71results about How to "Good alcohol solubility" patented technology

The invention relates to a preparation method of alcohol soluble normal-temperature curing bi-component polyurethane-acrylate resin. The preparation method comprises the following steps of: preparing a substance A; preparing a substance B; and mixing the substance A and the substance B in the proportion of 3-6:1 to obtain the alcohol soluble normal-temperature curing bi-component polyurethane-acrylate resin, wherein the raw material substance A comprises acrylate, epoxy group monomer, vinylacetate or styrene, more than one type of active functional group monomer, initiating agent and industrial alcohol; and the raw material substance B comprises oligomer polyalcohol, polyisocyanate, chain extending agent, catalyst, polyamine, solvent and industrial alcohol. The alcohol is completely used as the solvent, and the alcohol solubility is favorable; compared with a bi-component polyurethane product, the components contain no toxic and dissociative isocyanate, and the obtained product has strong environmental adaptation, low requirements on moisture and interface cleaning degree, high drying speed after being coated, normal-temperature curing, good glossiness, large adjustable range of glass temperature and wide application range.

The invention discloses a method for blasting plant biomass walls with oxygen, comprising the following steps of: firstly, adding ethanol, hydrogen peroxide with concentration of 30% and water to crushed plant biomass, mixing the materials to oxidize and soak the materials, and conveying the oxidized and soaked materials to an oxygen blasting tank via a feeding port of the oxygen blasting tank; secondly, sealing the feeding port of the oxygen blasting tank, regulating the temperature of the gas in the oxygen blast tank at 80-150 DEG C and the pressure within 1-4 MPa by conveying pressure air to the oxygen blasting tank, preserving heat and keeping pressure for 20-200 seconds to soak the plant biomass into ethanol, hydrogen peroxide with concentration of 30%, steam and water; and finally, completely opening the discharge port of the oxygen blasting tank within 3 seconds to reduce the pressure in the oxygen blasting tank to the normal pressure. The invention aims to provide the method for blasting plant biomass walls with oxygen, which can be used for completely and uniformly decomposing the plant biomass and realizing industrialization production and has high production efficiency.

The invention discloses a method for producing a phloretin by an enzymatic hydrolysis method, which comprises the following steps of: dissolving phlorizin raw materials with the phlorizin quality content of 10 percent to 80 percent in deionized water; adding activated sino-beta hydrolytic enzyme, stirring and carrying out enzymatic reaction for 5-72 hours at 20-90 DEG C, wherein the weight ratio of the phlorizin raw materials to the sino-beta hydrolytic enzyme is 1-50:1; rapidly raising temperature to 60-100 DEG C for inactivating for 15-25 min; solid-liquid separating, drying the solid to obtain the phloretin. The phlorizin in plants is taken as raw material, and the method has the advantages of easy raw materials acquisition, low price, simple production process, and easy control. In the invention, an aglycon configuration obtained by enzymolysis is not damaged and has stronger biological activity; the enzymatic hydrolysis has strong specifity, and the products obtained have little impurities; because the phloretin obtained by the method is white, the application field of the phloretin is broadened.

The invention discloses an absorbable medical suture line with good mechanical performance. The absorbable medical suture line comprises, by weight, 100-120 parts of modified polylactic acid, 20-40 parts of polyglycollide, 4-6 parts of sorbitol, 3-5 parts of methyl methacrylate and 5-6 parts of cassia oil. The preparation method of the modified polylactic acid includes: in ice-bath, adding chitosan into perchloric acid, well mixing, dripping sorbic acid chloride, stirring, cooling, preserving heat and purifying to obtain modified chitosan; taking polyethylene glycol, feeding inert gas, heating, preserving heat until the polyethylene glycol melt, adding stannous chloride and lactide, well mixing, heating, preserving heat and stirring, and purifying to obtain intermediate material; dissolving the modified chitosan in mixed solvent, adding triethylamine, well mixing, heating, refluxing, adding the intermediate material, well mixing, continuing refluxing, purifying and drying to obtain the modified polylactic acid.

