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85results about How to "Reduce embedding" patented technology

Hydraulic Fracturing Proppants

A method is given for treating a wellbore in a subterranean formation by hydraulic fracturing, slickwater fracturing, gravel packing, and the like, by using plate-like materials as some or all of the proppant or gravel. The plate-like materials are particularly useful in complex fracture systems, for example in shales. They may be used as from about 20 to about 100% of the proppant. Relative to conventional proppants, plate-like proppants demonstrate (a) enhanced crush resistance of the proppant due to better stress distribution among proppant particles, (b) diminished proppant embedment into formation fracture faces due to the greater contact surface area of proppant particles with the formation, (c) better proppant transport due to lower proppant settling rates, (d) deeper penetration into branched and fine fracture networks, and (e) enhanced proppant flowback control. Preferred plate-like proppants are layered rocks and minerals; most preferred is mica.
Owner:SCHLUMBERGER TECH CORP

Method for producing high performance lithium ion battery anode material LiFePO4/C

The invention relates to a preparation method for making lithium ion battery cathode materials of LiFePO4 / C by using the reducing agent and inorganic salts of iron source, phosphorus source, lithium source, carbon source and so on as raw materials. Adopt the combining method of sol-gel and microwave treatment and prepare ultrafine particles of LiFePO4 and carbon coat the particles at the same time. On this basis, change the property of LiFePO4 / C by metal doping of Cr3 plus , Co3 plus . By processing with industrial microwave oven of high power, the invention shortens processing time greatly, increases the yield remarkably, reduces material cost and energy loss, simplifies the processes, improves the efficiency of industrial production of lithium ion battery and is convenient for implementation in industry. Take it as cathode materials of lithium ion battery with high-rate discharge. The invention raises conductivity of lithium iron phosphate and at the same time improves charge discharge capacity and cycle numbers by carbon coating and metal element doping.
Owner:江苏君明高新科技有限公司

Film-coated modified propping agent, and preparation method and application thereof

The invention discloses a film-coated modified propping agent, and a preparation method and an application thereof. The film-coated modified propping agent is composed of a matrix and a resin layer uniformly coated out of the matrix, wherein the matrix is Hobq quartz sand; the resin layer is 1-10 wt% based on that of the matrix; and the resin layer comprises a resin binder and a curing agent, wherein the resin binder is bisphenol A epoxy resin, polyurethane resin or a combination thereof, the curing agent is an aliphatic polyamine curing agent an oralicyclic amine curing agent, and the usage amount of the curing agent is 10-50 wt% based on that of the resin layer. The preparation method of the film-coated modified propping agent is that the resin layer is coated on the outer surface of the matrix. The film-coated modified propping agent can be applied in fields of fracturing exploitation of oil and gas wells, is helpful to increase sand ratio and reduce usage amount of fracturing liquid, can effectively prevent backflow phenomenon, alleviates insertion of the propping agent, increases crack diversion capability, prolongs fracturing validity period, is helpful to increase oil output, reduces water yield and has significant meaning for solving the exploitation of low permeability oil field.
Owner:亿利沙材料科技有限责任公司

Foam dressing containing composite silver-zinc antibacterial material and preparation method of foam dressing

The invention provides a foam dressing containing a composite silver-zinc antibacterial material and a preparation method of the foam dressing. The foam dressing containing the composite silver-zinc antibacterial material comprises polyurethane foaming plastic and the composite silver-zinc antibacterial material, wherein the composite silver-zinc antibacterial material is adhered to the inside of the polyurethane foaming plastic, comprises the following raw materials in content: nano silver, nano zinc and a nano inorganic carrier; and the composite silver-zinc antibacterial material contains the following raw materials in percentage by mass: 10%-20% of silver and 20%-40% of zinc. The composite silver-zinc antibacterial material is dispersed into the foam dressing in a manner of foam molding or ultrasonic dipping together with foam. The foam dressing containing the composite silver-zinc antibacterial material is capable of effectively absorbing diffusate of the wound surface, and effectively inhibiting growth and breeding of staphylococcus aureus, pseudomonas aeruginosa and candida albicans.
Owner:SHENZHEN TSINGHUA YUANXING NANO MATERIAL CO LTD

