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47results about How to "Has a reducing effect" patented technology

Method for using biomass waste for preparing nitrogen-doped carbon nanotube coated metal particle composite material

The invention discloses a method for using biomass waste for preparing a nitrogen-doped carbon nanotube coated metal particle composite material. The method includes the following steps that firstly, the biomass waste and KOH are evenly mixed in deionized water, an obtained heterogeneous mixture is carbonized under the protection of inert gas, and biomass charcoal is obtained; and then, the biomass charcoal, a nitrogenous nonmetallic compound and water-soluble divalent metal salt are evenly mixed in methyl alcohol, the obtained heterogeneous mixture is subjected to pyrolysis under the protection of the inert gas, and therefore a target product is obtained. By the adoption of the method, a two-step pyrolysis technology is adopted for achieving growth of carbon nanotubes, and dispersion of metal nanoparticles and formation of a cooperative acting mechanism are promoted; the stability of the composite material is reinforced through the structure of carbon nanotube coated metal nanoparticles; the surface activity and dispersity of a carbon layer are improved through in-situ decoration of the nitrogen element; and the contact and active site point number is increased through the formation of a rich pore structure and the high specific surface area.
Owner:安徽皖瑞能源科技有限公司

Nano-grade ZnO loaded magnetic biological carbon composite photocatalyst and preparation method thereof

The invention provides a nano-grade ZnO loaded magnetic biological carbon composite photocatalyst and a preparation method thereof. The preparation method comprises the following steps: step 1: carrying out thermal hydrolysis on a biomass under an alkaline condition to extract plant fibers; after drying, carrying out pre-carbonization treatment; mashing and sieving with a sieve with the size of 10to 20 meshes; step 2: mixing a ferrous salt solution and a potassium hydroxide solution; adding soluble zinc salt; step 3: adding the sieved plant fibers into the solution formed by step 2; uniformlymixing and adding a potassium nitrate solution; after sufficiently stirring, treating a mixture in a water bath; continuously stirring and ageing until black gel is formed, so as to obtain a black gel solution; step 4: after washing and drying the black gel solution, generating dry gel; calcining the dry gel and continuously introducing inert gas; after washing and drying, obtaining the nano-grade ZnO loaded magnetic biological carbon composite photocatalyst. According to the nano-grade ZnO loaded magnetic biological carbon composite photocatalyst, magnetic biological carbon is used as a carrier of the photocatalyst, and the problem that the photocatalyst in chromium-containing sewage treatment is difficult to separate and recycle is solved.
Owner:湖南大辰环保股份有限公司

Preparation method of carbon-coated lithium iron phosphate with grade structure

InactiveCN103956493AAvoid FePO <sub>4</sub> productionHigh purityCell electrodesSecondary cellsHigh energyLithium-ion battery
The invention relates to a preparation method of a lithium iron phosphate material as a lithium ion battery positive electrode active substance. The preparation method comprises the following steps: dissolving a lithium source, an iron source and a phosphorus source in a reducing agent, adding a chelating agent, and uniformly stirring to form a mixed solution; performing a hydrothermal reaction; washing and drying to obtain lithium iron phosphate with a grade structure; and mixing with a carbon source, and calcining in a reducing atmosphere to obtain carbon-coated lithium iron phosphate with the grade structure. Compared with the prior art, the preparation method has the beneficial effects that the purity of the product is increased; the reducing agent has a reducing function, the chelating agent has a structure guiding function; the conductivity of lithium iron phosphate is enhanced, and the electrochemical property is improved; a resultant temperature interval is large, and a great application value and a bright development prospect are achieved; the specific capacity is high, the specific surface area is moderate, the cycle performance is good, the repeatability is high, the processing property is excellent, and the demand on a high energy storage device in practical production can be met.
Owner:WUHAN UNIV OF TECH

Cooperative treatment method for dioxin and heavy metal in flying ash on basis of steel slag and mineral slag

A cooperative treatment method for dioxin and heavy metal in flying ash on the basis of steel slag and mineral slag is characterized by comprising the following steps that (1) to-be-treated flying ashand a dehalogenation agent are mixed according to a mass ratio of 4:1-9:1, mixed milling is conducted by a planetary mill or a ball mill, and after 2-10 h of continuous ball milling, organochlorine degradation flying ash is obtained; (2) the organochlorine degradation flying ash and a curing agent are mixed according to the mass ratio of 4:1-9:1 and are stirred evenly, and a flying ash mixture isobtained; and (3) water or a reducing agent of the mass ratio of 15% is added into the flying ash mixture, the obtained mixture is put into a compaction die for compaction forming, pressure is 20-50kN, pressing time is 15-30 s, maintenance is conducted for 3-7 days, and a flying ash solidified body is obtained. Through the cooperative treatment method, dioxins and heavy metal pollutants can be treated simultaneously, steel slag serves as a main material of the dehalogenation agent and can be utilized efficiently, and the problem of a low comprehensive utilization rate of the steel slag is solved while the flying ash is treated.
Owner:CHANGJIANG RIVER SCI RES INST CHANGJIANG WATER RESOURCES COMMISSION

