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118results about How to "Fix interface issues" patented technology

Surface modification method for carbon nano tube

The invention provides a surface modification method for a carbon nano tube and belongs to the field of nanotechnology. The method includes step one, uniformly mixing a carbon nano tube which is subjected to acidification by a strong oxidizing acid with a silane coupling agent and deionized water, reacting under a certain condition, filtering, washing, and drying to obtain a primary modified carbon nano tube; step two, uniformly mixing the primary modified carbon nano tube with polyhydric alcohols and a concentrated sulfuric acid, reacting under a certain condition, filtering, washing to neutral, and drying to obtain a secondary modified carbon nano tube; uniformly mixing the secondary modified carbon nano tube with an organic carboxylic acid, an esterification reaction catalyst and N,N-dimethylformamide, reacting under a certain condition by the aid of the protection of inert gases, cooling to the room temperature, filtering, washing, and drying to obtain the surface modification carbon nano tube. When the prepared modified carbon nano tube which is provided with ester groups on the surface is mixed with a polyester resin, the interface-free mixing is achieved, and the heat stability and the mechanical property of the modified polyester resin can be improved.
Owner:TAIYUAN UNIV OF TECH

Fiber mesh tape-wound and reinforced composite pipe, preparation process and device

The invention relates to a fiber mesh tape-wound and reinforced composite pipe, a preparation process and a device, belonging to the technical field of forming processes of composite pipes. The composite pipe comprises an inner-layer core pipe and a post-coated layer, as well as a fiber mesh tape arranged between two layers, wherein the inner-layer core pipe is extruded by a core pipe extruding machine, the adhesive resin fiber mesh tape is heated through a post-heating box, and the composite pipe is finally obtained by traction through a post-traction machine, sizing through a vacuum spraying and sizing box and the like. According to the composite pipe disclosed by the invention, the technology is adopted, the preparation process is simple, the existing tape plastic covering treatment process and the composite pipe forming process are combined into a whole, the number of workers for production is reduced, and the degree of automation is improved; furthermore, the used device is a conventional device, and the cost is reduced; and in addition, adhesive resin is firstly coated on the outer surface of the core pipe, and the plain woven fiber mesh tape is further wounded, so that the interface problem in the pipe is effectively solved, the mechanical properties of the pipe are upgraded and the stability of the pipe during long-term use is also improved.
Owner:ZHEJIANG WEIXING NEW BUILDING MATERIALS CO LTD

Silicon carbide particle reinforcement aluminum-based composite for train brake disc and preparation method

Disclosed are a silicon carbide particle reinforcement aluminum-based composite for a train brake disc and a preparation method. The composite includes the following components of, by mass percentage, 15-25% of SiC particles, 18-24% of Si, 0.6-3.5% of Mg, 0.15-0.35% of Zr, 0.12-0.45% of Sc, and the balance Al and unavoidable impurities. According to the preparation method, SiC, Mg, Si, Zr and Sc with the particle size being 10-15 [mu]m are added into molten aluminum in the form of intermediate alloy, SiC with the particle size being 15-25 [mu]m is added into the molten aluminum in the form of particles, and thus the silicon carbide particle reinforcement aluminum-based composite is obtained. The SiC thin particles are added in the form of Mg-SiC, so that the problems of uniform dispersing difficulty of silicon carbide particles in a matrix and poor interface bonding are effectively solved, the particle reinforcement effect is fully played, and the toughness of alloy is improved. Meanwhile, transitional element zirconium and rare earth element scandium are added to replace titanium fine grains, the roughness and heat resistance of the aluminum-based composite are remarkably improved, and occurrence of heat fatigue cracks is restrained. In addition, the added rare earth scandium has a good modification effect on the interfacial compatibility of the silicon carbide particles and aluminum alloy.
Owner:湖南中南智造新材料协同创新有限公司

Carbonization reinforced regenerated aggregate, and preparation method and applications thereof

The invention discloses a carbonization reinforced regenerated aggregate, and a preparation method and applications thereof, and belongs to the technical field of building material. The preparation method comprises following steps: building garbage is crushed so as to obtain uniform aggregate particles; cement and admixture fine powder are weighted for uniform mixing so as to obtain a surface coated material; the prepared aggregate particles and the surface coated material are mixed, and are introduced into a granulator, water is sprayed uniformly for granulation so as to obtain a coated aggregate; the coated aggregate is introduced into a sealed environment or the natural environment for pre-curing; an aggregate obtained through pre-curing is introduced into a carbonization device for carbonization treatment so as to obtain the carbonization reinforced regenerated aggregate. The preparation method is adopted to prepare the light aggregate, so that aggregate light weight and high strength are achieved, aggregate cylinder compressive strength can be as high as 13.0MPa, and is higher than the using standard cylinder compressive strength 6.5MPa of common light aggregate. The production technology is simple; resource utilization of solid waste is realized; adsorption immobilization of carbon dioxide is realized; sintering is not needed; and low carbon emission and environment protection are realized.
Owner:NANJING UNIV OF TECH

