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46results about How to "Meet large-scale industrial production" patented technology

High-intensity high-hydroscopicity medical dressing containing carboxymethyl cellulose and preparation method thereof

InactiveCN103041437AReplace controllableThe degree of substitution is controllableFibre treatmentAbsorbent padsCarboxymethyl celluloseChemical adsorption
The invention provides high-intensity high-hydroscopicity medical dressing containing carboxymethyl cellulose and a preparation method thereof. The method comprises the following specific steps: preparing carboxymethyl cellulose non-woven fabric through two steps of alkali added aqueous medium process; combining the obtained carboxymethyl cellulose non-woven fabric with a non-woven fabric to form a unit through needling, so as to prepare the high-intensity high-water absorbability medical dressing containing carboxymethyl cellulose. The dressing has the advantages that the substituted ratio of the prepared carboxymethyl cellulose non-woven fabric is controlled among 0.1-.05, and the substitution is uniform; the space physical adsorption property of the carboxymethyl cellulose non-woven fabric is kept, and meanwhile, the chemical adsorption performance is improved; the obtained carboxymethyl cellulose non-woven fabric and the non-woven fabric are compounded to a unit, which improves the dryness strength of the dressing prepared by the invention, beautifies the appearance, and improves the hand feeling. Besides, the method is simple and convenient in preparation technology and lower in cost.
Owner:WUHAN TEXTILE UNIV

Ball grinder available for solid state reaction of powder

InactiveCN101823013AImprove mechanical energyMeeting the Energy Requirements of Solid-State Chemical ReactionsGrain treatmentsChemical reactionHigh energy
The invention relates to a ball grinder available for the solid state reaction of powder, which mainly comprises a ball grinding cylinder, an electromotor, a driving device, a grinding ball and a material inlet and outlet, wherein the horizontal type ball grinding cylinder is fixedly supported on a bracket; a jar is internally provided with the girding ball; the center of the ball grinding cylinder is provided with a rotatable main shaft; the main shaft is driven by the electromotor through the driving device to rotate; the main shaft is provided with a blade, wherein the rotating speed of the blade is 300-2000 r/min; the mechanical energy is transmitted to the grinding ball through the beating of the blade, so that the grinding ball can irregularly move with high speed; the bottom of theball grinding cylinder is in the shape of gradient with 0-30 degrees from the two ends to the center; the jar body of the ball grinding cylinder is provided with a cooling sleeve and an inlet and an outlet of cooling medium; and the jar body of the ball grinding cylinder is provided with an air exhausting opening and an air inlet. The ball grinder can lead the grinding ball to generate higher mechanical energy to provide high energy for inducing the solid state reaction among materials, thereby smashing, grinding and dispersing the materials and directly reacting to generate nanometer composite oxide.
Owner:BEIJING UNIV OF CHEM TECH

Nano linear calcium titanate and synthesis method thereof

The invention discloses nano linear calcium titanate and a synthesis method thereof. The synthesis method for the nano linear calcium titanate comprises the following steps of: 1) dispersing titanium dioxide in a strong alkali solution, and performing a hydro-thermal reaction with stirring to obtain a white deposit; 2) washing the white deposit by using water until the white deposit is neutral or weakly alkaline, dispersing the white deposit in a soluble calcium salt solution, controlling the temperature and the pH value of the system, and performing ion exchange reaction to obtain a calcium titanate deposit; and 3) performing centrifugal washing on the calcium titanate deposit until the calcium titanate deposit is neutral, and drying and baking the calcium titanate deposit to obtain the nano linear calcium titanate. The synthesis method for the nano linear calcium titanate is mild in reaction condition, simple in operation, rich in raw material source and low in cost, so that the synthesis method is suitable for mass production; and the synthesized nano linear calcium titanate is a solid alkali with a large specific area, has high ecological biocompatibility, and is expected to be applied in the fields of heavy metal ion contaminated waste water purification, ester exchange reaction catalysis, sclerous tissue repair and replacement and the like.
Owner:CENT SOUTH UNIV

Method for treating high-impurity lithium iron phosphate waste powder by using low-consumption phosphoric acid

The invention discloses a method for treating high-impurity lithium iron phosphate waste powder by using low-consumption phosphoric acid, which comprises the following steps of: pre-removing aluminum from lithium iron phosphate waste powder subjected to calcination treatment in an alkaline system, leaching aluminum-removed filter residues by using phosphoric acid and hydrogen peroxide, keeping the pH value at 2-3 all the time in the leaching process, selectively leaching Li, removing impurity copper and residual Al in the aluminum-removed filter residues to obtain FePO4 leaching residues, purifying the FePO4 leaching residues by adopting excessive phosphoric acid, supplementing a proper amount of Fe and an oxidizing agent at the same time, further removing impurities such as residual Cu, and converting hydroxyl iron phosphate generated in the selective leaching process into high-purity iron phosphate. The method is simple in process, suitable for treating high-impurity waste lithium iron phosphate powder obtained through disassembly, and capable of directly obtaining battery-grade iron phosphate and lithium phosphate. The method is easy to operate, the consumption of phosphoric acid as a leaching agent is low, the cost is low, the lithium recovery rate is high, and the iron phosphate is high in purity and meets the requirements of battery-grade iron phosphate.
Owner:ZHUZHOU SMELTER GRP