The invention discloses an alcohol-soluble molybdenum oxide interface layer material synthesis method and application. Metal molybdenum powder serves as the raw material, hydrogen peroxide serves as oxidant, organic acid is adopted as stabilizer and cosolvent, alcohol serves as a proton donor, and synthesized molybdenum oxide powder is of an amorphous structure. The invention further discloses an organic solar cell device with alcohol-soluble molybdenum oxide as an interface layer. Molybdenum oxide synthesized through the method is good in alcohol solubility and film forming performance, can evenly form a film on a transparent electrode and an organic active layer, can achieve low-temperature processing and is compatible with a flexible substrate. A molybdenum oxide modified anode interface layer can effectively achieve cavitation extraction, and greatly improves photoelectric efficiency of devices. Meanwhile, the stable material overcomes instability of electrode interfaces and organic layer interfaces to a certain extent, and accordingly stability of organic solar cells is improved.

A heterocyclic sulphonazo metal chelate compound and its preparation method. In a phosphoric acid system, getting a diazonium salt of a nitrogen heterocyclic aromatic amine by a mild diazotization method, the diazonium salt coupling with different components, and getting a series of heterocyclic sulphonazo compounds; the heterocyclic sulphonazo compound chelating with different bivalent metal to get a series of heterocyclic sulphonazo metal chelate compounds. The heterocyclic sulphonazo metal chelate compound could produce an excellent film by spin coating, and be used for the optical storagemedium for DVD-R. The compound has a low thermal decomposition temperature ( no more than 350degree C), which is advantageous for improving sensitivity of DVD-R dyes.

The invention relates to a temperature-sensitive gel type nano-silver foam aerosol for women, which comprises a gel system and a propellant dimethyl ether evenly mixed in the gel system, wherein the gel system contains nano-silver colloidal particles, a temperature-sensitive high molecular polymer and a diluting agent. The volume of the propellant the dimethyl ether is 8 to 15 percent of that of the gel system. An ejected matter is foam during the use of the temperature-sensitive gel type nano-silver foam aerosol, the deep administration can be performed, and a medicine can quickly swell and comprehensively contacts a focus after reaching the focus, and is dispersed evenly and permeated fully in a cavity; and at the same time, the nano-silver foam aerosol forms semisolid shaped gel in special physiological environment of a drug application position, has strong adhesiveness, is convenient for vagina mucosa to absorb to play effect, and effectively improves the compliance of patients and the bioavailability of nano-silver. The temperature-sensitive gel type nano-silver foam aerosol for the women has the advantages of convenient use, exact therapeutic effect, and no drug dependence.

The invention discloses a cashew amine epoxy curing agent for a marine heavy anti-corrosion coating. The curing agent is sequentially prepared from the following raw materials in parts by weight: 20 to 23 parts of cardanol, 1 to 1.2 parts of diethylenetriamine, 12 to 15 parts of 37 percent formaldehyde aqueous solution, 9 to 10 parts of diethylenetriamine, and 7 to 8 parts of 37 percent formaldehyde aqueous solution. According to the cashew amine epoxy curing agent for the marine heavy anti-corrosion coating, the raw material composition and the optimal proportion and the adding sequence of the raw materials are selected through a large quantity of experiments, and the proportion of each component is scientific and reasonable; acetal is catalyzed by adopting diethylenetriamine to control the viscosity parameter, and then Mannich addition is carried out on the periphery of molecules to improve the alcohol solubility; and the cashew amine curing agent prepared by the method is high in activity, viscosity and solid content and good in compatibility, does not release oil, and can overcome many defects of the cashew amine epoxy curing agent prepared by the method in the prior art.