Sandy conglomerate oil deposit fracturing crack control design method

The invention provides a sandy conglomerate oil deposit fracturing crack control design method, and belongs to the field of oil exploration. The method comprises the steps that 1, a sandy conglomerate oil deposit numerical model is built, then, sandy conglomerate oil deposit parameters and sandy conglomerate fracturing technological parameters are analyzed, and a sandy conglomerate multi-factor capacity model is built; 2, a sandy conglomerate oil deposit crack propagation model is built, wherein block physical property distribution rules are analyzed, statistical distribution rules are combined, and crack propagation morphological description is performed; 3, crack propagation simulation calculation is performed, and crack geometric parameters including crack length, crack height and crack width are obtained; 4, a sandy conglomerate crack control method is determined; 5, a calculation result obtained in the step 3 and the simulation result of the model in the step 1 are subjected to contrastive analysis, crack geometric parameters with the maximum yield in the sandy conglomerate multi-factor yield model in the step 1 are found, and crack design is completed.
Owner:CHINA PETROLEUM & CHEM CORP +1

Chemical mechanical polishing method and apparatus

In a CMP process for polishing copper and a barrier metal formed on a substrate to form a buried copper interconnect, a polishing pad is subjected to dressing under a dressing pressure of 29 g / cm<2 >so that the surface roughness of the polishing pad becomes 3 mum to 5 mum inclusive. Thereby, dishing of the copper interconnect can be reduced as compared with a known method without reducing the removal rate of the copper and barrier metal.
Owner:PANASONIC CORP

Method for achieving controller area network (CAN) bus network nodes

The invention discloses a method for achieving controller area network (CAN) bus network nodes. In a field programmable gate array (FPGA), a soft core driver connected with a soft core bus is adopted. The soft core driver is connected with a CAN drive software processor through a processor bus, and a CAN interface chip completing transmission of a single-ended signal to a CAN interface is connected between a CAN soft core controller end and a CAN bus. An interrupt request signal of a CAN soft core controller in the FPGA is transmitted to a processor interrupt tube pin connected behind a reverser through the reverser. The soft core controller transmits a soft core chip select signal generated by combining a 31st -bit to 8th -bit signal output by the CAN drive software processor and a chip select signal output by the CAN drive software processor into the CAN soft core controller. The soft core driver converts a processor bus interface into a soft core bus interface, and then transmission and receiving of CAN data of the CAN bus network nodes can be achieved through the CAN soft core controller. The method is simple in structure, flexible in design and suitable for a system composed of a processor and a field programmable gate array chip.
Owner:10TH RES INST OF CETC

Preparation method of organic nanocrystals

The invention disclose organic nanocrystals. According to the invention, an organic crystal raw material and a modification agent are dissolved in an organic solvent, and the mixture is well mixed by stirring; and the mixed solution is dropped onto a heating substrate for evaporation, such that organic nanocrystals are obtained. The method is called a rapid evaporation method. According to the method, crystal precipitation speed is high and there is no time for polymerization, such that nanocrystals appear, and microcrystal size distribution can be controlled within a range of 1-200 nanometers. Therefore, microcrystals with needed dimensions can be prepared according to actual requirements. With the organic nanocrystal rapid evaporation preparation method, organic crystal production cost is reduced, and organic crystal applications in optoelectronic application fields such as semiconductor manufacturing, optical communication, sensing imaging, sensing measurement, display, solid-state lighting, biomedicine, data storage, solar energy, optical interconnect, organic light-emitting diode, solar photovoltaic device, nano sensing, nano label, nanolithography and the like are expanded.
Owner:上海多磨新材料科技有限公司 +2

Ternary cathode active material of lithium ion battery, preparation method thereof, cathode material, lithium ion battery and product thereof

