Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

52results about How to "The lattice constant decreases" patented technology

Irradiation-resistant high-entropy alloy and preparation method thereof

The invention provides irradiation-resistant high-entropy alloy and a preparation method thereof. The general formula of the irradiation-resistant high-entropy alloy is TiZrHfVMoTaxNby, wherein X is no more than 0.25 and no less than 0.05, y is no more than 0.5 and no less than 0.05, and x and y are molar ratio. The preparation method of the irradiation-resistant high-entropy alloy comprises the following steps: sequentially mixing Ti, Zr, Hf, V, Mo, Ta and Nb, and then adopting vacuum electromagnetic suspension induction smelting or vacuum electric arc melting to obtain the irradiation-resistant high-entropy alloy. The irradiation-resistant high-entropy alloy is excellent in performance; helium ion simulated irradiation does not generate irradiation hardening damage; on the condition thatthe helium bubble size and traditional alloy size is equivalent, the bubble density is far lower than the density of the traditional alloy, and the lattice constant after irradiation is reduced abnormally; the irradiation resistance of the irradiation-resistant high-entropy alloy is far better than that of the traditional alloy; the irradiation-resistant high-entropy alloy has excellent strengthand plasticity; the compression yield strength of the irradiation-resistant high-entropy alloy under the cast condition is as high as 1.1 Gpa, and the compression ratio and elongation exceed 50%.
Owner:DALIAN UNIV OF TECH

Preparation process for high-silicon super-hard PVD coating

The invention provides a preparation process for a high-silicon super-hard PVD coating. The preparation process comprises the following steps: I, pre-processing a workpiece surface; II, clamping and loading a workpiece; III, performing vacuum-pumping on a furnace chamber; IV, heating the workpiece; V, etching and cleaning a target material and the workpiece; VI, preparing a high-silicon coating; VII, cooling the workpiece. The preparation process is used for obtaining the high-silicon super-hard PVD coating by controlling vacuum degree of a film-coating furnace chamber, bias voltage of a base body, a flow rate of nitrogen gas, target current and the like, wherein the flow rate of the reaction gas nitrogen gas (N2) ranges from 130 sccm to 210 sccm, the bias voltage of the base body ranges from 40 V to 120 V, and the vacuum degree of the furnace chamber ranges from 0.005 mbar to 0.060 mbar. By changing the element components of the coating, high silicon element content is obtained, so that the coating has characteristics of relatively high strength, hardness, wear resistance, high-temperature stability and corrosion resistance. A coating tool prepared by the process can be used for cutting a material with hardness of HRC65, and has relatively good using performances in comparison with a conventional coating.
Owner:SHANGHAI INST OF TECH

TiAlN ultra-hard composite coating provided with hardness gradient layer for supporting and preparation method of TiAlN ultra-hard composite coating

The invention discloses a TiAlN ultra-hard composite coating provided with a hardness gradient layer for supporting and a preparation method of the TiAlN ultra-hard composite coating. The TiAlN ultra-hard composite coating provided with the hardness gradient layer for supporting sequentially comprises a matrix material, an expansion layer and a deposition layer from bottom to top. The matrix material is a conductive material. The expansion layer is a plasma nitrocarburizing layer. The deposition layer is a nitrogen-aluminum-titanium coating. Through a compact TiAlN ultra-hard film, the matrixmaterial has sufficient wear resistance. The plasma nitrocarburizing layer has a hardness gradient and thus can remarkably improve the capacity to support a hard and brittle surface layer, and the bearing capacity of the TiAlN ultra-hard film is effectively improved. In addition, the residual stress value of the surface of a part is increased through nitrogen and carbon, and the fatigue resistanceof the part is made higher. Furthermore, nitride and carbide of the nitrocarburizing layer are better matched with the TiAlN film in thermophysical performance, a film / matrix interface is better fused, and thus the film has higher and more reliable bonding force and also has better thermal fatigue resistance.
Owner:NO 43 INST OF CHINA ELECTRONICS TECH GRP CETC

High frequency surface acoustic wave device with AlN (aluminum nitride) film as interlayer and preparation method thereof

The invention provides a high frequency surface acoustic wave device with an AlN (aluminum nitride) film as an interlayer. The device is characterized in that an a-axis preferred orientation AlN film is taken as a CVD (chemical vapor deposition) diamond substrate and a c-axis preferred orientation ZnO film is taken as an interlayer, the substrate and the interlayer are formed into an IDT(interdigital transducer)/ZnO/a-axis preferred orientation AlN/diamond multi-layered membrane structure and the structure is stacked with the IDT in sequence to form the high frequency surface acoustic wave device; the preparation method comprises the following steps of preparing an a-axis preferred oritention AlN film interlayer, and preparing a c-axis preferred oritentation ZnO film on the a-axis preferred orientation AlN film interlayer. The device and the preparation method provided by the invention have the following advantages that the sound velocity frequency dispersion caused by a large sound velocity gap between nanodiamond and ZnO can be solved, the application demand of the surface acoustic wave with high frequency above 4.8 GHz can be met, and moreover, the process is simple and easy to implement, and is beneficial for large-scale population and application.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

Electrochemical method for preparing fluorine-containing hydroxyapatite/zirconia transition coating on surface of medical titanium

