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56results about How to "Excellent resistance to organic solvents" patented technology

Method for preparing negative photosensitive polyimide based on 2,2-di[4-(2,4-diaminophenyloxy)phenyl]hexafluoropropane

The invention discloses a method for preparing negative photosensitive polyimide which is based on 2, 2-bis<4-(2, 4-diaminophenoxy) phenyl> hexafluoropropane. The method takes the 2,2-bis<4-(2,4-diaminophenoxy)phenyl> hexafluoropropane and dihydric acid anhydride as raw materials for carrying out the polymerization reaction, hyper-branched fluoride-containing polyamic acid which takes the macromolecular chain end group as the anhydride group is obtained, the hyper-branched fluoride-containing polyamic acid is further reacted with p-hydroxyaniline or m-hydroxyaniline, hyper-branched fluoride-containing polyimide which takes phenolic hydroxyl as the end group by chemical imidization reaction is obtained, phenolic hydroxyl end-blocked fluoride-containing hyper-branched polyimide powder is obtained by precipitation, washing and vacuum drying process, and the hyper-branched fluoride-containing polyimide photosensitive material with the negative photosensitive performance is obtained by undergoing the functionalization after the dissolution. The material has high photosensitive performance, high resolution and excellent process, and the cured product has low water absorption, excellent heat resistance, dielectric performance and mechanical performance, thus having great application prospect in the field of electronic micro-electronics.
Owner:DONGHUA UNIV +1

Resin composition and organic-electrolyte battery

Provided is a resin composition having excellent adhesion to metals and high resistance to organic solvents. In particular, the resin composition is suitable for use as a sealing material for organic-electrolyte batteries which has excellent adhesion to terminals or current collectors constituted of a highly heat-resistant metal such as stainless steel or nickel, is less apt to deteriorate even upon contact with high-temperature organic electrolytes, and is less apt to affect the electrolytes. Also provided is a highly reliable organic-electrolyte battery in which the electrolyte is prevented from oozing out from the electrolyte layer by the action of the resin composition. The resin composition is characterized by comprising an epoxy resin (A) comprising an epoxy resin (E1) having an aromatic ring and an alicyclic skeleton and a latent hardener (B). The organic-electrolyte battery has a positive electrode comprising a current collector (13) and a positive active-material layer (2) electrically bonded to the surface thereof, a negative electrode comprising a current collector (13) and a negative active-material layer (6) electrically bonded to the surface thereof, and an electrolyte layer (7) disposed between the positive electrode and the negative electrode, the battery including a sealing part formed by tightly filling the gap between the peripheral edge parts of the two opposed current collectors (13) with a cured object (12) formed from the resin composition.
Owner:AJINOMOTO CO INC +1

Lithium ion battery safety coating and application thereof as well as lithium ion battery

The invention discloses a lithium ion battery safety coating. The lithium ion battery safety coating is prepared from a vinyl silane coupling agent, a binder and polyethylene microspheres through thefollowing steps: adding toluene and the vinyl silane coupling agent to the polyethylene microspheres, performing reflux reaction for 20-28 hours, filtering and drying to obtain polyethylene powder, and then mixing the polyethylene powder with the binder, sequentially stirring and dispersing to prepare a safety coating paste, and coating the safety coating paste to form a safety coating. The invention also discloses an application method of the lithium ion battery safety coating and a corresponding lithium ion battery. The safety coating disclosed by the invention has thermal blocking characteristics, can block the transmission of lithium ions in an electrolyte, ensures that side effects of heat production no longer occur, and improves the thermal stability of the battery; the safety coating has excellent organic solvent resistance characteristics and voltage resistance characteristics, and is applicable to the lithium ion battery; and the prepared lithium ion battery has the advantagesof high safety, no smoke, no fire, no combustion and the like.
Owner:WANXIANG 123 CO LTD +1

Thermosetting anti-welding printing ink with low dielectric constant and dielectric loss and preparation method of thermosetting anti-welding printing ink

The invention provides thermosetting anti-welding printing ink with low dielectric constant and dielectric loss and a preparation method of thermosetting anti-welding printing ink. The preparation method comprises the steps of reacting by virtue of long-carbon-chain aliphatic diamine monomers, aromatic diamine monomers with acid groups, aromatic dianhydride monomers with the acid groups and mono-anhydride monomers with the acid groups, cyclizing polyamide acid to obtain modified polyimide, and finally crosslinking modified polyimide with a hardening agent, so as to prepare the thermosetting anti-welding printing ink, wherein the dielectric constant of the thermosetting anti-welding printing ink is less than 3, the dielectric loss of the thermosetting anti-welding printing ink is less than 0.01, and the thermosetting anti-welding printing ink is applicable to high-frequency electronic equipment. Besides, tests show that the thermosetting anti-welding printing ink prepared by virtue of the preparation method has the characteristics of good electrical property, rupture resistance, welding resistance, warping resistance, flame resistance, acid resistance, alkali resistance and organic solvent resistance, low moisture rate and the like.
Owner:TAIFLEX SCI

Fluoride-free oil-proof paper as well as preparation method and application thereof