Preparation method for carbon fiber powder reinforced tungsten-based composite material

The invention discloses a preparation method for a carbon fiber powder reinforced tungsten-based composite material. The preparation method is achieved in the way that tungsten powder and carbon fiberpowder pretreated through rhenium plating are taken as raw materials to undergo raw material treatment, laser sintering, sample post-treatment and other steps correspondingly. According to the preparation method, the preparation process is simple, energy saving and emission reduction are achieved, the effect of being environment-friendly is achieved, in the case of the prepared composite material, the crystallinity is good, the density is high, the average density is 17.32 g / cm<3>, the average relative density is 98.97%, the product hardness is high, the average hardness can reach up to 340.9HV0.2, the toughness is good, the minimum fracture toughness is 6.5 MPa.m<1 / 2>, no degreasing process is adopted, so that the deformation problem caused by the complex degreasing process is avoided,in addition, the rhenium on the surface of the carbon fiber powder successfully blocks direct contact between the carbon and the tungsten, and the rhenium has excellent wettability to the tungsten, sothat a composite material interface transition layer is formed, the interface problem in the preparation process is solved, the preparation procedure of the product prepared through the method is greatly shortened compared with a traditional vertical fusion sintering method, and the preparation method can be developed into a 3D printing technology downstream to realize the direct production of the terminal product.
Owner:重庆金锐新材料技术研究院有限公司

Galvanizing carbon fiber foamed light metal and preparation method thereof

The invention provides a galvanizing carbon fiber foamed light metal and a preparation method thereof, and relates to foamed light metal technical field. The foamed light metal is composed by galvanizing carbon fiber and light metal. The preparation method comprises the following steps: (1) electroplating carbon fiber in a solution formed by zinc chloride, ammonium chloride, boric acid and dextrin; (2) adding a certain amount of galvanizing short fiber and carboxy methyl amylum ester into saturated salt water and followed by stirring uniformly, and adding a certain amount of salt particle to mix the mixture uniformly and followed by compaction; (3) heating the above mixture and followed by a heat preservation treatment to form a preform; (4) putting the preform into a mould, and filling salt particle to the full around the preform for compaction; (5) heating the preform to a temperature of 300-350 DEG C and followed by a heat preservation treatment, and pouring an overheated light metal solution into the mould to fill gap of the salt particle; (6) washing the salt particle away with water after cooling and solidification to obtain the galvanizing carbon fiber foamed light metal. The galvanizing carbon fiber foamed light metal has the advantages of high strength, high modulus and the like, and has wide and practical application.
Owner:TAIYUAN UNIVERSITY OF SCIENCE AND TECHNOLOGY

Preparation method of composite electrode, composite electrode and lithium ion battery

The invention provides a preparation method of a composite electrode. The preparation method comprises the following steps: mixing a ternary positive electrode material, a solid electrolyte and a conductive agent to obtain a precursor; carrying out discharge plasma sintering on the precursor, so that the ternary positive electrode material, the solid electrolyte and the conductive agent are combined into a whole to obtain a composite electrode. The invention further provides the composite electrode and a lithium ion battery. According to the preparation method of the composite electrode provided by the invention, through discharge plasma sintering treatment, the ternary positive electrode material, the solid electrolyte and the conductive agent are tightly combined together in the case that own structures of the ternary positive electrode material, the solid electrolyte and the conductive agent are not damaged, and meanwhile, the interface problem between the electrode and the solid electrolyte in the lithium ion battery is solved; meanwhile, compared with the traditional hot pressing method and a pressureless sintering method, in the preparation method disclosed by the invention,sintering and hot pressing are carried out simultaneously, thereby greatly shortening the preparation time.
Owner:SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV

High-flame-retardant waterborne polyurethane and preparation method thereof

The invention provides waterborne polyurethane and a preparation method thereof. The preparation method comprises the following steps: letting phosphorus-free polyol react with specific phosphorus-containing polyol as shown in a formula (1), a phosphorus-containing stabilizer as shown in a formula (2) and polyisocyanate to form a prepolymer, emulsifying, and reacting with a phosphorus-containing chain extender to form the waterborne polyurethane. Phosphorus-containing groups are introduced into a soft segment of a polyurethane molecular chain by adopting phosphorus-containing polyol shown as the formula (1) to form a part of a waterborne polyurethane structure unit, so that the waterborne polyurethane structure unit has flame retardance under the condition that a flame retardant is not added; by adopting the phosphorus-containing stabilizer as shown in the formula (2), emulsification of phosphorus-containing waterborne polyurethane can be promoted, and the problem that emulsion is unstable after chain extension is solved, so that the problems that when a phosphorus-containing group is introduced into a polyurethane molecular structure, emulsification is difficult, and a waterbornedispersion liquid is difficult to form are solved. Moreover, phosphine-containing groups are introduced into the soft segment, the stabilizer and the chain extender of the waterborne polyurethane, sothat the flame retardance is greatly improved; and meanwhile, the binding power of the waterborne polyurethane is also enhanced by introducing a specific phosphorus-containing structure.
Owner:SHANGHAI DIMU NEW MATERIAL TECH

