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50 results about "Aminoethylene" patented technology

Ultraviolet light and moisture dual-curing polyurethane hot melt adhesive and preparation method thereof

The invention relates to the field of hot melt adhesives, in particular to an ultraviolet light and moisture dual-curing hot melt adhesive and a preparation method thereof. The ultraviolet light and moisture dual-cured polyurethane hot melt adhesive is prepared from the following raw materials in parts by weight: 20 to 50 parts of thermoplastic resin, 20 to 50 parts of polyester polyol, 5 to 35 parts of polyether polyol, 1 to 10 parts of trifunctional small molecular polyol, 1 to 10 parts of hydroxyl-terminated acrylate or amino-terminated vinyl monomer, 2 to 20 parts of polyisocyanate, 0.1 to 1 part of catalyst, 1 to 5 parts of photoinitiator, 0.2 to 2 parts of silane coupling agent and 0.2 to 2 parts of defoaming agent. The polyurethane hot melt adhesive containing double reaction groups of vinyl and isocyanate is prepared by reacting a vinyl functional monomer containing terminal hydroxyl or amino, polyester and polyether polyol with polyisocyanate. After the hot melt adhesive is applied, the molecular weight of the vinyl polymer in the product is further increased through ultraviolet irradiation to form a large-molecular-weight reticular high polymer to generate pressure sensitivity and better initial adhesion strength, so that the functions of quick positioning and no pressure maintaining are achieved.
Owner:COLLTECH DONGGUAN BONDING TECH CO LTD

Preparation method of foamed ceramic heat-preserving material

The invention relates to a preparation method of a foamed ceramic heat-preserving material. The preparation method comprises the following steps: 1) dissolving kaolin and an aminovinyl silane coupling agent in water, heating in a water bath, and ultrasonically dispersing to obtain a viscous liquid; 2) adding rinkolite powder and titanium dioxide powder and stirring and dispersing at a high speed to obtain dispersed mixed slurry; 3) adding sodium sulfate powder, ball-milling and pelleting to obtain mixed particles; and 4) ball-milling the mixed particles, a foamed ceramic blank and an inorganic foamer in the ball-mill, and finally carrying out high-temperature sintering. The material provided by the invention has the advantages that 1) kaolin is used as a functional modifier, so that the corrosion resistance and mildew prevention of the ceramic material can be improved, and meanwhile, kaolin also serves as filler to improve the mechanical strength of the foamed ceramic; 2) the used rinkolite powder is an environment-friendly new material; and as a solid-solid phase change energy storage material, the rinkolite powder has high-and-low-temperature resistance and can improve the heat efficiency of the foamed ceramic and reduce the contraction and expansion of the foamed ceramic, thus achieving the effects of light weight and good heat-preserving performance.
Owner:苏州远略知识产权运营有限公司

Environment-friendly non-autoclaved tubular pile water reducing agent and preparation method thereof

The invention discloses an environment-friendly non-autoclaved tubular pile water reducing agent characterized by comprising the following components in parts by weight: 10 to 20 parts of 1,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / 4,6-diamino-1,3,5-triazine-2-acetic acid polycondensate, 5 to 10 parts of 7-amino-3-vinyl-3-cephem-4-carboxylic acid / 4,4'-diaminostilbene-2,2'-disulfonic acid / polyethylene glycol monoallyl ether / 4-vinylphenylboronic acid copolymer, 1 to 3 parts of 9-fluorenecarboxylic acid, 0.3 to 0.6 part of an initiator, 2 to 5 parts of plant polysaccharide and 35 to 45 parts of water. The invention further discloses a preparation method of the environment-friendly non-autoclaved tubular pile water reducing agent. The environment-friendly non-autoclaved tubular pile water reducing agent disclosed by the invention is remarkable in water reducing effect, has the advantages of low dosage, excellent plasticizing performance, no obvious negative influence on the comprehensive performance of concrete, good energy-saving and environment-friendly performance in the preparation and use processes, high reaction activity, low reaction temperatureand capabilities of effectively enhancing the compressive strength, remarkable reduction of the hardening and viscosity of the concrete and improvement of the construction performance of the concrete.
Owner:赵良文

A kind of ultraviolet light and moisture dual curing polyurethane hot-melt adhesive and preparation method thereof

