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122results about How to "Improve the effect of surface modification" patented technology

Method for preparing ultrafine platy copper-zinc alloy powder

InactiveCN102151835AImprove qualityAvoid the unevenness of the powder surfaceHigh energyNitrogen
The invention relates to a method for preparing ultrafine platy copper-zinc alloy powder by using a horizontal stirring and grinding method, belonging to the technical field of preparation of metal powder material. The method comprises the steps of: mixing the copper-zinc alloy powder, grinding media and various grinding aids, putting the mixture into a sealed grinding bin of a horizontal high-energy stirring machine, introducing a protective atmosphere which mainly contains inert gas such as nitrogen and argon and the like, introducing water or oil with the temperature of 15-100 DEG C into a water cooling sleeve of a ball milling machine, controlling the rotating speeds at different stages, grinding, dispersing, modifying and grading the alloy powder to finally obtain copper alloy powder with the meshes of minus 300. In the method, the annealing process of the traditional method is abolished, and proper grinding process parameters are adopted, and the method has the advantages of short production process, high production efficiency, stable process and the like, and the prepared powder material has good platy effect and surface performance. The method also can be used for zinc-aluminum mixing ball milling and the production of powder such as zinc-aluminum alloy powder and the like, in which the degree of oxidation needs to be controlled.
Owner:KUNMING UNIV OF SCI & TECH

Preparation method and product of surface modified lithium battery high-nickel positive electrode material

The invention belongs to the field of secondary lithium ion batteries, and discloses a preparation method of a surface modified lithium battery high-nickel positive electrode material. The preparation method comprises the following steps: putting high-nickel positive electrode material into a reaction cavity of an atomic layer deposition system, and vacuumizing the reaction cavity for 5 to 10 s, so that the temperature of the reaction cavity is 140 to 160 DEG C; introducing a reaction source so that the pressure of the reaction cavity reaches 5 to 8 mbar; introducing N2 to take away redundant reaction source in the reaction cavity; introducing water to react with the reaction source, and carrying out surface deposition on the high-nickel positive electrode material to obtain an oxide film; introducing N2 to take away redundant water in the reaction cavity; and repeating the above steps to obtain the surface modified lithium battery high-nickel positive electrode material. The invention also provides the surface modified lithium battery high-nickel positive electrode material prepared by the method, and a positive electrode piece and a lithium ion secondary battery prepared from the material. The positive electrode material has the advantages of simple and practicable preparation method, easily controlled thickness for a cladding layer and the like, and is applicable for large-scale production.
Owner:HUAZHONG UNIV OF SCI & TECH

Surface modified lithium battery high-nickel anode material and preparation method thereof

The invention belongs to the field of lithium ion secondary batteries, and more concretely relates to a surface modified lithium battery high-nickel anode material and a preparation method thereof. The method includes the following steps: weighing a certain amount of transition metal salt and high-nickel anode material, preparing a transition metal salt solution, making the transition metal salt solution drip into the high-nickel anode material and drying the high-nickel anode material, immersing and drying the high-nickel anode material many times till the whole transition metal salt solution drip into the material, continuing drying the high-nickel anode material and grinding the material, processing the ground material in an air furnace, and finally obtaining the high-nickel anode material the surface of which is wrapped in transition metal oxides. The high-nickel anode material prepared from the above method is used for preparing lithium ion secondary batteries. The surface modified high-nickel anode material enables the first-circle efficiency and the cycle performance of a secondary battery to be greatly improved. Moreover, the preparation method is simple and feasible, the surface modified high-nickel anode material is low in cost and suitable for large-scale production, etc.
Owner:HUAZHONG UNIV OF SCI & TECH

Method for Improving the Electrochemical Performance of Hydrogen Storage Alloy Powder Using Electropolymerized Polyaniline

