% of Al, 0-3wt% of Sn and 0-4wt% of Zr and the balance of Ti. Components of the alloy in the invention are optimally designed, low-stacking fault energy large-sized ultra-fine grain/nanocrystalline titanium alloy can be obtained by smelting, thermal processing and cold processing, the titanium alloy has excellent match of strength and plasticity, the preparing method breaks through limitation of preparing of a titanium alloy nano-material in the prior art, processing control difficulty and manufacturing cost are reduced, the production efficiency is improved and the titanium alloy and preparing method have a broad application prospect.

The invention relates to a crystal material with a bigger size, which is manufactured by using a seed crystal induction vertical directional solidification casting method, in particular to a polycrystal or monocrystal material suitable for photoelectric application, such as silicon or silicon germanium. A traditional seed crystal used for casting a silicon crystal has a bigger size and higher consumption, thus, the invention provides a seed crystal with a smaller size and lower consumption, a method of casting a polycrystal or a monocrystal with the bigger size by using the seed crystal and the directional solidification method, the crystal material obtained by adopting the method, including a semiconductor crystal, and an application of the seed crystal in manufacturing semiconductor devices.

The invention discloses a method for improving phosphorus diffusion uniformity of a solar cell. The method comprises the following steps of: (1) placing a silicon slice in a diffusion furnace and raising the temperature of each region in the furnace to 700 to 780 DEG C, wherein the environment in the furnace is uniform nitrogen atmosphere, and the flow rate of the nitrogen gas is 8 to 30L/minute; (2) simultaneously introducing phosphorus-carrying source gas at the speed of 0.8 to 2L/minute and dry oxygen at the speed of 0.4 to 2.5L/minute after the temperature is stable, ensuring that the gas environment in the furnace is uniform, and diffusing for 10 to 40 minutes; (3) stopping introduction of the phosphorus-carrying source gas source and the dry oxygen, synchronously and uniformly raising the temperature of each region in the furnace at the rate of below 5 DEG C/minute, raising temperature to 810 to 900 DEG C and diffusing for 10 to 40 minutes; and (4) reducing temperature and discharging out of a boat. Through uniform gas and consistent temperature in the furnace, the phosphorus diffusion uniformity during preparation of the battery plate is improved, and the conversion efficiency of the solar cell is improved to a certain extent.

The invention generally relates to a vertical directional solidification casting method using seed crystal induction, which is used for manufacturing a crystal material with a reserved crystal orientation and comprises a polycrystal material and a monocrystal material. When a traditional method for casting the crystal by using the seed crystal induction is used for producing the crystal with a bigger size, the problems that the seed crystal consumption is high, a mixed crystal is easy to generate, the internal stress is high, the monocrystal material is hard to obtain or the expected quality requirement is hard to reach and the like exist. The problems are solved by the invention through providing a gradually-changed crystal growth area of which the horizontal cross section is gradually increased, thereby, a good crystal growth effect is obtained, and the obtained cast monocrystal or polycrystal material, such as silicon or silicon germanium, has fewer defects, high quality and a good performance, and is especially suitable for the application of the semiconductor field and the photovoltaic field.

The invention relates to a hot-rolled deep-punched pickled plate for automobile structures and a production method thereof. The hot-rolled deep-punched pickled plate for the automobile structures comprises the components in percentage by weight: 0.02-0.05% of C, not more than 0.05% of Si, 0.10-0.30% of Mn, 0.40-0.60% of Cr, 0.01-0.02% of Ti, not more than 0.15% of P, not more than 0.008% of S, 0.02-0.07% of Als, and the balance of Fe and inevitable impurities. The production method of the hot-rolled deep-punched pickled plate for the automobile structures comprises the step of: controlling the chemical components in the steel, the hot rolling process, the pickling process and other parameters to manufacture the hot-rolled deep-punched pickling plate for the automobile structures. The hot-rolled deep-punched pickled plate for the automobile structures has the characteristic of excellent deep punching performance; and the production method of the hot-rolled deep-punched pickled plate for the automobile structures has the advantages of low difficulty in process control, strong operability, simple method, low cost and the like.