A silver ion bactericide has a broad-spectrum antibacterial effect and avoids drug resistance as well as strain variation of microorganisms. Therefore, silver ions are currently an important research direction of the biomedical technology industry. According to the invention, an in-situ synthesis method is adopted for the first time to prepare a conductive conjugate polyelectrolyte / silver halide nanocomposite; and a long-acting broad-spectrum antibacterial effect is realized by adopting a silver halide nanocomposite taking the conductive conjugate polyelectrolyte as a carrier as a broad-spectrum antibacterial material and controlling the size of the silver halide nanoparticles complexed in the conductive conjugate polyelectrolyte to regulate the release rate of silver ions. In the invention, the application of the conductive conjugate polyelectrolyte in biomedicine and particularly the antibacterial field is exploited, and an antibacterial material which avoids toxic and side effects to a human body and is easy to spray and regulate and convenient to use is provided; and the antibacterial material has a broad application prospect in various conduits (catheters and air ducts), dressings and preparations as well as the long-acting mould and bacteria prevention of precise instruments.

The invention relates to a preparation method of a Chinese medicinal composition for nourishing blood, benefiting vital energy, regulating menstruation and dissipating cold. The Chinese medicinal composition is prepared by deer embryo, antler gelatin, prepared rehmannia root, ginseng, Chinese angelica, chuanxiong rhizome, bighead atractylodes rhizome, tuckahoe and liquorice. Compared with the prior art, the invention has obvious effect in the treatment, has fine production process, fast acting, increases new optional dosage form, removes the bad smell and improves the patient compliance.

The invention discloses an environment-friendly water-based coating for preparing glitter powder, and belongs to the field of fine chemical engineering. The coating consists of the following components in percentage by weight: 40-50% of alcohol-soluble acrylic resin, 15-22% of alcohol-soluble damar resin, 5-8% of a curing agent and 20-30% of an alcohol solvent. The invention also discloses a preparation method for the coating. The coating is capable of greatly improving the environmental performance by not using benzene solvents; moreover, the components are simple and synergetic with one another, so that the curing time is shortened, the adhesive force is strengthened and the total quality of the coating is improved. Compared with the traditional coatings, the cost of the coating is greatly reduced, the cost of the traditional coatings is about 25 yuan / kg and the cost of the coating is about 9.8 yuan / kg; the curing time of the traditional coatings is about 25-30s and the curing time of the coating is about 10-15s, so that the curing time is greatly shortened; the adhesive force is greatly strengthened; the preparation method is simple and the preparation cost is low.

The invention discloses alcohol-soluble polyamide resin for plastic printing ink and a preparation method thereof. The preparation method comprises: adding dimer acid and sebacic acid into a reactionkettle, introducing nitrogen gas, regulating a pressure, heating for 5min, then sequentially adding diamine, a molecular weight regulator, acetic acid and glycerin, warming, and carrying out pressure-maintaining stirring for 3 to 4h so as to obtain polyamide resin; then adding isophthalic acid, diphenolic acid and ethanol amine, regulating the pressure and temperature, stirring for 1 to 2h, then carrying out decompression, discharging water vapor, when the pressure is reduced to 1atm, stopping reaction, and cooling to obtain the alcohol-soluble polyamide resin. According to the alcohol-solublepolyamide resin for the plastic printing ink, which is obtained by adopting the preparation method disclosed by the invention, an acid value is smaller than 6KOHmg / g, an amine value is smaller than 6KOHmg / g, a softening point is 110 to 120 DEG C, and freezing resistance is qualified; the alcohol-soluble polyamide resin has excellent adhesive strength, gelling resistance, weather resistance and low-temperature stability.