InactiveCN109119614AIncrease discharge densityStable structureCell electrodesGrapheneTin dioxideManganese
The invention provides a ternary positive electrode active material of a lithium ion battery and a preparation method thereof, a positive electrode material, a lithium ion battery and a product thereof, which relate to the technical field of ternary materials. The ternary cathode active material of a lithium ion battery comprises a nickel-cobalt-manganese cathode material, a nanometer tin dioxideand graphene oxide, wherein the nanometer tin dioxide is coated on the surface of the nickel-cobalt-manganese cathode material, and the nickel-cobalt-manganese cathode material coated with the nanometer tin dioxide on the surface is embedded in the graphene oxide laminated structure; the ternary cathode active material of the lithium ion battery alleviates the technical problems of poor rate performance and poor cycle performance of a traditional cathode active material. The invention also provides a preparation method of the abovementioned cathode active material, a cathode material, a lithium ion battery and a product thereof.
Owner:HUBEI UNIV OF ARTS & SCI

Application of taking oligopeptide and derivatives thereof as template molecule, and imprinting technology based preparation method of angiotensin synthetic receptor

The invention discloses an application of taking oligopeptide and derivatives thereof as a template molecule, and an imprinting technology based preparation method of an angiotensin synthetic receptor. The template molecule comprises any section of a peptide bond at a nitrogen end or a carbon end of an angiotensin II, and derivatives thereof, or any section of the peptide bond at the nitrogen end or the carbon end of an angiotensin I and the derivatives thereof. The application takes the template molecule as an imprint to prepare the angiotensin synthetic receptor; the angiotensin acceptor is prepared in a way that the template molecule, a function monomer, a cross-linking agent, a surface-active agent and the like are mixed according to a certain rate, and then an initiator is added. The acceptor is good in biocompatibility, can high selectively capture and neutralize the angiotensin II and the angiotensin I, and cuts off functions of the angiotensin II and the angiotensin acceptor (AT1) as well as functions of the angiotensin I and angiotensin converzyme (ACE), so as to control the blood pressure. The acceptor can be applied to separation, concentration and measuring of the angiotensin I or II.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Electrolyte of lithium ion battery adopting natural graphite as negative material

The invention relates to the technical field of electrolyte of a lithium-ion battery, in particular to electrolyte of a lithium ion battery adopting natural graphite as a negative material. The electrolyte comprises solute adopting lithium salt and an organic solvent for dissolving the solute, and a film additive which is beneficial to formation of a solid electrolyte film is added into the solvent. By adopting the technical scheme of the invention, the film additive which is beneficial to the formation of an SEI (Solid Electrolyte Interface) is added in the electrolyte, therefore, more stable SEI film can be formed on the surface of the natural graphite, the stability of the SEI film is improved, and the embedding quantity of solvent molecules is reduced.
Owner:DONGGUAN SHANSHAN BATTERY MATERIALS

Terminal application protecting method and device

The invention discloses a terminal application protecting method. The method comprises the steps that the application attributes of a terminal application are encrypted; the main logic of the terminal application is achieved through a programming language, and a decryption algorithm is packaged; when an instruction for starting the terminal application is received, the encrypted application attributes are called, the encrypted application attributes are decrypted, the decrypted application attributes are checked, and after the application attributes pass the check, the main logic of the terminal application is called. The invention further discloses a terminal application protecting device. According to the scheme, the terminal application can be effectively prevented from being tampered, and malicious advertisement embedment is reduced.
Owner:TENCENT TECH (SHENZHEN) CO LTD

Integral DOC catalyst for marine diesel engine tail gas purification and preparation process thereof

The invention relates to the technical field of marine diesel engine tail gas post-treatment, in particular to an integral DOC catalyst for marine diesel engine tail gas purification and a preparation process thereof. The integral DOC catalyst for marine diesel engine tail gas purification takes cordierite honeycomb ceramic as the carrier, in terms of 100% of the mass of the cordierite honeycomb ceramic, the active components loaded on the cordierite honeycomb ceramic carrier includes: greater than or equal to 3%wt of palladium, and greater than or equal to 6%wt of the sum of cerium oxide and zirconium oxide. The DOC catalyst can well adapt to the special work conditions of marine diesel engine tail gas treatment, and also can effectively improve the problems of catalyst poisoning, catalytic carrier channel blockage, and high sulfate content of the tail gas.
Owner:ZHEJIANG UNIV