The invention discloses a production method of a 440MPa-grade thin gauge hot-rolling pickling automobile sheet. The hot-rolling pickling automobile sheet is prepared from the chemical element components in percentage by weight: C is 0.07-0.09, Si is less than or equal to 0.05, Mn is 1.00-1.20, P is less than or equal to 0.020, S is less than or equal to 0.020, Nb is 0.010-0.020, Als is 0.030-0.050, Ti is 0.010-0.030, N is less than or equal to 0.008, and the balances are Fe and unavoidable impurities. The preparation method sequentially includes the following steps of liquid iron pre-desulfuration processing, converter steel-making, steel ladle LF refining, continuous casting, casting blank heating, rough rolling, finish rolling, laminar flow cooling, high temperature coiling, skin rolling, pickling, rinsing, oil coating and coiling. According to the production method, the measures of low temperature heating, the rough rolling, high pressure dephosphorization before the finish rolling,dephosphorization before the rough rolling and between the finish rolling passes, and corrosion inhibitor adding in the pickling are adopted, and the surface quality of a steel coil is improved; andthe reduction rate of the finish rolling, the finishing rolling temperature, coiling temperature precision control and high temperature coiling are adopted, stability of a steel coil general rolling technology is ensured, and the strip shape quality and the performance general volume stability of the steel coil are improved.

The invention discloses a preparation method of a single-crystal-morphology lithium ion battery positive electrode material. The preparation method comprises the following steps: (1) adding a metal salt solution and a sodium hydroxide solution into a reaction kettle, and carrying out a co-precipitation reaction to prepare precursor slurry; (2) mixing a precursor slurry with a lithium source and a doping agent by a wet method, and performing spray drying to obtain a precursor mixture; (3) performing primary sintering on the precursor mixture to obtain a primary sintering product; and (4) washing the primary sintering product with water, mixing the washed product with a coating agent, and carrying out secondary sintering to obtain the single-crystal-morphology lithium ion battery positive electrode material. In the preparation method, the precursor slurry is prepared by adopting an ammonia-free process, particles formed by stacking a plurality of fine particles are formed, the specific surface area of the precursor is very large and is greater than 100m < 2 >/g, and the precursor with an ultrahigh specific surface area is easier to form a single-crystal positive electrode material with uniformly dispersed primary particles after being sintered, so that development of the capacity is facilitated.

The invention provides a method for manufacturing a tantalum target material. The method comprises the following steps: firstly, carrying out hot forging on a tantalum ingot and then carrying out first annealing on the hot-forged tantalum ingot to form a first tantalum target material billet; rolling the first tantalum target material billet to form a second tantalum target material billet; and carrying out second annealing on the second tantalum target material billet to obtain the tantalum target material. The tantalum target material formed according to the technical scheme has fine internal grains and uniform internal microstructure and thus the defects such as delamination inside the tantalum target material are effectively avoided, the sputtering rate of the tantalum target material and the quality of the formed tantalum film in the subsequent use process are improved.

The invention discloses a method for manufacturing force responsive photonic crystal materials based on inverse compressing nano-forming technology. Electron beam lithography technology and reactive ion etch technology are employed. A nanometer magnitude pattern is etched on a rigid template to serve as a mother template according to preset photonic crystal structure parameters. An elastic polymer soft template with an inverse nanometer magnitude pattern can be made and serves as a secondary template. With highly elastic gel as filling material and visco-elastic polymer as moulding material, the pattern on the mother template is copied on to the visco-elastic polymer in a high fidelity way through inverse compressing, so as to produce nanometer magnitude and structure-controllable force responsive photonic crystal. Compared with the prior art, the method has the advantages of simple process, short flow, easily controlled technological parameters, repeatedly usable templates, high product precision level, stable and reliable product quality and low cost.