The invention discloses an alcohol soluble high-ionic selective negative ion exchange membrane, a preparation method thereof and an application of the exchange membrane. A material of the ion exchangemembrane is a tadpole type poly phenylene oxide ionizer PPO-DMODA with a long hydrophobic alkyl side chain, ion selective permeability is 91%-97% at the indoor temperature within the range of ion-exchange capacity of 1.38-2.0meq / g, and sheet resistance is 3.5-30.6 omega / cm<2>. According to the preparation method, the long hydrophobic alkyl side chain is introduced on a PPO (poly phenylene oxide)framework, the method solves the problem of low zwitterion selectivity of the PPO-type negative ion exchange membrane under high IEC (ion-exchange column chromatography), a tadpole type poly phenyleneoxide ionizer structure with the long hydrophobic alkyl side chain can effectively restrain water absorbing swelling of the membrane, zwitterion selective permeability of the membrane and ionic conductivity are improved, the membrane has good mechanical property and performance stability, and requirements of electrodialysis and reverse electrodialysis processes for comprehensive performances of the negative ion exchange membrane can be met.

The invention discloses an alcohol-soluble beta-glucan extract, a preparing method and application thereof and health-care wine, and relates to the technical field of extraction of plant components. The preparing method of the alcohol-soluble beta-glucan extract comprises the steps of taking a medicinal material of hordeum vulgar L.var.nudumHook.f, adding an acid solution, and conducting acid extraction; adding alpha-amylase and glucoamylase into an acid extraction solution for enzymolysis, and then conducting enzyme denaturing to obtain an enzymolysis extraction solution; centrifuging and concentrating the enzymolysis extraction solution to obtain a concentrated solution; adding an ethanol solution into the concentrated solution for alcohol precipitation to obtain an alcohol precipitationsolution; filtering and drying the alcohol precipitation solution. The technology is simple, the operation is convenient, the production period is short, the efficiency is high, and the alcohol-soluble beta-glucan extract is suitable for industrial mass production; the alcohol solublility of the prepared alcohol-soluble beta-glucan extract is good, the alcohol-soluble beta-glucan extract can be dissolved into ethanol of different concentrations and is suitable for producing hordeum vulgar L.var.nudumHook.f beta-glucan products; the alcohol-soluble beta-glucan extract is applied to preparing the health-care wine; the health-care wind contains a large amount of hordeum vulgar L.var.nudumHook.f beta-glucan.

The invention relates to an inverted organic solar cell adopting a phthalocyanine derivative film as a cathode buffer layer and the preparation method thereof. Crystallization order degree of phthalocyanine derivatives used as buffer layer materials is effectively controlled by solvent steam annealing processing or transfer chamber airflow annealing processing, and roughness of a film surface is reduced, and then the synthetic method of the ionic phthalocyanine derivatives ZnPc(OC8H17OPyCH3I) is simple, and ethanol soluble performance is good, and therefore an environmental-friendly non-toxic harmless ideal cathode interface material is provided. The inverted structural device provided by the invention does not contain acidic hole transfer material PEDOT:PSS and a low power function metal electrode, and therefore the efficiency and the stability of the device are improved obviously. Compared with the prior art, the preparation method is novel, preparation technology is simple, and costs are low, and therefore the effective method of improving the performance of the solar cell is provided. The 80% efficiency of the prepared organic solar cell device is maintained after 500hours, and therefore the efficiency is higher than that of conventional devices.

The invention provides bio-based polyurethane water-based ink and a preparation method thereof. The preparation method comprises three steps of preparation of a prepolymer, emulsification desolvation and preparation of ink resin. The bio-based polyurethane water-based ink comprises the following components: bio-based isocyanate, bio-based macromolecular polyol, polypropylene carbonate polyol, a carboxylic acid type hydrophilic chain extender, a sulfonic acid type hydrophilic chain extender and a cross-linking agent, wherein the molar ratio of the bio-based isocyanate to the bio-based macromolecular polyol to the polypropylene carbonate polyol is 3:1:0.5-6:1:0.5, the mass of the carboxylic acid type hydrophilic chain extender is 1-2% of the mass of a polyurethane prepolymer, the mass of the sulfonic acid type hydrophilic chain extender is 2-6% of the mass of the polyurethane prepolymer, and the mass of the cross-linking agent is 1.5%-5.5% of the mass of polyurethane emulsion. According to the ink, the defect that inorganic auxiliaries such as matting powder need to be added to matte resin is overcome, the scratch resistance of the resin can be improved through the added cross-linking agent, and the alcohol solubility of the water-based ink resin is also improved through the addition of the polypropylene carbonate polyol.