Deep shale gas spiral type variable-parameter fracturing method

The invention discloses a deep shale gas spiral type variable-parameter fracturing method. The deep shale gas spiral type variable-parameter fracturing method comprises the following steps: (1) evaluating a pre-fracturing formation; (2) determining the position of a section shower hole and carrying out perforating operation; (3) determining a fracturing fluid system and a proppant; (4) optimizingfracture parameters and fracturing construction parameters; (5) carrying out acid pretreatment; (6) fracturing and injecting low viscosity quick water in a first stage; (7) fracturing and injecting medium viscosity quick water in the first stage; (8) fracturing and injecting a glue solution in the first stage; (9) after the pumping in the first stage is finished, stopping pumping for 5-10 min; and(10) carrying out fracturing and pumping in a second stage; and (11) carrying out displacing operation. The deep shale gas spiral type variable-parameter fracturing method disclosed by the inventionhas the advantages that the fullness of a small and micro-scale fracture can be furthest enhanced, and the reducing rate of the effective fracture volume with the time is reduced. Therefore, the long-time fracturing stable yield is increased.
Owner:CHINA PETROLEUM & CHEM CORP +1

Hydroxyl acrylic emulsion for water-based two-component anti-doodling anti-sticking coating and preparation method of hydroxyl acrylic emulsion

The invention relates to hydroxyl acrylic emulsion for a water-based double-component anti-doodling anti-sticking coating and a preparation method of the hydroxyl acrylic emulsion. The hydroxyl acrylic emulsion comprises a vinyl-containing polymerizable monomer, a hydroxyl acrylate monomer, a cross-linking monomer, polymerizable organic silicon, an emulsifier and the like. The hydroxyl acrylic emulsion with a core-shell structure is prepared by adopting a step-by-step emulsion polymerization method, and hydroxyl and organic silicon are simultaneously distributed on a shell layer of emulsion particles. The coating meets national standard requirements, has the characteristics of low VOC content, small smell, high crosslinking density, strong permeability resistance, good scratch resistance,low surface tension and the like, is applied to the fields of building outer walls, urban communal facilities and the like, and can achieve good anti-doodling and anti-sticking effects.
Owner:WANHUA CHEM GRP CO LTD +1

Method for purifying dimethyl sulfoxide

ActiveCN106674066AEliminate hidden dangersAchieve the effect of deacidification and water removalOrganic chemistryOrganic compound preparationPurification methodsDistillation
The invention belongs to the technical field of chemical reagent purification, and relates to a method for purifying dimethyl sulfoxide. Specifically, the method comprises the following steps of: 1) performing deacidification and dehydration; 2) performing reduced pressure distillation; 3) performing primary melting crystallization; and 4) performing secondary melting crystallization. The method is low in requirement on production equipment and easy in industrialization; compared with a common method, the method provided by the invention is capable of preparing a purified dimethyl sulfoxide product with satisfactory purity (greater than or equal to 99.99%) and relatively high yield (about 85%).
Owner:SINOPHARM CHEM REAGENT

Method for reducing embedding of sand blasting medium into electroplating steel surface

The invention relates to a method for reducing the embedding of a sand blasting medium into an electroplating steel surface. The method comprises the following steps: regulating air pressure; performing sand blasting on a steel workpiece; activating the workpiece subjected to the sand blasting, soaking the workpiece with cyanogen, electroplating, performing bright dipping, removing hydrogen, performing secondary activation, and passivating; the surface quality of the steel workpiece is improved; the probability of black spots on the surface of the steel workpiece is reduced; the quality of the workpiece is improved.
Owner:SHENYANG AIRCRAFT CORP

Fracturing method for reservoirs based on schistose propping agents and gas wetting reversal agents