The invention provides a method for producing low alkali cement by using high alkali raw materials, which includes the steps of: putting the raw material limestone with alkali equivalent about 0.80% into a dry cement rotary kiln through a normal channel for putting the raw material into the kiln; adding chlorine-containing substances into the rotary kiln at the locations of a kiln head, a kiln head fuel burner, a flue chamber at kiln tail end, a pre-decomposition kiln or a pre-burning furnace; opening holes at the positions of the bottom part of the pre-decomposition kiln, an ascending flue channel, the flue chamber at kiln tail end or the tail grade cylinder of a pre-heater and inducting the chlorine-containing smoke gas enriched in the positions into a smoke dust collection system and collecting the smoke dust in the smoke gas. The smoke dust collection system comprises a mixing room. The method for producing low alkali cement by using high alkali raw materials uses the special property that alkali metal ions, chloride ions and sulfate ions mutually affect the melting point temperature under the high temperature coexistence condition, adds the chlorine-containing substances during the production process, and leads the chlorine in wastes to be reacted with the alkali in the raw materials by controlling the proportion between the alkali metal ions, chloride ions and sulfate ions entering the cement kiln, thereby achieving the double effects of reducing the alkali in the cement and processing high-chlorine wastes.

The invention discloses a refined processing method of apocynum venetum fiber. The refined processing method comprises steps as follows: wetting activation of apocynum venetum bast, beating into cakes and caging, directional catalytic oxidation, chemical degumming and postprocessing, wherein after the apocynum venetum bast is subjected to wetting activation with organic amine solvents, lignin, pectin and hemicellulose are subjected to the directional catalytic oxidation with a ferrite solution and an activator. A series of technological means including wetting activation processing, the directional catalytic oxidation and the like are organically combined, so that the refined processing method of the apocynum venetum fiber has the characteristics that the degumming effect is good, and a finished apocynum venetum fiber product is good in fineness, length, strength and other indexes, excellent in quality, good in spinnability and the like; besides, the consumption of chemicals during processing is low, the environmental protection pressure is low, and the technology is simple to control; the consumption of utilities such as water, electricity, gas and the like is low, the efficiency is high, and the refined processing method is applicable to industrial production.

A technique for automatically eliminating the self DC component of system in power metering features that a very simple and effective circuit structure is used to automatically elimitate the measuring error caused by input misadjustment, and in turn the false power caused by internet DC component (misadjustment). If the input signal has a DC component, it can be used to calculate active power.

The present invention discloses a preparation method of force responsiveness nanometer magnitude photonic crystal materials. Through adoption of the electron beam lithography technology and the reactive ion etch technology, a rigid template with a nanometer magnitude pattern is etched and taken as a filling template according to photonic crystal structure parameters designed in advance, high-elastic gel with good mechanical property is taken as matrix materials, and a visco-elastic polymer is taken as filling materials; and through the mode of the filling template, the photonic crystal pattern designed in advance in the high fidelity mode is transferred into the visco-elastic polymer, and the nanometer magnitude and structure controllable photonic crystal materials with force responsiveness are prepared through spin coating, stacking and the like. Compared to the current technology, the preparation method of force responsiveness nanometer magnitude photonic crystal materials is simple in technology and short in flow, technology parameters are easy to control, the template can be reused, the precision of products is high in level, the quality is stable and reliable, and the cost is low, etc.

The invention relates to a method for supplementing lithium to a negative pole piece. The method comprises the following specific steps: arranging a first calendering roll, a first composite roll, a second composite roll and a second calendering roll which are adjacently arranged in sequence, and coating silicon oil on roll surfaces of the first calendering roll, the first composite roll, the second composite roll and the second calendering roll; respectively unwinding two lithium strips to enter a gap between the first calendering roll and the first composite roll and a gap between the secondcalendering roll and the second composite roll, carrying out calendering to cause the lithium strips to be attached to the roll surfaces of the first composite roll and the second composite roll; unwinding the negative pole piece to enter a gap between the first composite roll and the second composite roll, and carrying out transfer printing on the lithium strip from the roll surfaces of the first composite roll and the second composite roll to the negative pole piece so as to obtain the lithium-supplemented negative pole piece. The method has the beneficial effects that base strips do not need to be adopted for protecting the lithium strips, so that the operation process of the traditional production process is greatly simplified, the process control difficulty is greatly reduced, the production cost is saved, and meanwhile the thickness accuracy of calendered lithium foils is improved.

