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42 results about "Microcosmic salt" patented technology

Microcosmic salt (see infobox for other names) is a salt found in urine with the formula Na(NH₄)HPO₄. It is left behind in the residues after extracting the urea from dried urine crystals with alcohol. In the mineral form, microcosmic salt is called stercorite.

Preparation method of water-based compound rare earth nano La1-x-yCexTbyPO4 fluorescent particle for fingerprint manifestation

The invention discloses a water-based rare earth nano fluorescent particle for fingerprint manifestation and a preparation method thereof, belonging to the field of biomarkers. The water-based rare earth nano fluorescent particle comprises the following components of La1-x-yPO4:CexTby, wherein x=5-40 percent and y=5-25 percent. The preparation method comprises the steps of: weighting three rare earth inorganic salts according to a certain stoichiometric ratio, adding water for dissolving, and then dropping a sodium tripolyphosphate solution; then regulating the pH value to be equal to 7.0-11.0 by using an NaOH solution, controlling a bath temperature to be 30-100 DEG C, reacting for 1.5-3.5h to obtain a white suspension colloid; washing by using water and centrifuging to remove nitrate ions and excessive microcosmic salts; dissolving by using deionized water to obtain a transparent colloid solution; dropping a sodium hexametaphosphate solution as a stabilizing agent, stirring and standing for one night, then dropping a surface modifying agent to ensure that the mol ratio of the rare earth ions and the surface modifying agent is 1:(0.5-5); and regulating the pH value to be equal to 7.0-11.0 by using the NaOH solution, heating to 80-100 DEG C, stirring for 1-3h to form a rare earth complex with functional groups. The invention has simple process, low cost, better manifestation effect on fingerprints on the surface of a smooth object, and good application prospect.
Owner:BEIJING UNIV OF CHEM TECH

Polyacrylic acid-calcium phosphate composite nano-drug carrier and preparing method and application thereof

The invention relates to a polyacrylic acid-calcium phosphate composite nano-drug carrier and a preparing method and application thereof. The preparing method includes the following steps: (1) a microcosmic salt aqueous solution is rapidly poured into a calcium source aqueous solution, ammonium hydroxide is added to adjust the pH value, even stirring is carried out, and centrifugation washing is carried out after a reaction is carried out to obtain sediment; and (2) the sediment obtained in the step (1) is dispersed into deionized water again, polyacrylic acid is added, and stable polyacrylic acid-calcium phosphate composite nanoparticle suspension liquid is obtained through ultrasonic dispersion. The polyacrylic acid-calcium phosphate composite nano-drug carrier has the beneficial effects that the process is simple, raw materials are easy to obtain, the production process is environment-friendly and safe, the preparing period is short, and the overall process can be completed within one hour. The polyacrylic acid-calcium phosphate composite nano-drug carrier is good in biocompatibility, safe and free of toxic and side effects. Loading and slow releasing of a medicine can be achieved, the toxic and side effects caused by short-time high-concentration medicines can be avoided, and the using rate of the medicines can be improved.
Owner:WUHAN UNIV OF TECH

Method for manufacturing selective emitter structure with low surface concentration and soft doped zone

A method for manufacturing a selective emitter structure with low surface concentration and a soft doped zone includes the steps that (1) the surface of a substrate to be prepared is corroded and cleaned, and the surface of the substrate is completely dried after cleaning; (2) the clean substrate prepared in the step (1) is soaked in a solution with high oxidability to carry out wet chemical oxidation on the surface of a silicon wafer, and then the surface of the substrate is completely dried; (3) a microcosmic salt aqueous solution of 0.5-20% is deposited on the surface of the substrate in a spin coating and spraying mode, and then the surface of the substrate is dried; (4) phosphorus ink or silicon ink is deposited on an electrode area on the surface of the substrate coated with a phosphorus source in the step (3) in a screen printing mode, and then the surface of the substrate is dried; (5) the temperature of a diffusion furnace rises, nitrogen is introduced into a diffusion quartz tube, when the temperature reaches 780-890 DEG C, the clean substrate prepared in the step (4) is placed into a constant-temperature area of the diffusion quartz tube, a fire door of the diffusion furnace is sealed, and after the temperature of the diffusion furnace is stable, oxygen is introduced into the diffusion quartz tube; (6) the substrate is taken out and cooled after the diffusion process is over.
Owner:INST OF ELECTRICAL ENG CHINESE ACAD OF SCI +1