InactiveCN103184497AAlleviate shortcomings such as thermal expansion coefficient mismatchHigh strengthImpression capsElectrolytic inorganic material coatingSolubilityApatite
The invention discloses an electrochemical method for preparing a fluorine-containing hydroxyapatite/zirconia transition coating on the surface of medical titanium. The method comprises the steps that: electro-deposition is carried in an electrolytic tank with a three-electrode system, wherein a medical titanium chip is adopted as a working electrode; a Zr(OH)4 plating is deposited in a zirconyl nitrate solution with a certain concentration and a certain pH value, wherein the deposition current is 11.1mA and the deposition time is 40s; a fluorine-containing hydroxyapatite (FHA) plating is deposited in an electrolyte which has a certain concentration and a certain pH value and which is composed of calcium nitrate, ammonium dihydrogen phosphate, and sodium fluoride, wherein the deposition current is 0.8mA and the deposition time is 3600s; and vacuum sintering is carried out under a temperature of 450 DEG C, such that the FHA/ZrO2 transition coating is obtained. According to the invention, fluorine partially substitutes hydroxyl group in apatite, fluorine ions are smaller than hydroxyl groups, and FHA lattice constant is small, such that FHA solubility is lower than HA. A coating morphology is changed from a micron-level chrysanthemum petal shape into a nano-level cone shape. With an antibacterial effect of F ions, dental caries can also be prevented. ZrO2 serves as a transition layer between the titanium substrate and the FHA coating, and the bonding strength between the FHA/ZrO2 transition coating and the Ti substrate is greatly improved. The bonding strength between the FHA/ZrO2 transition coating and the titanium substrate is high, a physiological solubility resistance is high, and antibacterial performance is good. The provided product has certain potential to be developed into an oral medical material with good development prospect.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

Blue light-ultraviolet continuously-adjustable aluminate fluorescent powder and preparation method thereof

The invention provides a blue light-ultraviolet continuously-adjustable aluminate fluorescent powder and a preparation method thereof. A Si-N bond is substituted for a Al-O bond; after the substitution, the internal structure of the fluorescent powder is improved; and thus, the luminescent spectrum of the fluorescent powder is continuously adjustable from blue light to ultraviolet light according to different substitution proportions. The fluorescent powder is more stable due to the doping of the Si-N key. The Si-N bond and Al-O bond have similar bond lengths, Si and Al, and O and N have similar bonding characteristics according to the diagonal line principle, so the Al-O bond in the aluminate-base fluorescent powder can be easily partially substituted by the Si-N bond; according to the charge compensation effect, after (SiN)+ is substituted for (AlO)+, the charge balance can be maintained; the bond length of the Si-N bond is slightly smaller than that of the Al-O bond, so that the matrix lattice constant is reduced, the cell volume is correspondingly reduced, and the atomic arrangement in the matrix is closer; and N with relatively smaller electronegativity can stabilize the Ce<2+>, so the material stability and light-emitting stability of the fluorescent powder are enhanced.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

TiZrMnFe quaternary getter alloy material and preparation method and application thereof

The invention discloses a TiZrMnFe quaternary getter alloy material and a preparation method and application thereof. The chemical formula of the TiZrMnFe quaternary getter alloy material is TixZr1-xMnFe (x is equal to 0-0.4), and the TiZrMnFe quaternary getter alloy material is specifically composed of, by mass, 2.3 wt%-10.4 wt% of titanium, 29.6 wt% to 41.6 wt% of zirconium; 27.8 wt% to 29.8 wt%of manganese; and 28.0 wt% to 30.3 wt% of iron. The crystal form of the TiZrMnFe quaternary getter alloy material is a C14 type laves crystal structure, and the grain size of the TiZrMnFe quaternarygetter alloy material is 20 microns to 50 microns. The preparation method comprises the steps that Ti, Zr, Mn and Fe pure metal with a certain stoichiometric ratio is weighed, proportioned and smeltedto obtain an alloy ingot, heat treatment is conducted, and the alloy ingot obtained after heat treatment is subjected to crushing, ball milling and sieving to be prepared into TiZrMnFe air suction alloy powder with different particle sizes. The alloy powder is pressed into getter products in various shapes through a cold press, or alloy powder adsorption slurry is brushed on the surface of a device through an adhesive. The preparation process is simple and feasible, the nitrogen adsorption capacity of the getter per unit mass is high and is superior to that of a ternary ZrMnFe alloy, and thepreparation cost is low.
Owner:CENT SOUTH UNIV

Two-dimensional photor crystal polarization beam dividing device

The planar photon crystal bundle-dispersing polarimeter refers to the field of electromagnetic wave bundle-dispersing polarimeter. Its character is that insert the dielectric stick to the background media whose refractive index is much lower than that of the dielectric stick to form a planar seasonal structure. Along the incident direction of the electromagnetic wave, it's orderly composed of three parts that are the left transmission-enhancing film, the main part and the right transmission-enhancing film. The radius of the dielectric stick in the main part is higher than that of the other two parts. The incident side of the main part is pressed close to the outdiffusing side of the left transmission-enhancing film, and the incident side of the right transmission-enhancing film is pressed close to the side of the outdiffusing side of the main part. This invention has an advantage that the fixity of all the standards of the photon crystal itself won't metamorphose. When the work wavelength is the same, the crystal lattice constant of this invention is much smaller than that of the present planar photon crystal bundle-dispersing polarimeter. Therefore it's portable and cabinet. This invention can also transmit two reciprocally vertical polarizing ponderance at the same time, so it's polarizing degree is high and the transmitted index is big.
Owner:TSINGHUA UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products