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99 results about "Para-tertiary-butylphenol" patented technology

Preparation method for vegetable oil modified rosin phenolic resin

The invention provides a preparation method for vegetable oil modified rosin phenolic resin. The preparation method comprises the following steps of firstly, feeding rosin into a reaction kettle, raising the temperature to be 180DEG C, adding vegetable oil, continuously raising the temperature to be 210 to 215DEG C and keeping the temperature for 1 to 1.5 hours, and carrying out addition reaction; secondly, feeding pentaerythritol and magnesium oxide into the reaction kettle, reducing the temperature to be 160 to 170DEG C, feeding dodecylphenol and p-tert-butylphenol according to the mole ratio of 1:1.01 to 1.03, then continuously reducing the temperature to be 120 to 130DEG C, feeding paraformaldehyde according to the mole ratio of phenol to aldehyde being 1:2.0 to 2.1, and keeping the temperature for 2 to 2.5 hours; thirdly, raising the temperature in the reaction kettle to be 260 to 270DEG C, keeping the temperature, carrying out esterification reaction until an acid value is smaller than 25mgKOH/g, and carrying out reduced pressure distillation to obtain a low-boiling-point substance, namely the vegetable oil modified rosin phenolic resin. The resin prepared by the preparation method provided by the invention has the advantages of high viscosity, good solubility, high molecular weight, uniformity in distribution and suitability for offset lithography of ink.
Owner:桂林兴松林化有限责任公司

Preparation method of molecular imprinting sorptive extraction stirring bar by using alternative template

The invention relates to a preparation method of a molecular imprinting sorptive extraction stirring bar by using an alternative template, belonging to the technical field of analytical chemistry and sample pretreatment. The method includes firstly using p-tert-butylphenol as a template molecule, dissolving the template molecule and a functional monomer in a solvent, uniformly mixing by ultrasound and standing, then adding a crosslinking agent and an initiator to obtain an assembly solution, and removing oxygen by ultrasound; injecting the assembly solution into a glass capillary with an inner diameter of 1.4mm, then inserting into a glass capillary with an outer diameter of 1.0mm, performing water bath heating for polymerization, removing the larger glass capillary, taking out the small glass capillary, cutting into appropriate length with a blade, inserting a iron core and sealing ends, sleeving silicon tubes on both ends, and cleaning with methanol, to obtain the molecular imprinting sorptive extraction stirring bar using p-tert-butylphenol as the alternative template. The obtained stirring bar can be applied to extraction analysis of trace amount of environmental estrogen bisphenol A in a water sample.
Owner:KUNMING UNIV OF SCI & TECH

Treatment method for waste salt water generated in production process of polycarbonate

The invention relates to a treatment method for waste salt water generated in the production process of polycarbonate. The treatment method comprises the following steps: the temperature of the wastesalt water generated in the production process of the polycarbonate PC and containing bisphenol A, p-tert-butylphenol and quaternary ammonium salt is regulated to 20-60 DEG C by a heat exchanger, thenthe waste salt water is introduced into an acid-regulating kettle, and the pH value is regulated to 1-4; then trace suspended solids are removed by a coarse filter and a precise filter, and the wastesalt water is conveyed to a high-position groove; the waste salt water flows into macroporous resin adsorbing columns by gravity to be adsorbed, then enters an alkaline-regulating kettle, and the pHvalue is regulated to 10-14; finally, the waste salt water enters active-carbon adsorbing columns to be adsorbed. The treatment method has the beneficial effects that phenolic organic matters in the waste salt water of the PC can be completely removed, and most of quaternary ammonium salt is removed; in the treated salt water, the content of the quaternary ammonium salt is less than 1ppm, the content of TOC (Total Organic Carbon) is less than 10ppm and the content of TN (Total Nitrogen) is less than 3ppm; as a raw material, the treated salt water can be used for a process for preparing causticsoda by a chlor-alkali ion membrane, and can not cause increase of voltage of an electrolytic cell, so that sodium chloride and water in the waste salt water can be recycled, and the recycling of thematerials is realized.
Owner:QINGDAO UNIV OF SCI & TECH +2

Special cable for oil platform

InactiveCN106380647AImprove mechanical propertiesExcellent hot air aging performanceRubber insulatorsMelamine phosphatePolyvinyl chloride
The invention discloses a special cable for an oil platform. The special cable comprises a cable core and a sheath, wherein a modified nitrile rubber composite material is prepared from the following raw materials in parts by weight: 100 parts of nitrile rubber, 38 to 43 parts of ethylene propylene diene rubber, 2 to 5 parts of ethylene-vinyl acetate, 2 to 8 parts of chlorinated polyethylene, 0.5 to 2 parts of stearic acid, 0.5 to 3 parts of zinc oxide, 1 to 2 parts of p-tert-butylphenol-formaldehyde resin, 0.5 to 2 parts of DCBP, 0.5 to 1.5 parts of trimethylol-propane trimethacrylate, 3 to 15 parts of silicon aluminum carbon black, 2 to 10 parts of nanosilicon dioxide, 3 to 15 parts of aedelforsite, 3 to 15 parts of polyvinyl chloride, 1 to 5 parts of melamine phosphate, 2 to 10 parts of 6-chloro-N,N-diethyl-1,3,5-triazine-2,4-diamine, 10 to 30 parts of phosphorus silicon and nitrogen fire retardants, 1 to 2.5 parts of diethylene glycol distearate, 1 to 3 parts of 2-deoxy-2,2 difluoro-pentofuranose-1-ketone-3,5-dibenzoate, 1 to 3 parts of anti-aging agents, 0.5 to 2 parts of accelerants and 0.5 to 2 parts of silane coupling agents. The special cable for the oil platform provided by the invention has the advantages that the mechanical property is excellent; the aging-resistant and low-temperature-resistant performance is good; the fire-resistant and oil-resistant performance is excellent.
Owner:重庆三峡电线电缆科技股份有限公司

Polychloroprene adhesive and preparation method thereof

The invention discloses a polychloroprene adhesive and a preparation method thereof. The polychloroprene adhesive is characterized by being composed of following main components: chloroprene rubber, dehydrated malic acid resin, p-tert-butyl phenol polyacetylene resin, active magnesium oxide, an anti-aging agent, a solvent, a catalyst, a formaldehyde absorbent, and a formaldehyde remover. The polychloroprene adhesive and the preparation method thereof have the advantages that: (1) the polychloroprene adhesive does not contain benzene, methyl benzene, dimethyl benzene, and halohydrocarbons toxic solvents, has a high content of non-volatile materials, and can satisfy the environmental requirements; (2)the preparation method substitutes hydrated malic acid resin and p-tert-butyl phenol polyacetylene for phenolic resin as the tackifying agent, thus controls the release of free formaldehyde from the source, and at the same time guarantees a good adhesive property; (3) a formaldehyde absorbent and a formaldehyde remover are added, can continuously release negative ions, firstly captures free formaldehyde and then eliminates the free formaldehyde, has a high capture efficient of free formaldehyde and a long effective time, and is capable of continuously eliminating the free formaldehyde released from the decorating materials for a long time.
Owner:GUANGDONG SANVO CHEM IND TECH
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