Finishing method of high water absorption hydrophilic nonwoven fabric for medical treatment

The present invention provides a finishing method of a high water absorption hydrophilic nonwoven fabric for medical treatment. The finishing method comprises: (1) low temperature plasma treatment: taking a nonwoven fabric base cloth, and carrying out low temperature plasma treatment on at least one surface of the nonwoven fabric base cloth, wherein the low temperature plasma treatment comprises: carrying out low temperature plasma treatment on the nonwoven fabric base cloth under a normal pressure by using N2, Ar or He gas as a working gas by using a ceramic electrode through dielectric barrier discharge; (2) online liquid injection: coating a fatty acid ester finishing liquid on the surface of the nonwoven fabric base cloth, and carrying out high temperature drying; and (3) cutting and packaging. According to the present invention, the method does not require the vacuum condition, can directly achieve the online liquid injection, and can directly perform the low temperature plasma treatment under the normal pressure without other additional equipment conditions; and the produced non-woven has characteristics of soft handfeeling and comfort, and can especially meet the high water absorption requirement in the medical industry, and the method can well meet the large-scale industrial production.
Owner:CHTC JIAHUA NONWOVEN CO LTD

Method for producing L-4-hydroxyisoleucine by microbial enzyme conversion method

The invention relates to a method for producing L-4-hydroxyisoleucine by a microbial enzyme conversion method. The method comprises the following steps: 1, culturing a mature bacterial strain; 2, grafting mature escherichia coli recombinant bacteria which are capable of inducing production of L-4-hydroxyisoleucine into a fermentation tank, and carrying out fermentation culture, wherein the temperature of the fermentation process is controlled in two stages, i.e., 4 to 36 DEG C in the earlier stage and 30 to 32 DEG C in the later stage; 3, collecting thallus after fermentation, adding phosphate buffer and washing, then adding alpha-oxoglutarate, isoleucine, ferrous sulfate, magnesium sulfate and ascorbic acid, and carrying out forced ventilation for catalysis; 4, removing bacteria from the catalytic liquid with a ceramic membrane, filtering with an ultrafiltration membrane, decoloring with activated carbon, desalting with faintly acid cation exchange resin, adsorbing effluent with 732 cation exchange resin and eluting with ammonia water, carrying out evaporation concentration and recrystallization to obtain the L-4-hydroxyisoleucine. The preparation method disclosed by the invention is simple and efficient in reaction system and simple and feasible in extraction process. The conversion rate is up to over 95.4 percent, and the purity of the product can reach over 98 percent.
Owner:HENAN JULONG BIOLOGICAL ENG CO LTD +1

Bioactive peptide and preparation method thereof

The invention discloses a bioactive peptide and a preparation method thereof. The preparation method comprises the following steps: using milk or casein as a raw material, selecting an appropriate protease, carrying out enzymatic hydrolysis under certain conditions, carrying out concentration by adopting a membrane technology, desalting the obtained concentrate in a reverse osmosis manner, and drying the desalted concentrate by adopting a vacuum freeze-drying technique or a low-temperature spray drying technique in order to prepare polypeptide powder rich in bioactive peptides; and screening the polypeptides having anticoagulation activity through molecular fishing, sequencing the screened polypeptides to obtain an amino acid sequence, and synthesizing the final highly-pure polypeptide product in a solid phase synthesis manner. An identification result shows that the angiotensin converting enzyme inhibition rate and the thrombin inhibiting peptide inhibition rate of the peptide disclosed in the invention are high, the angiotensin converting enzyme inhibition rate of 1 mg of antithrombotic peptide dry powder is 30-80%, and the thrombin inhibition rate of 1 mg of the antithrombotic peptide dry powder is 70-98%. The method for preparing the bioactive peptide from the milk or casein has the advantages of richness in the raw material, low price, and meeting of large-scale industrial production.
Owner:DALIAN POLYTECHNIC UNIVERSITY

Cassava degradable plastic as well as production process and production equipment thereof