The invention discloses a fracturing method for reservoirs (including hydrocarbon reservoirs, coal seams and so on) based on schistose propping agents and gas wetting reversal agents. When the fracturing method for the reservoirs is applied, schistose (including gangues, walnut shells and so on) propping agents with the total weight of the propping agents being 1.0%-99.0% are added to sand-carrying fluid, and others are traditional spherical (including quartz sand, ceramic particles, and so on) propping agents; gas wetting reversal agents which accounts for 0.0%-10.0% of the total weight of fracturing prepad fluid are added to the fracturing prepad fluid; and the wettability of the surfaces of the propping agents are changed into aerophily by adopting the gas wetting reversal agents, namely, gas wetting. According to the fracturing method for the reservoirs (including the hydrocarbon reservoirs, the coal seams and so on) based on the schistose propping agents and the gas wetting reversal agents, the gas extraction effect such as coal-bed methane wells or downhole hydraulic fracturing is improved through the fracturing method, fracturing fluid adding the gas wetting reversal agents,and the schistose propping agents, so that the flow conductivity of coal-bed methane is improved, and then the production of the coal-bed methane is increased effectively.
Owner:CHINA UNIV OF GEOSCIENCES (BEIJING)

High-rate long-cycle performance multi-element composite positive electrode material and preparation method thereof

The invention relates to a high-rate long-cycle performance multi-element composite positive electrode material and a preparation method thereof, wherein the positive electrode material is a hollow structural sphere with D50 of 2-7 microns, and the chemical formula of the positive electrode material is LixNiyCozMn1-y-zO2; the positive electrode material is internally doped with 0.02-1mass% of a Zcompound, wherein Z is at least one of Nb or Ta; an aluminum compound accounting for 0.01-1mass% of a matrix is coated on the surface of the positive electrode material; and in the chemical formula, x, y and z are the values of the molar ratio of the related elements, wherein x is greater than 0.9 and less than 1.3, y is greater than or equal to 0.2 and less than 1, z is greater than 0 and less than 0.5, and y+z is less than or equal to 1. By virtue of the hollow structure of the invention, the infiltration and liquid retention capability of the non-aqueous electrolyte can be enhanced, the path of lithium ion transmission can be effectively shortened, and an effective structure support is provided for high-current high-rate charge and discharge; and the hardness of the hollow sphere structure can be increased, the crystal lattice junction also can be stabilized, and meanwhile, the cycling performance of the material is greatly improved.
Owner:HENAN KELONG NEW ENERGY CO LTD

Vibration resistant flex flange ball stud

A ball stud (12) with a relatively short grip length, adapted for use with a turbocharger, having a flexible flange (18) extending from a center of the ball stud (12). The flexible flange (18) is between a ball section (14) and a first shaft portion (20) adjacent to the flexible flange (18) and preferably a narrower threaded shaft portion (22) extending further from the ball section (14). The first shaft portion (20) may be tapered to fit in a complementary aperture (32) of a plate (30). The flexible flange (18) preferably includes a narrow circumference (24) adjacent to a center of the ball stud (12) with a circumferential lip (26) adapted to engage a plate (30). The flexible flange (18) allows subtle flex for thermal expansion and essentially changes a spring rate of the ball stud (12) to emulate a longer fastener.
Owner:BORGWARNER INC

Hydraulic fracturing proppants

A method is given for treating a wellbore in a subterranean formation by hydraulic fracturing, slickwater fracturing, gravel packing, and the like, by using plate-like materials as some or all of the proppant or gravel. The plate-like materials are particularly useful in complex fracture systems, for example in shales. They may be used as from about 20 to about 100% of the proppant. Relative to conventional proppants, plate-like proppants demonstrate (a) enhanced crush resistance of the proppant due to better stress distribution among proppant particles, (b) diminished proppant embedment into formation fracture faces due to the greater contact surface area of proppant particles with the formation, (c) better proppant transport due to lower proppant settling rates, (d) deeper penetration into branched and fine fracture networks, and (e) enhanced proppant flowback control. Preferred plate-like proppants are layered rocks and minerals; most preferred is mica.
Owner:SCHLUMBERGER TECH CORP

Part mounting head, pick-up nozzle, pick-up nozzle manufacturing method

The present invention provides a component mounting head in which the suction and holding surface (14) of a component (1) of a suction nozzle (3) is formed of semiconducting ceramics, so that the component is in direct contact with the component during suction and holding. The suction holding surface has the characteristics of being a semiconductor, thereby preventing the disadvantages accompanying the generation of static electricity in the suction nozzle and the disadvantages accompanying the suction nozzle and the member being brought into an electrically conductive state .
Owner:PANASONIC CORP