The invention specifically discloses a preparation method of flower wine, which is prepared from 1-30kg of flower powder and 1000kg of wine by the following steps: (1) drying flowers at 35-90 DEG C until the water content is less than 3%, and crushing into 350-600-mesh powder to obtain the flower powder; (2) mixing the flower powder, saccharomycetes and water according to the weight ratio of 1: 0.25: 0.5, putting the mixture into a container, and fermenting at the temperature of 36-38 DEG C for 144-168 hours; (3) turning and stirring the fermentation material once every 3 hours in the fermentation process; (4) adding a proper amount of wine into the fermented material, mixing, and fermenting for 360 hours at the temperature of 18-25 DEG C; (5) stirring once every two hours in the fermentation process, wherein the stirring time is 5-8 minutes; (6) after fermentation is finished, carrying out reduced pressure distillation under the conditions that the pressure is-0.07 MPa to-0.1 MPa and the distillation temperature is 35-55 DEG C to obtain 10kg of alcohol liquid with the concentration of 15% V / V or above; and (7) adding 10kg of the alcohol liquid into 1000kg of wine, and uniformly stirring and mixing to obtain the flower wine. The wine is white spirit, yellow wine, grape wine or beer.

The invention relates to a star-like amphiphilic conjugated molecule material, and a preparation method and application thereof. The material adopts a fluorene structure as a skeleton, pyrene as a capping group and phosphonate as a polar side group and selects different alkyl chains, and the obtained star-like amphiphilic conjugated molecule compound has a structural general formula as shown in the following formula I: (the formula I is as shown in the specification), wherein R is one of alkyl, alkoxy, alkylphenyl and alkyl phenyl with phosphate; Ar is one of benzene, triphenylamine and tri-indene. The material has the advantages of simple chemical structure, low synthesis cost and the like, has high solution processability, film-forming property and multifunctional optical-electrical characteristic, and can realize high-brightness blue light emitting and efficient cathode interface modification functions simultaneously. An organic light-emitting diode which takes the material as a light-emitting layer and an interface modification layer simultaneously can realize excellent optical-electric characteristic through a simplified device structure and solves the technical problem that high-performance multi-layer devices are processed and manufactured by the solution.

The present invention discloses an ionic cathode buffer layer molecule type material, wherein an aryl phosphorus oxygen group is introduced into an ammonium radical ion salt, such that the alcohol solubility and the amorphous property are high, the solubility in the weakly polar solvent can be reduced, and the erosion of the weakly polar solvent can be resisted. The present invention further discloses a preparation method and applications of the ionic cathode buffer layer molecule type material. Compared with the existing organic small molecule cathode buffer layer material, the ionic cathode buffer layer molecule type material of the present invention is used in the multilayer solution processing inversion device structure.

The invention discloses a tobacco double-layer solid flavor ball preparation method and an application thereof. Colorless and transparent liquid polyethylene glycol with the molecular weight of 200-600 and white waxy solid polyethylene glycol with the molecular weight of 800-2000 are mixed, dissolved and then solidified in cold to form white pasty soft solid. One or a plurality of types of white solid polyethylene glycol with the molecular weight of 4000-10000 are mixed according to an optional proportion, dissolved and then solidified in cold to form white hard solid. The white pasty soft solid and the white hard solid serve as a ball core and a ball shell of a flavor ball respectively, the breakable structural characteristic of the flavor ball can be achieved, slight noise is generated when the flavor ball is broken, and participation and interestingness of a consumer smoking a cigarette are enhanced. The ball shell of the prepared flavor ball is compact in structure, flavors in the ball core can be effectively protected from volatilization, the structure of the ball core is loose when the cigarette is smoked and the flavor ball is broken, and the flavors can be taken out by smoke.