The invention relates to a method for improving the electrochemical performance of hydrogen storage alloy powder by utilizing electropolymerization polyaniline, and belongs to the technical field of the surface treatment of hydrogen storage alloy. The method comprises the following steps of: putting hydrogen storage alloy powder of which the granularity is between 100 and 400 meshes into mixed solution containing phenylamine and protonic acid in a certain ratio, and stirring uniformly at a speed of between 50 and 100 revolutions / minute, wherein the mass ratio of the hydrogen storage alloy powder to the mixed solution is 10 / 100-100 / 100; and applying direct-current voltage of between 1 and 2 V for 0.5 to 5 minutes by taking the hydrogen storage alloy powder as an anode and graphite as a cathode, so that the phenylamine performs electro-deposition polymerization reaction on the surface of the hydrogen storage alloy powder to form a polyaniline membrane layer. In the method, a polyanilinewrapped membrane with electrical conductivity and corrosion resistance is formed on surfaces of hydrogen storage alloy powder particles to improve the hydrogen storage capacity, high-multiplying power discharging performance and cyclic stability of the hydrogen storage alloy. The method has the characteristics of simplicity of operation, low production cost, obvious improvement effect and the like.
Owner:INNER MONGOLIA XIAOKE HYDROGEN STORAGE ALLOY CO LTD +1

Surface modified nanometer material serving as lubricating oil additive as well as preparation method and application thereof

The invention belongs to the technical fields of a nanometer material and lubricating oil, and discloses a surface modified nanometer material serving as a lubricating oil additive as well as a preparation method and an application thereof. The preparation method mainly comprises the following steps: putting a mixture of powder to be treated and a surface modification agent as well as grinding balls in a ball-milling tank of an improved dielectric barrier discharge plasma assisted mechanical milling device, feeding a discharge atmosphere medium, controlling the temperature of the ball-milling tank, adjusting discharge parameters, and starting the mechanical milling device so as to carry out dielectric barrier discharge plasma assisted mechanical milling, thus obtaining the surface modified nanometer material. The obtained powdery surface modified nanometer material can be added to the lubricating oil so as to improve the performance of the lubricating oil. The preparation method is simple to operate and good in controllability; the obtained surface modified nanometer material is small in particle size, high in activity, good in surface modification and extremely easy to deposit, flatly spread and diffuse on a mechanical friction surface and has excellent dispersion property in the lubricating oil, so that the friction of mechanical movement parts is reduced, and the worn surface is repaired.
Owner:麦卡伦(厦门)润滑油有限公司

Bovine serum albumin coated ferriferrous oxide nano-particle T1-MRI (Magnetic Resonance Imaging) contrast medium and preparation method thereof

The invention relates to a bovine serum albumin coated ferriferrous oxide nano-particle T1-MRI (Magnetic Resonance Imaging) contrast medium and a preparation method thereof. The method specifically comprises the following steps: (1) dissolving bovine serum albumin into secondary water A; ultrasonically dissolving to prepare a bovine serum albumin solution; (2) adding soluble ferric iron salts and soluble ferrous salts into secondary water B and dissolving to prepare an iron source solution; (3) putting the bovine serum albumin solution into an inert atmosphere and heating and stirring; adding the iron source solution into the bovine serum albumin solution to prepare a BSA-Fe precursor; and (4) raising the temperature to 50-100 DEG C and rapidly adding concentrated ammonia water, and reacting at a constant temperature for 5min-30min to prepare the bovine serum albumin coated ferriferrous oxide nano-particle T1-MRI contrast medium. Compared with the prior art, the preparation method is simple and the controllability is good; and obtained bovine serum albumin coated ferriferrous oxide nano-particles have the characteristics of good biocompatibility, easiness of being discharged out of a body, small toxicity and good T1 imaging effect.
Owner:SHANGHAI NORMAL UNIVERSITY

Graphene material directional arrangement and silica gel pad composite molding method and product

ActiveCN110157196AImprove thermal conductivityAvoid defects such as falling offVulcanizationHydrogen
The invention provides a graphene material directional arrangement and silica gel pad composite molding method and a thermally conductive silica gel pad product. A graphene powder material is wetted and dispersed and surface modified by adopting an organic volatilizable dilution solvent and a coupling agent. The obtained graphene dispersion liquid is added to the upper surface of a substrate pad in a spraying or coating mode. With volatilization of the organic dilution solvent, graphene can realize good directional arrangement, and excellent thermal conductivity and soaking performance of thethermally conductive pad are realized. Meanwhile, in a high-temperature vulcanization process, the coupling agent containing unsaturated groups adsorbed on the surface of graphene can generate crosslinking reaction with hydrogen-containing silicone oil and vinyl on the surface of the pad, thereby realizing firm connection between the graphene material and the raphene material directional arrangement and silica gel pad composite molding method and pad and solving the problems of defects such as insufficient strength, easy occurrence of falling off and the like in the bonding process of the graphene and the thermally conductive silica gel pad in the prior art.
Owner:中科热科技江苏有限公司