The invention relates to the technical field of cassava degradable plastic as well as a process and equipment thereof, and in particular relates to a cassava degradable plastic as well as a production process and production equipment thereof. The cassava degradable plastic consists of the following components in percentage by weight: 75-91% of cassava starch, 5-20% of polyolefin, 0.5-2% of a catalyst, 0.5-2% of a coupling agent, 0.5-2% of an initiator and 1-3% of filler. The production process comprises the following steps: carrying out gelatinizing pretreatment, carrying drying pretreatment, then mixing and kneading powder at a high speed, reacting and extruding in a twin-screw extrusion reacting machine, and finally bracing, dicing, drying and sub-packaging to obtain the cassava degradable plastic. The cassava degradable plastic production equipment comprises a sieving machine for sieving the filler and a stirrer for mixing materials, and further comprises gelatinizing equipment for gelatinizing the cassava starch, a high-speed mixing and kneading machine, a twin-screw melting-extrusion reacting machine and a bracing and dicing device; the stirrer is connected to the high-speed mixing and kneading machine; the high-speed mixing and kneading machine is connected to the twin-screw melting-extrusion reacting machine; and the twin-screw melting-extrusion reacting machine is connected to the bracing and dicing device. The degradation rate can reach more than 85%.
Owner:DONGGUAN FANGZHONG SPORT PROD

Rolling method of biodegradable medical Zn-Li alloy

The invention discloses a rolling method of a biodegradable medical Zn-Li alloy and belongs to the technical field of biodegradable medical materials and metal rolling. The method includes: homogenizing alloy ingots: rising temperature to 200-280 DEG C at a speed of 2-6 DEG C per min, holding the temperature for 1-2h, rising the temperature to 300-380 DEG C at a speed of 0.5-1 DEG C per min, holding the temperature for 1-2h, and cooling along with a furnace; after alloy is preheated, hot rolling: putting the alloy back into the furnace and holding the temperature for 10-20min after the secondtime of rolling, and quenching in water after the fourth time of rolling, wherein rolling start temperature is 300-380 Deg C, press-down amount of each time of rolling is 25-40%, and rolling is performed for four times in total; warm rolling: rolling once, and quenching in water, wherein rolling start temperature is 60-250 DEG C, and press-down amount is 50-70%. Through a simple rolling process, the biodegradable Zn-Li alloy with high strength and high plasticity is obtained, the problem of low section plasticity caused by common plastic processing methods is avoided, and material using requirements of various human implantation devices are met. The method is low in cost and easy for large-scale production in factories, thereby having extremely high popularization value and extensive application prospect in the field of medical materials.
Owner:北京尚宁科智医疗器械有限公司

High-efficiency energy-saving cured carbon felt, and preparation method thereof

The invention discloses a high-efficiency energy-saving cured carbon felt, and a preparation method thereof. The high-efficiency energy-saving cured carbon felt is prepared from, by weight, 650 to 720parts of soft felt, 30 to 40 parts of a dilluent, 50 to 100 parts of a curing agent, 200 to 300 parts of a resin, and 25 to 35 parts of an inorganic filing material. The preparation method comprisesfollowing steps: 1, felt cutting; 2, rubber preparation; 3, rubber coating; 4, manufacturing and moulding; 5, high temperature oven drying; 6, machining; 7, coating; 8 high temperature calcining; and9, detection. The high-efficiency energy-saving cured carbon felt is low in thermal conductivity, excellent in thermal insulation performance, uniform in density, low in heat storage capacity, quick in degassing, low in outgassing amount in vacuum, possesses heat impact resistance; product pollution or hearth pollution is not caused; furnace body effective space is enlarged; installation and maintenance are convenient; thermal insulation requirements of various monocrystalline growth furnaces and polysilicon ingot furnaces are satisfied. The preparation method is simple, is suitable for largescale industrialized production, and is promising in application prospect.
Owner:NINGJIN JINGXING ELECTRONICS MATERIAL

A cassava degradable plastic and its production process and production equipment

The invention relates to the technical field of cassava degradable plastic as well as a process and equipment thereof, and in particular relates to a cassava degradable plastic as well as a production process and production equipment thereof. The cassava degradable plastic consists of the following components in percentage by weight: 75-91% of cassava starch, 5-20% of polyolefin, 0.5-2% of a catalyst, 0.5-2% of a coupling agent, 0.5-2% of an initiator and 1-3% of filler. The production process comprises the following steps: carrying out gelatinizing pretreatment, carrying drying pretreatment, then mixing and kneading powder at a high speed, reacting and extruding in a twin-screw extrusion reacting machine, and finally bracing, dicing, drying and sub-packaging to obtain the cassava degradable plastic. The cassava degradable plastic production equipment comprises a sieving machine for sieving the filler and a stirrer for mixing materials, and further comprises gelatinizing equipment for gelatinizing the cassava starch, a high-speed mixing and kneading machine, a twin-screw melting-extrusion reacting machine and a bracing and dicing device; the stirrer is connected to the high-speed mixing and kneading machine; the high-speed mixing and kneading machine is connected to the twin-screw melting-extrusion reacting machine; and the twin-screw melting-extrusion reacting machine is connected to the bracing and dicing device. The degradation rate can reach more than 85%.
Owner:DONGGUAN FANGZHONG SPORT PROD
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