The invention belongs to the technical field of polymer materials, and in particular provides a block copolymer of polyalkylthiophene and alkyl phosphite alkyl thiophene, and a preparation method thereof. A polar phosphite group is introduced into a side chain of full-conjugated polyalkylthiophene block copolymer to prepare an alcohol / organic amphiphilic polythiophene high polymer material. The block copolymer has good alcohol solublility and workability; and in addition to the advantage of keeping the whole rigidity of a main chain, the block copolymer can conduct self-assembly into a variety of nanostructures, including fibrous and microphase separation structure, through simple regulation of the ratio of two blocks. These nanostructures help to improve the performance of organic / polymer optoelectronic devices, such as improvement of the efficiency of polymer solar cells. Therefore, the block copolymer provided by the invention can be used as a solar cell donor material.

An alcohol-soluble acrylic thermoplastic resin and a preparation method thereof. The resin comprises raw materials in the following weight ratio: 8-30 parts of methacrylate, 25-50 parts of acrylate, 10-20 parts of active functional group monomer, tertiary carbonic acid 2-5 parts of glycidyl ester, 2-5 parts of cationic functional monomer, 0.5-0.7 part of initiator, 10-15 parts of rosin addition polymer, and 0.2-0.5 part of catalyst. It has the characteristics of low pollution, low cost, good wetting and dispersibility of pigments, fast drying, and good printing suitability.

The invention discloses an ink suitable for tempered glass. The ink is prepared from 30-40 parts of multielement acrylate copolymer resin, 2-5 parts of polyketone resin, 3-5 parts of pigment, 1-3 parts of dispersing agent, 0.5-1 part of adhesion promoter, 0.2-0.4 part of chelator, 15-20 parts of ethanol, 1-3 parts of boron oxide, 1-3 parts of aluminum oxide, 1-3 parts of acid-resistant titanium oxide, 1-3 parts of alkali-resistant zirconium oxide, 1-3 parts of low-melting-point silicic acid, 40-50 parts of silicon rubber resin, 3-5 parts of amino resin dye, 1-4 parts of amino resin dye, 1-3 parts of amino resin dye, 50-60 parts of EVA (ethylene-vinyl acetate) resin liquid, 10-15 parts of butyl acetate, 0.2-0.5 part of defoaming agent, 2-3 parts of emulsifier and 6-10 parts of deionized water. The alcohol-soluble multielement acrylate used as the main body resin of the ink is matched with the special synthetic resins to be used for grinding the pigment, thereby enhancing the color developing property and flowability of the ink. The finally added accelerator and chelator enhance the adhesive force and heat resistance of the ink.

The invention provides (Z,E)-5-OH-3-(phenyl-derivative-methylene)-dihydroflavone-7-O-glucoside and a preparation method and application thereof; a structural general formula of the (Z,E)-5-OH-3-(phenyl-derivative-methylene)-dihydroflavone-7-O-glucoside is shown as in formula (I) shown in the description, wherein R1 may be -glucose, -[[6-O-(6-deoxy-alpha-L0mannopyranosyl)-beta-D-glucopyranosyl]oxy], -[[2-O-(6-deoxy-alpha-L-mannopyranosyl)-beta-D-glucopyranosyl]oxy], or 7-beta-D-glucopyranose acid, R2 may be -H, -OH, or -OCH3, R3 may be single group or multiple groups of -H, -OH, -OCH3, -O-glucose, -O-glucuronic, -O-neohesperidose, -F, -Cl, and -Br, and R4 may be single group or multiple groups of -H, -OH, -OCH3, -Cl, -Br, -NO2, -COOH, and methylenedioxy. Such compound has good antioxidant, anti-inflammatory, antibacterial, antivirus, anticancer and cardiovascular protection effects, and is widely applicable to the industries, such as food, cosmetics, and drugs.