The present invention relates to one kind chromatic dispersion compensating fiber with negative chromatic dispersion and negative chromatic dispersion slope in C band optical communication window. The fiber includes fiber core and cladding of SiO2, and features that its fiber core includes at least four layers, of which the first layer has positive relative refractive index difference, the middle layer has negative relative refractive index difference and the maximum difference between relative refractive index differences of the first layer and the middle layer not lower than 2.45 %. The present invention can obtain relatively high negative chromatic dispersion and negative chromatic dispersion slope, high RDS value and wide RDS range, low attenuation and low PMD value, and can meet various compensation requirement of G.655.

The invention provides a low-cadmium CIGS-based thin-film solar cell and a manufacturing method thereof. The thin-film solar cell sequentially comprises a substrate, a back electrode, a CIGS absorption layer, a CdS layer and an upper electrode from the bottom up. Cu atoms on the surface of the CIGS absorption layer are partially replaced by Cd atoms to form a surface modified layer. The thickness of the CdS layer ranges from 20nm to 35nm. The manufacturing method comprises the following steps of (a) depositing the back electrode on the substrate; (b) depositing the CIGS absorption layer on the back electrode; (c) depositing the CdS layer on the CIGS absorption layer; and (d) depositing the upper electrode on the surface of the CdS layer. In the step c, an operation for modifying the surface of the CIGS surface is performed before the CdS layer is deposited. While the overall high CIGS cell conversion efficiency is kept, the thickness of the CdS layer is greatly lowered. The Cd content of a whole cell module is greatly reduced.

The invention discloses a preparation method of a titanium dioxide-polyaniline composite corrosion-resistant coating. According to the preparation method, the steps of preparing nanometer titanium dioxide, synthesizing titanium dioxide-polyaniline, coating the surface of a metal plate with the titanium dioxide-polyaniline, and the like are synchronously carried out in a hydrothermal reaction kettle, and are completed through one step. The technical problem in the prior art that nanometer titanium dioxide is easy to agglomerate in a mixed solution system comprising the nanometer titanium dioxide and polyaniline is solved well, the technological process is greatly shortened, and the process control difficulty is reduced; besides, the step of heating and drying the composite coating required in the prior art is eliminated, and a series of technical problems that a coating easily cracks due to organic matter volatilization to further influence the combination firmness between the composite coating and a metal matrix, and the like are solved. The preparation method has the characteristics of being short in technological process, simple to control, stable and reliable in product quality, and the like, and the titanium dioxide-polyaniline composite corrosion-resistant coating prepared is suitable for being used as cathodic protection of copper, steel or stainless steel base material.

The invention discloses a refining processing method for an apocynum venetum fiber. The method comprises the steps of infiltrating and activating apocynum venetum bast; performing steam explosion activating treatment; caking and putting into a cage; performing directional catalytic oxidizing; chemically degumming and post-processing. Organic amine is adopted for infiltrating and activating and steam explosion activating treatment is performed, and then a ferrite solution and an activating agent are adopted for performing directional catalytic oxidization on lignin and hemicellulose; through the organic combination of a series of technical methods, such as, infiltration and activation, steam explosion, degumming and directional catalytic oxidization, the production method provided by the invention has the characteristics of good degumming effect, excellent indexes including finish fineness, length, strength and the like of the acquired apocynum venetum fiber, high quality, excellent spinning property, and the like; the chemical consumption is low; the environment-friendly pressure is low; the technical control is simple; the consumption of the public works, such as water, electricity and gas, is low, the efficiency is high and the method is suitable for industrial production.