The application discloses a kind of adjustable defect sub-nanometer gold load
nickel iron composite photoanode catalyst, preparation method and application, deionized water is introduced into
nitrogen and is deoxidized, multi-walled
carbon nanotube treated by strong acid is placed in deionized water after deoxidation, after
ultrasonic dispersion is uniform, together with FeCl2, NiCl2, HMT and
ammonium fluoride is added into reaction kettle, reaction is carried out at 120 DEG C for 6 hours, after cooling, it is taken out, using deionized water is filtered, washed after, HAuCl4 is quickly added, sealed and is stirred in
dark room, after reaction is finished, it is filtered, washed,
nitrogen is dried at
room temperature and is preserved in
oxygen-free
atmosphere.The application is synthesized Au / NiFe (hydroxyl)
oxide / CNT composite catalyst by in-situ oxidation technology one step.The method can be simultaneously controlled on the basis of
heterojunction Defects, the synergistic effect of both makes the catalyst performance be further optimized.Synthesis method is simple and direct, and
catalytic effect is obviously improved.