Catalytic ion reduction and anaerobic hydrolytic acidification cooperated industrial wastewater pretreatment method

The invention belongs to a wastewater treatment technology, relating to a method for coordinated pretreatment of nondegradable industrial wastewater by means of catalyzed iron reduction and anaerobic hydrolysis acidification. The method comprises the following steps: step 1, a catalytic iron filter material is prepared and pressed into a unitized catalytic iron filter material; step 2, a common anaerobic hydrolysis-acidification reaction tank is arranged; step 3, the catalytic iron filter material is put in the anaerobic hydrolysis-acidification reaction tank; and step 4, sewage is fed into the anaerobic hydrolysis-acidification reaction tank, flows through the catalytic iron filter material and is discharged, and the hydraulic residence time is between 3 and 8 hours for anaerobic hydrolysis-acidification reaction. The method not only removes poisonous functional group of poisonous contaminant so as to reduce the toxic action on anaerobe generated by the poisonous contaminant, but also hydrolyzes nonbiodegradable contaminant into easily biodegradable small molecular substance; therefore, the method improves the comprehensive biodegradability of wastewater, and has the advantages of high treatment efficiency and excellent treatment effect.
Owner:ZHENJIANG WATER IND CORP +1

Graphene-reinforced heat-conducting polymer composite material and preparation method thereof and heat-conducting product

The invention discloses a graphene-reinforced heat-conducting polymer composite material and a preparation method thereof and a heat-conducting product, relates to the technical field of heat-conducting materials, and is used for improving the dispersity of graphene in the graphene-reinforced heat-conducting polymer composite material, so that the graphene composite material has relatively good heat-conducting property. The preparation method of the graphene reinforced heat-conducting polymer composite material comprises the following steps: carrying out liquid-phase stripping on graphite to obtain a graphene dispersion liquid; mixing the first modifier with the graphene dispersion liquid by a mill to obtain modified graphene dispersion liquid; separating from the modified graphene dispersion liquid to obtain modified graphene; and carrying out melt blending on the modified graphene, a heat-conducting filler, a polymer matrix and a processing aid to obtain the graphene reinforced heat-conducting polymer composite material. The graphene-reinforced heat-conducting polymer composite material is prepared by the preparation method of the graphene-reinforced heat-conducting polymer composite material. The heat conduction material comprises the graphene reinforced heat conduction polymer composite material.
Owner:内蒙古信敏惠纳米科技有限公司

High-strength heat-conducting silica gel gasket and preparation method thereof

The invention discloses a high-strength heat-conducting silica gel gasket and a preparation method thereof, and the high-strength heat-conducting silica gel gasket is suitable for the fields of heat dissipation of new energy lithium batteries and the like. A carbon fiber powder material is wetted and dispersed and surface modified by adopting an organic volatilizable dilution solvent and a coupling agent. A carbon fiber dispersion liquid is brushed on the upper surface of a substrate gasket. With the volatilization of the organic dilution solvent, carbon fibers can be arranged parallel to theplane of the heat-conducting gasket, so that the high heat-conducting performance of the carbon fiber material along the fiber axial direction is exerted, and the gasket has a good heat equalizing function in the plane direction of the gasket. The directionally arranged carbon fiber material can play a role similar to skeleton strengthening and greatly improve the etching and tearing and other mechanical properties of the gasket. In the high-temperature vulcanization process, the coupling agent which contains unsaturated groups and is bonded on the surface of the carbon fibers by chemical bonds can generate crosslinking reaction with hydrogen-containing silicone oil and vinyl on the surface of the gasket, thereby realizing firm connection between the carbon fiber material layer and the gasket and facilitating subsequent calendaring processing.
Owner:中科热科技江苏有限公司
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