Method for roasting vanadium pentoxide extracted by scherbinaite coal contained primary ore

The invention relates to a method for roasting vanadium pentoxide extracted by scherbinaite coal contained primary ore. After being smashed to certain mesh degree, scherbinaite coal contained primary ore is sent into the main bed and the secondary bed of a fluidzed bed furnace; different blasting intensities when the main bed and the secondary bed roast are controlled, twice fluidization roasting is carried out to completely decarburize; after the decarburization material of the main bed and the secondary bed is added with barium salt, the mixture is roasted in a rotary kiln. The invention has the beneficial effects of short process flow, simple and easy operation, high yield and low production cost and can realize production automation control; vanadium has high immersion ratio which can be above 80%; and sulfuric acid consumption amount is low, only about 50 kg of sulfuric acid is consumed for each ton of cinder. The invention is the optimum path for comprehensively utilizing scherbinaite coal contained primary ore and can realize 'one ore three factories', i.e. a stone coal mine, a power station, a vanadium plant and a cement plant. The scherbinaite coal contained primary ore is in fluidized bed roasting to generate electricity; electricity is generated for the cinder to extract vanadium; the vanadium extracting tailings are high-quality filler of the cement plant to realize comprehensive utilization of resources, thus creating great economic benefit and social benefit.
Owner:淅川县玉典钒业有限责任公司

Method for performing microwave solvothermal in-situ synthesis on carbon-coated lithium iron phosphate

The invention relates to a method for performing microwave solvothermal in-situ synthesis on carbon-coated lithium iron phosphate. The method comprises the following steps: dispersing a lithium source and an iron source in an alcohol reducing agent; adding a phosphorus source, stirring, adding a chelating agent, and stirring, thereby obtaining a precursor solution; adding part of the precursor solution into a microwave reactor, heating and reacting to obtain a product; washing the obtained product and drying, thereby obtaining a precursor; and calcining the precursor in a reducing atmosphere, thereby obtaining the product. The method disclosed by the invention has the beneficial effects that the time can be saved by virtue of in-situ carbon coating, and the uniformity of coated carbon can be ensured. Meanwhile, the conductivity of the lithium iron phosphate can be enhanced by virtue of the coated carbon, and the electrochemical performance is improved; the lithium iron phosphate is of a three-dimensional bi-continuous structure, nano-particles in the structure are connected with one another, a three-dimensional network is formed, the lithium-ion transmission distance is greatly shortened, and the electrochemical performance of the material is improved; the reaction period is short, and the process is simple; and the prepared lithium iron phosphate is high in specific capacity, good in cycle performance, high in repeatability and excellent in processability.
Owner:WUHAN UNIV OF TECH

Heavy metal activator and application thereof in soil joint restoration

The invention provides a heavy metal activator and application thereof in soil joint restoration. The activator preparation comprises the following steps that (1) straws are crushed and sieved, the crushed straws are added into an alkaline solution, a heating reacting is conducted, filtering is conducted after finishing the heating reaction, the filtration residue is taken and washed with water, washing is repeated until the eluent is neutral, and drying is conducted to obtain the lignin-removed straws; (2) urea is added into the lignin-removed straws, composting fermentation is conducted, rapeseed meal is added after the fermentation is thoroughly decomposed, a functional microbial agent is added, secondary fermentation is conducted after uniform stirring, and then after the second fermentation, the straw bio-organic fertilizer is obtained; and (3) organic acid is added into the straw bio-organic fertilizer, and uniform mixing is conducted to obtain the heavy metal activator. According to the application, through crop-rotation combined planting of soybeans and oilseed rape, the heavy metal is activated by the heavy metal activator, so that heavy metal in the soil can be convertedinto an effective state as much as possible to realize the continuous absorption of heavy metal, the joint restoration efficiency is improved, and the easy-to-implement and efficient combined restoration method is also provided for restoring heavy metal contaminated farmland soil.
Owner:湖南泰谷生态工程有限公司

Preparation method of low-oxide-inclusion high-performance powder metallurgy nickel-base superalloy