Durable, antistatic and dustproof finishing agent for flocking fabrics and preparation method thereof

The invention discloses a durable, antistatic and dustproof finishing agent for flocking fabrics. The finishing agent is prepared by matching, by weight, 50-100 parts of methyl hydrogen silicone oil, 70-120 parts of allyl polyethoxy polypropoxy ether, 1.5-5 parts of vinyl trialkoxy silane and 0.1-0.16 part of chloroplatinic acid ethanol solution, making the materials subjected to addition reaction to obtain silicone oil co-modified by polyether and alkoxy, adding 480-820 parts of water for dilution and adding 10-20 parts of glyoxal aqueous solution and 400-500 parts of guanidine hydrochloride aqueous solution for mixing. The flocking fabrics finished through the finishing agent are soft and smooth in hand feel and have excellent antistatic properties, and the fabric surface is not prone to adsorb dust.
Owner:LIAONING FIXED STAR FINE CHEM

Negative electrode active material, and preparation method and application thereof

The invention relates to a negative electrode active material as well as a preparation method and application thereof. The negative electrode active material comprises an inner core and a carbon coating layer formed on the surface of the inner core, the inner core comprises nanometer silicon and a lamellar Mxene material, and the nanometer silicon is distributed on the surface of the lamellar Mxene material and / or between lamellas. The lamellar Mxene material disclosed by the invention is tightly combined with silicon and also has excellent combinability with a carbon coating layer, so that the conductivity of the silicon can be effectively improved, and de-intercalation and intercalation of lithium ions in the silicon are promoted; in addition, the lamellar Mxene material disclosed by theinvention is beneficial to surface layer adhesion of nano silicon, so that the nano silicon is uniformly dispersed in an Mxene material lamella; and finally, the lamellar Mxene material is combined with the carbon coating layer, so that excellent mechanical properties are achieved, and the stability of a composite structure is improved.
Owner:HUI ZHOU BTR NEW MATERIAL TECH

Capacitor touch screen manufacturing process

InactiveCN103440078AReduces the possibility of air bubblesGuaranteed service lifeInput/output processes for data processingAdhesiveEngineering
The invention discloses a capacitor touch screen manufacturing process. By digging a hole in OCA (Optical Clear Adhesive) and placing a button icon in the OCA, the process can realize embedment of the button icon, thereby greatly reducing the possibility of bubble generation during bonding and pressing, ensuring the service life of the products and having artistic product appearance; besides, the ITO (Indium Tin Oxide) Film is processed by mature laser process, so that the yield in volume production can be easily controlled.
Owner:GUANGDONG GREEN PRECISION COMPONENTS CO LTD

Preparation method of sol-gel molecularly imprinted microspheres for detecting melamine

The invention discloses a preparation method of sol-gel molecularly imprinted microspheres for detecting melamine. The preparation method adopts the following technology and the technology comprises the following steps: (1) preparing aminated SiO2 nanoparticles; (2) preparing a melamine molecularly imprinted material MEL-MIPs / SiO2. According to the preparation method, a sol-gel method is adopted,3-aminopropyltriethoxysilane is used as a functional monomer, tetraethyl orthosilicate is used as a crosslinking agent, hexadecyl trimethyl ammonium bromide is used as a pore-forming agent and a sodium hydroxide solution is used as an initiator to prepare imprinted microspheres MEL-MIPs / SiO2 which have a specific identification capability and are used for carrying out sensitivity detection.
Owner:TIANJIN POLYTECHNIC UNIV

Lithium-rich manganese-based cathode material with crosslinking structure and preparation method thereof