Method for preparing lithium iron phosphate anode material

The invention relates to a method for preparing a lithium battery material, and discloses a method for preparing a lithium iron phosphate anode material. The method comprises the following steps that(1) slurry preparing: ferric salt and microcosmic salt are added into aqueous alkali, and heating reaction is carried out to obtain ferro-phosphorus compound slurry; (2) wet ball-milling: dopant modifier, carbon source and lithium salt are added into the slurry, the wet ball-milling is carried out until the particle size is 50-150 nanometers; (3) spray granulation: spray granulation is carried outon the ball-milled slurry to obtain spherical precursor; (4) high temperature sintering: the spherical precursor is sintered under an inert atmosphere, and the lithium iron phosphate anode material is obtained after the temperature is cooled to a room temperature. According to the method for preparing the lithium iron phosphate anode material, the preparation technology is simple, the energy consumption is lower, the particle size of the lithium iron phosphate anode material is smaller, the distribution is even, the carton coating effect is good, the compacted density is high, the gram volumeis high, a lithium ion battery prepared with the material has better performance and high cost performance, and is the lithium iron phosphate anode material applied to practical production and application.
Owner:杭州金马新能源科技有限公司

Imine alkali metal salt and ion liquid as well as application thereof as non-water electrolyte

The invention discloses an application of imine alkali metal salt and an ion liquid as non-water electrolyte, and provides an ion liquid consisting of perfluoroalkyl sulfimide alkali metal salt with 'S-perfluoroalkyl sulfimide', perfluoroalkyl sulfimide anion with 'S-perfluoroalkyl sulfimide', as well as sulfonium salt, ammonium salt, microcosmic salt cation. According to the application, an intermediate fluoro-alkyl(S-perfluoroalkyl imino) sulfamide of perfluoroalkyl sulfimide is prepared by reacting (perfluoroalkyl sulfonyl)(perfluoroalkyl sulfinyl) imino with sulfur valence state of +4 and hydroxylamine oxygen sulfonic acid, the routes that fluoro-alkyl(S-perfluoroalkyl imino) sulfamide is prepared from (perfluoroalkyl sulfonyl)(perfluoroalkyl sulfinyl) imino through three steps of chlorination, fluorination and amination are effectively shortened, the operation is simple and convenient, the yield and the purity are high, the alkali metal salt has relatively good thermal stability and hydrolysis resistance, has high conductivity and oxidation potential in the conventional carbonic ester solution, and is good in compatibility with widely applied electrode materials, and the ion liquid can be applied to lithium ion batteries and carbon-based super capacitors.
Owner:HUAZHONG UNIV OF SCI & TECH +1

A magnetically responsive multi-gradient drug-loaded microsphere prepared by double in situ hybridization

The invention discloses a multi-gradient drug-loading microsphere having magnetic response and prepared through dual in-situ hybridization. According to the dual in-situ hybridization principle and the nano self-assembly technology, a bone repair drug-loading microsphere is developed; chitosan serves as an organic matrix, ferric chloride and ferrite serve as precursors of inorganic phase Fe3O4, and a calcium-microcosmic salt solution serves as a precursor of inorganic phase hydroxyapatite; a chitosan solution containing traditional Chinese medicine and icariin is fully and evenly mixed with the ferric chloride and the ferrite firstly, and then is evenly and fully mixed with soluble calcium salt, by means of a high-voltage static microsphere forming device, the mixture is dipped into an alkali liquor containing soluble phosphate drop by drop, the mode that organic macromolecules are adopted in biomineralization to control inorganic phase growth is simulated, the organic macromolecules become nuclear crystals on the organic matrix in a dual in-situ hybridization mode, and the multi-gradient drug-loading microsphere is prepared. The novel bone repair material is simple in preparation process, biocompatibility is good, and the capacity of controlling slow release of medicine is obviously enhanced through unique biological magnetic guide quality and multi-gradient performance.
Owner:FUZHOU UNIV
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