Composite powder of metal-metal carbide coated carbon particle and preparation method thereof

The invention relates to composite powder of a metal-metal carbide coated carbon particle and a preparation method thereof, and belongs to the technical field of metal powder. The metal-metal carbidecoated carbon particle is composed of a metal layer, a metal carbide layer and a carbon particle, wherein the metal carbide layer is coated on the surface of the carbon particle, and the metal layer is coated on the surface of the metal carbide layer; according to the composite powder, superfine carbon particles and matrix metal powder are used as raw materials, and mechanical force is applied, sothat the superfine carbon particles penetrate through and / or are inlaid into the matrix metal powder, and then in-situ carburization is performed so as to obtain the metal carbide layer. The preparation method comprises the steps of performing mechanical milling on degummed short carbon fiber and the metal powder first so as to obtain a large quantity of superfine carbon particles which are uniformly inlaid into the metal powder, then separating and annealing at high temperature, so that solid-phase reaction occurs between the carbon particles and surrounding metal, and the metal-carbon particle composite powder of which metal carbide is uniformly coated on the surfaces of the carbon particles is obtained.
Owner:CENT SOUTH UNIV

Sheet hydroxyapatite/polylactic acid nanometer composite prepared through in-situ intercalation method

The invention provides a new method for preparing a sheet nanometer hydroxyapatite / polylactic acid composite through an in-situ compound intercalation method for solving the problems that a traditional blending method is complex in preparation step, poor in nanoparticle dispersion, contradictory in strength and toughness and the like. The method includes the steps of preparing long-range orderly nanometer sheet hydroxyapatite with lauric acid as template agent, conducting ring opening polymerization on lactide molecules between layers of hydroxyapatite to form polylactic acid through the in-situ polymerization intercalation method with lactide monomers as the raw material, and forming the organic and inorganic nanometer composite of a nacre-like structure. Breakthrough is achieved on the aspects of strength and toughness of the composite at the same time, the tensile strength of the composite with addition amount of 5% is increased by 40% compared with that of pure polylactic acid, and the elongation at break is increased by 30%. The preparation process is simple, surface treatment does not need to be conducted on hydroxyapatite, no substances with biological toxicity are introduced in the whole process, and biological compatibility is high.
Owner:NORTH CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Organic amine surface-modified metal sulfide material, manufacture method and applications thereof

The invention provides an organic amine surface-modified metal sulfide material, which is composed of a metal sulfide material and an organic amine shell, wherein the organic amine shell is covered on the metal sulfide material. The metal sulfide material and the organic amine shell are bound together through strong chemical bonds, so the chemical and physical properties of the provided material are very stable. Because the metal sulfide material and the organic amine shell are strongly bound together, the shell will not fall off the metal sulfide material even under various chemical reactions or after a plurality of circulation usages. The invention also provides a method for carrying out organic amine surface modification on the metal sulfide material. The modification method comprises the following steps: mixing the metal sulfide material and an organic compound / polymer containing an amino functional group in an organic phase, and then heating the system to carry out chemical synthesis. The invention further provides the applications of the provided metal sulfide material, which is mainly used as a semiconductor luminescent material, a photo-electric and electro-optical conversion material, a photoelectric catalysis material, a photo-thermal material, a bio-labeling material, a coloring material, and the like.
Owner:BEIJING GIGNANO BIOINTERFACE

Microcapsule fire extinguishing agent and preparation method thereof

The invention provides a microcapsule fire extinguishing agent and a preparation method thereof. The microcapsule fire extinguishing agent comprises a flame-retardant shell composed of a low-melting-point copolymer and a cooling inner core containing a cooling material, wherein the flame-retardant shell coats the cooling inner core to form microcapsule particles with a core-shell structure, the low-melting-point copolymer is formed by copolymerizing a low-melting-point high-molecular polymer monomer and a flame retardant, the flame-retardant shell melts and explodes automatically when the external environment reaches the preset starting temperature, and the cooling inner core in the flame-retardant shell is released. The microcapsule fire extinguishing agent provided by the invention adopts an in-situ polymerization preparation method, and the microcapsule fire extinguishing agent with different starting temperatures is prepared by regulating and controlling the reaction parameters such as the variety of low-melting-point high-molecular polymer monomers, the mass ratio of the low-melting-point high-molecular polymer monomers to the cooling material, the copolymerization reaction time and pressure and the like, so that the microcapsule fire extinguishing agent is suitable for different scene requirements. The microcapsule fire extinguishing agent provided by the invention has targeting property, also has dual effects of cooling and fire extinguishing, and has huge application value.
Owner:HUAZHONG UNIV OF SCI & TECH
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