The invention relates to a lithium-rich manganese-based cathode material with a crosslinking structure and a preparation method thereof. The preparation method specifically comprises the following steps of (1) preparing a mixed reaction solvent of deionized water and organic alcohol; (2) mixing and dissolving soluble nickel, cobalt and manganese salts into the mixed reaction solvent; (3) heating the mixed reaction solvent to the reflux state by a microwave radiation manner; (4) under the continuous reflux state, adding an alkaline resource, and maintaining reaction, so as to obtain a nickel, cobalt and manganese hydroxide precursor; (5) fully mixing the nickel, cobalt and manganese hydroxide precursor and a lithium source, and calcining, so as to obtain the final lithium-rich manganese-based cathode material. The prepared lithium-rich manganese-based cathode material has the advantages that a crosslinking net-shaped structure is formed, the pore radius is rich, the crystallizing degreeis high, and the lithium ions are quickly disembedded and embedded at low resistance; the method for preparing the precursor of the lithium-rich manganese-based material is simple, the time is short,the organic solvent can be repeatedly recycled and used, the cost is reduced, the environment-friendly effect is realized, and the production efficiency is greatly improved.
Owner:安普瑞斯(无锡)有限公司

Nanosheet piled lithium iron phosphate/graphene composite material and preparation method thereof

The invention discloses a nanosheet piled lithium iron phosphate / graphene composite material and a preparation method thereof. The composite material is an anode material formed by compounding micron-level shuttle type particles formed by piling up nanosheet type lithium iron phosphate in situ with graphene. The preparation method comprises the following steps: 1, respectively dissolving a lithium source and an iron source in ethylene glycol; 2, dripping phosphoric acid and the lithium source-containing solution into the iron source-containing solution in sequence, and respectively adding ammonium persulfate and graphene oxide to form dispersion liquid; 3, transferring the dispersion liquid into a stainless steel reaction kettle with a polytetrafluoroethylene inner container, reacting at certain temperature for a period of time, naturally cooling to room temperature, respectively washing obtained precipitates with deionized water and absolute ethyl alcohol, performing centrifugal separation, and placing into a drying box for drying; 4, roasting an obtained precipitate sample under protection atmosphere, and performing furnace cooling to room temperature to obtain the nanosheet piled lithium iron phosphate / graphene composite material. The preparation method disclosed by the invention is simple in technological flow and low in cost, and the obtained anode material is excellent in electrochemical property.
Owner:CENT SOUTH UNIV

Full-aromatic phenol-amine copolymer containing multifunctional groups and preparation method and application thereof

The invention relates to a full-aromatic phenol-amine copolymer containing multifunctional groups and a preparation method and application thereof. The method comprises the steps that a phenylenediamine monomer solution reacts with a benzenediol monomer solution under the action of an oxidizing agent solution to obtain the full-aromatic phenol-amine copolymer containing the multifunctional groups, and the copolymer is used for adsorbing antibiotics in water. Compared with the prior art, copolymerization is performed on the benzenediol monomers and the phenylenediamine monomers to obtain the aromatic nucleus copolymer which contains a large number of amino groups, imine groups and hydroxyl groups and is rich in pi electrons, the copolymer can have an adsorption reaction with most organic substances, then the copolymer can efficiently remove the antibiotics such as ciprofloxacin in the water, and the ciprofloxacin removing rate can be more than 99 percent; the prepared full-aromatic phenol-amine copolymer containing the multifunctional groups has the advantages of being simple, convenient and efficient, low in cost and higher in yield and has the scale production potential, and the highest yield can reach 95.6 percent.
Owner:TONGJI UNIV

Preparation method of high-rate lithium ion ternary cathode material

The invention provides a high-power lithium ion cathode material and a preparation method thereof. The cathode material is LiaNixCoyMnzO2 (a is greater than or equal to 0.98 and less than or equal to1.10, x is greater than or equal to 0.4 and less than or equal to 0.95, y is greater than or equal to 0 and less than or equal to 0. 4, z is greater than or equal to 0 and less than or equal to 0.4, and x + y + z is equal to 1. The ternary hollow structural cathode material prepared according to the preparation method disclosed by the invention has a regular shape and narrow particle size distribution, and the structure can enhance the liquid retention ability for non-aqueous electrolyte, can effectively shorten a path of lithium ion transmission, and provides an effective support for high-current discharge and high-rate charge and discharge.
Owner:HENAN KELONG NEW ENERGY CO LTD
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