The invention relates to the field of hot melt adhesives, in particular to an ultraviolet light and moisture dual-curing hot melt adhesive and a preparation method thereof. The ultraviolet light and moisture dual-cured polyurethane hot melt adhesive is prepared from the following raw materials in parts by weight: 20 to 50 parts of thermoplastic resin, 20 to 50 parts of polyester polyol, 5 to 35 parts of polyether polyol, 1 to 10 parts of trifunctional small molecular polyol, 1 to 10 parts of hydroxyl-terminated acrylate or amino-terminated vinyl monomer, 2 to 20 parts of polyisocyanate, 0.1 to 1 part of catalyst, 1 to 5 parts of photoinitiator, 0.2 to 2 parts of silane coupling agent and 0.2 to 2 parts of defoaming agent. The polyurethane hot melt adhesive containing double reaction groups of vinyl and isocyanate is prepared by reacting a vinyl functional monomer containing terminal hydroxyl or amino, polyester and polyether polyol with polyisocyanate. After the hot melt adhesive is applied, the molecular weight of the vinyl polymer in the product is further increased through ultraviolet irradiation to form a large-molecular-weight reticular high polymer to generate pressure sensitivity and better initial adhesion strength, so that the functions of quick positioning and no pressure maintaining are achieved.
Owner:COLLTECH DONGGUAN BONDING TECH CO LTD

Wear-resistant flame-retardant automotive floor leather and preparation method thereof

InactiveCN111304931AAvoid the defects of weak bondingImprove adhesionRoad vehiclesTextiles and paperMethacrylatePolymer science
The invention discloses wear-resistant flame-retardant automotive floor leather. The wear-resistant flame-retardant automotive floor leather is characterized by consisting of a fiber cloth base layerand a wear-resistant flame-retardant surface adhesive layer, wherein the wear-resistant flame-retardant surface adhesive layer is prepared from the following raw materials in parts by weight: 20-30 parts of 2,4-diamino-6-vinyl-S-triazine/1-adamantyl methacrylate/3,4,5-trifluorocinnamic acid copolymer, 8-15 parts of hyperbranched polyurethane acrylate, 50-60 parts of 3,5-di(6-isocyanate hexyl)-2H-1,3,5-oxadiazine-2,4,6(3H,5H)-triketone/1,3-dihydroxy ethyl adamantane polycondensate, 3-5 parts of epoxy modified hexamethylene tetramine, 1-3 parts of black phosphorus, 10-15 parts of nano boron fibers, 1-3 parts of diamond, 1-3 parts of coupling agent, 3-6 parts of amino modified polysiloxane and 0.2-0.4 parts of azodiisobutyronitrile. The invention also discloses a preparation method of the wear-resistant flame-retardant automotive floor leather. The wear-resistant flame-retardant automotive floor leather disclosed by the invention is good in wear-resisting property, remarkable in flame-retardant effect, excellent in environment protection property and antibacterial property, light in weight, high in mechanical strength, good in aging resistance and weather resistance and long in service life.
Owner:朱冬梅

Continuous production method for recovering phenylacetic acid from 7-amino-3-vinyl cephalosporanic acid production wastewater

The invention discloses a continuous production method for recovering phenylacetic acid from 7-amino-3-vinyl cephalosporanic acid production wastewater. The method comprises the following steps: acidifying wastewater, extracting phenylacetic acid in the wastewater into an organic phase by using an organic solvent, stripping the organic solvent from the extracted wastewater, directly discharging the wastewater into a sewage station, washing the organic phase containing phenylacetic acid by using liquid caustic soda, and washing phenylacetic acid in the organic phase into water; and after the washing,recycling and reusing organic phase in the raw wastewater for phenylacetic acid extraction, after washing, acidifying water phase, and then performing cooling crystallization to recover phenylacetic acid. According to the process, the problem that phenylacetic acid is difficult to recover from the phenylacetic acid-containing wastewater can be solved, the recovered phenylacetic acid can be sold as a byproduct, and after the phenylacetic acid is recovered, the wastewater can be directly discharged to a sewage station after the organic solvent is stripped, so that the environment is protected, and certain economic benefits are generated.
Owner:山东普洛得邦医药有限公司 +1