The invention provides a preparation method of a low-oxide-inclusion high-performance powder metallurgy nickel-base superalloy, and belongs to the field of metal materials. The preparation method comprises the steps that firstly, spherical prealloyed powder is prepared from the components by adopting a vacuum gas atomization powder processing technology in percentage by mass: 0.16-0.19% of C, 9.8-12% of Cr, 16.5-17.5% of Co, 7.7-8.8% of W, 0.65-0.88% of Mo, 5.75-6.30% of Al, 0.025-0.033% of B, 0.055%-0.087% of Zr, and the balance of of Ni; then the prealloyed powder with certain granularity and TiH2, TaH and HfH2 powder with certain content and granularity are selected for being uniformly mixed; a mixture is loaded in a rubber covering sleeve for cold isostatic compaction; then the rubbercovering sleeve is removed and a formed green body is placed in a high vacuum hot-pressing furnace for hot-pressing sintering compactness according to a certain sintering process; then the compact sintered green body is forged or rolled according to the requirement to obtain workblank parts; and finally, the parts are subjected to timeliness treatment. By adopting the preparation method of the low-oxide-inclusion high-performance powder metallurgy nickel-base superalloy, the oxygen content of prepared nickel-base superalloy materials is low, and high endurance strength and high low-cycle fatigue can be obtained.
Owner:安徽爱科德新材料科技有限公司

Method for extracting activated sludge extracellular polymers

The invention belongs to the technical field of sewage biology, and particularly relates to a method for extracting activated sludge extracellular polymers. The method comprises the following steps: pretreating activated sludge, carrying out soluble extracellular polymeric substance (S-EPS) extraction, carrying out loosely bound extracellular polymeric substance (LB-EPS) extraction, carrying out ionic tightly bound extracellular polymeric substance (TB-EPS) extraction, and carrying out hydrophobic tightly bound extracellular polymeric substance (TB-EPS) extraction. According to the method forextracting the activated sludge extracellular polymers, the liquid phase environment of EPS extraction is optimized, the combination of different extraction methods is screened, an inorganic ion extraction agent is selected, and different types of surfactants are screened to separately and sequentially extract four different types of EPS, namely S-EPS, LB-EPS, ionic TB-EPS and hydrophobic TB-EPS in the activated sludge, so that extraction efficiency of different types of EPS is high, purity is high, and the cell damage is small. The adopted inorganic ionic extraction agents are small in changedegree of the extracellular polymer, are green and environmentally friendly, and are accurate in quantification.
Owner:CHONGQING UNIV

Fully-closed working chamber for vehicle sterilization, disinfection and deflavour

A fully-closed working chamber for vehicle sterilization, disinfection and deflavour comprises a working chamber main body consisting of a chamber body, an equipment chamber and an operation chamber, wherein the chamber body is provided with a main door for the entry of the vehicle needing sterilization and disinfection and an auxiliary door for the entry of staff; the main door is connected directly with the outdoor and the auxiliary door is connected indirectly with the operation chamber; the top of the chamber body is provided with an interlayer as the equipment chamber within which a ventilation purification system mainly comprising a fan, a ventilating pipe and an air volume control valve and an exhaust discharge system mainly comprising an exhaust fan, an electric valve and a discharge pipe; the chamber body is further provided with an efficient ultraviolet germicidal lamp and a negative ion generator. The invention has the advantage of good sterilization and disinfection, high working efficiency, complete function of sterilization, disinfection and deflavour and omni-directional sterilization and disinfection for the external and the internal of the vehicle, which quickly, fully and basically solves the problem of air pollution in the vehicle.
Owner:沈阳大鼎企业管理咨询有限公司

Copper-silver-loaded few-layer graphene-based composite material as well as preparation method and application thereof

The invention discloses a preparation method of a copper-silver-loaded few-layer graphene-based composite material, which comprises the following steps: S1, taking graphite powder, absolute ethyl alcohol, cyclohexane, anhydrous cupric sulfate, Tween 80, span 80, PVP and deionized water as raw materials, and uniformly mixing through vortex to prepare a uniform and stable graphite water-in-oil emulsion; s2, performing low-temperature freezing on the graphite water-in-oil emulsion prepared in the step S1 for 2 hours, and then performing ultrasonic treatment for 2 hours; s3, sodium borohydride is added into the graphite water-in-oil emulsion treated in the step S2, then low-temperature freezing is conducted for 2 h, and then ultrasonic treatment is conducted for 2 h; and S4, adding a 2% PVP aqueous solution containing silver nitrate into the graphite water-in-oil emulsion treated in the step S3, performing low-temperature freezing for 2 hours, and performing ultrasonic treatment for 2 hours to obtain the few-layer graphene-based composite material CuxO / Ag-coated FLG. The preparation method is simple in synthesis process and high in yield. The hydrogen peroxide sensor prepared from the few-layer graphene-based composite material CuxO / Ag-coated FLG is excellent in sensing performance.
Owner:GUANGDONG PHARMA UNIV
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