Synthesis of hexavalent chromium imprinted material on graphene oxide-mesoporous silicon surface and its application in water treatment

The invention belongs to new materials and applications in the field of water treatment, and specifically relates to the preparation of a hexavalent chromium ion imprinted polymer and its application in treating water with hexavalent chromium. Traditional hexavalent chromium adsorption materials have low adsorption capacity, poor selectivity, long time, and are difficult to reuse. Therefore, the present invention prepares a new material for efficiently treating hexavalent chromium in water. The preparation method is: prepare graphene oxide by the improved Hummer method, and then load mesoporous silicon on the surface of graphene oxide to obtain a specific surface area of ​​about 780m 2 / g of graphene oxide-mesoporous silicon composite (GO-MS). With GO‑MS as carrier, hexavalent chromium ion as template, 3‑(2‑aminoethylamino)propyltrimethoxysilane as functional monomer and crosslinking agent, sol‑gel reaction was carried out at room temperature, and hydrogen Sodium oxide solution was used to elute the hexavalent chromium in the product, and then vacuum-dried. The material can selectively adsorb hexavalent chromium, reaching adsorption equilibrium in 30 minutes, with an adsorption capacity of 438 mg / g, and can be reused 5 times.
Owner:GUANGDONG UNIV OF TECH

Hydrogen sulfide corrosion inhibitor applied to thermal recovery of thickened oil and preparation method thereof

The invention relates to a hydrogen sulfide corrosion inhibitor applied to thermal recovery of thickened oil and a preparation method thereof, belonging to the fields of formulas and technologies of chemical agents used for oil fields. The corrosion inhibitor comprises the following components in percentages by mass: 15% to 30% of stearic acid, 14% to 24% of diethylenetriamine, 5% to 15% of thiourea, 1% to 6% of an NPC-9 type surfactant and 30% to 60% of a formaldehyde aqueous solution. The preparation method comprises the following steps: (1) adding stearic acid and diethylenetriamine into a xylene solvent, carrying out heating to 150 to 160 DEG C, carrying out stabilizing for 2 to 3 h, then carrying out heating to 190 to 200 DEG C, carrying out a reaction for 3 h, and carrying out cooling so as to obtain an imidazoline stearate intermediate; (2) adding the imidazoline stearate intermediate, diethylenetriamine and thiourea into the xylene solvent, carrying out heating to 100 to 130 DEG C, carrying out a reaction for 4 to 5 h, and carrying out cooling so as to obtain aminoethylene-thioureidoimidazoline; and (3) uniformly mixing the formaldehyde aqueous solution with the NPC-9 type surfactant under stirring, adding aminoethylene-thioureidoimidazoline, and carrying out uniform mixing so as to obtain a required corrosion inhibitor. According to the invention, the preparation method is simple; and the corrosion inhibitor has the advantages of good temperature resistance, good compatibility with an additive, good adsorption effect and good corrosion inhibition effect.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

A kind of preparation method of foam ceramic insulation material

The invention relates to a preparation method of a foamed ceramic heat-preserving material. The preparation method comprises the following steps: 1) dissolving kaolin and an aminovinyl silane coupling agent in water, heating in a water bath, and ultrasonically dispersing to obtain a viscous liquid; 2) adding rinkolite powder and titanium dioxide powder and stirring and dispersing at a high speed to obtain dispersed mixed slurry; 3) adding sodium sulfate powder, ball-milling and pelleting to obtain mixed particles; and 4) ball-milling the mixed particles, a foamed ceramic blank and an inorganic foamer in the ball-mill, and finally carrying out high-temperature sintering. The material provided by the invention has the advantages that 1) kaolin is used as a functional modifier, so that the corrosion resistance and mildew prevention of the ceramic material can be improved, and meanwhile, kaolin also serves as filler to improve the mechanical strength of the foamed ceramic; 2) the used rinkolite powder is an environment-friendly new material; and as a solid-solid phase change energy storage material, the rinkolite powder has high-and-low-temperature resistance and can improve the heat efficiency of the foamed ceramic and reduce the contraction and expansion of the foamed ceramic, thus achieving the effects of light weight and good heat-preserving performance.
Owner:苏州远略知识产权运营有限公司
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