The invention belongs to the technical field of oil-proof paper, and discloses fluoride-free oil-proof paper as well as a preparation method and an application thereof. The preparation method of the oil-proof paper comprises the following steps: putting a sodium hydroxide/urea/water solution into a refrigerator for precooling, moving out the mixed solution, adding dissolved pulp, stirring the mixture at room temperature, and then placing the mixture into the refrigerator for freezing treatment; moving out the mixture after a period of time, and unfreezing the mixture at room temperature; carrying out centrifugal treatment, and collecting supernate to obtain a transparent cellulose coating; coating paper with the obtained cellulose coating, then soaking the paper in a coagulating bath, andcoagulating the coating for a period of time at a certain temperature; and drying the paper to obtain the fluoride-free oil-proof paper. According to the invention, a cellulose regeneration method isadopted to cover the surface of the paper, so that hydrogen bonds among cellulose are rearranged, pores are reduced, and the paper has good barrier property on grease, organic solvents, water vapor and the like. The fluoride-free oil-proof paper provided by the invention can be used in the field of food packaging, and has a good application prospect in preparation of disposable tableware.
Owner:SOUTH CHINA UNIV OF TECH

Aqueous polysiloxane resin and preparation method thereof

The invention discloses aqueous polysiloxane resin and a preparation method thereof. The aqueous polysiloxane resin is prepared from a pre-emulsion A, an emulsion B and a solution C as raw materials. The preparation method comprises the following steps: 1) preparing the pre-emulsion A; 2) preparing the emulsion B; 3) preparing the solution C; 4) pouring a part of the pre-emulsion A into a reaction container, dripping a part of the emulsion B, and at the same time heating the reaction container to 55-65 DEG C to react for 0.5-1 hour so as to prepare a light blue fluorescent seed emulsion; 5) simultaneously dripping the rest pre-emulsion A and the emulsion B into the fluorescent seed emulsion, heating to 55-65 DEG C to react for 2-3 hours, after the reaction is completed, cooling to the room temperature, adjusting the pH value to be 7-8, dripping the solution C, stirring for 10-30 minutes, and filtering, thereby obtaining a filtrate, that is, the aqueous polysiloxane resin. The aqueous polysiloxane resin is good in storage stability and flexibility, good in adhesion property, high in hardness and good in impact resistance, water resistance, salt water resistance, artificial aging resistance and chemical corrosion resistance. The aqueous polysiloxane resin is simple in preparation method, gentle in reaction condition and stable in process procedure.
Owner:WUHAN HOSTS COATING MATERIAL CO LTD

Processing method of molybdenum mineral dressing waste water

The invention discloses a processing method of molybdenum mineral dressing waste water. The processing method comprises following steps: 1, molybdenum mineral dressing waste water is introduced into apre-precipitation pool for precipitation so as to obtain pre-precipitation pool bottom sludge and a pre-precipitation pool supernatant; 2, the pre-precipitation pool supernatant is introduced into aflat ceramic membrane pool, and a flat ceramic membrane assembly is adopted for purifying to remove small particles and reduce the turbidity of produced water; 3, unfiltered waste water in the flat ceramic membrane pool is introduced into a reaction pool through a pipeline for reaction; and 4, waste water from the reaction pool is introduced into a precipitation pool for precipitation so as to obtain a precipitation supernatant and a precipitation pool bottom sludge. According to the processing method, the flat ceramic membrane is adopted for processing of molybdenum mineral dressing waste water, so that small particles can be removed with high efficiency, the turbidity of produced water is low, the technology is stable, waste water amount is reduced greatly, the adding amount of medicinesis low, operation cost is reduced greatly, precipitation pool equipment size and occupied land area are reduced at the same time, and investment cost is reduced.
Owner:SANDA FILM SCI & TECH XIAMEN

Supported catalytic filler and preparation method and application thereof

The invention discloses a supported catalytic filler and a preparation method and application thereof, belonging to supported catalytic fillers. The supported catalytic filler is provided with a filler carrier, a porous adhesive layer and a catalytic active component, and the catalytic active component fills in the pores of the porous adhesive layer or combined with the surface of the porous adhesive layer. The preparation method comprises the following steps: dissolving a porous structure medium in a pore-forming agent, adding a cross-linking agent to form an adhesive solution, dipping the filler carrier in the adhesive solution, taking out the filler carrier for curing to obtain a filler carrier containing a cured adhesive layer, removing the pore-forming agent in the adhesive layer, andcarrying out vacuum drying to obtain the filler carrier with a porous adhesive layer; and putting the filler carrier with the porous adhesive layer into a coupling agent solution, then putting the filler carrier with the porous adhesive layer into an aqueous PSS-Na solution, enabling PSS-Na to infiltrate into the micropores of the adhesive layer and to react with resin for combination, then putting the filler carrier into a dilute sulfuric acid solution for acidification, carrying out washing with water to remove residual acid, and carrying out vacuum drying to obtain the supported catalyticfiller. The prepared supported catalytic filler can be applied to a reaction separation process.
Owner:XIAMEN UNIV

A kind of aqueous polysiloxane resin and preparation method thereof

The invention discloses aqueous polysiloxane resin and a preparation method thereof. The aqueous polysiloxane resin is prepared from a pre-emulsion A, an emulsion B and a solution C as raw materials. The preparation method comprises the following steps: 1) preparing the pre-emulsion A; 2) preparing the emulsion B; 3) preparing the solution C; 4) pouring a part of the pre-emulsion A into a reaction container, dripping a part of the emulsion B, and at the same time heating the reaction container to 55-65 DEG C to react for 0.5-1 hour so as to prepare a light blue fluorescent seed emulsion; 5) simultaneously dripping the rest pre-emulsion A and the emulsion B into the fluorescent seed emulsion, heating to 55-65 DEG C to react for 2-3 hours, after the reaction is completed, cooling to the room temperature, adjusting the pH value to be 7-8, dripping the solution C, stirring for 10-30 minutes, and filtering, thereby obtaining a filtrate, that is, the aqueous polysiloxane resin. The aqueous polysiloxane resin is good in storage stability and flexibility, good in adhesion property, high in hardness and good in impact resistance, water resistance, salt water resistance, artificial aging resistance and chemical corrosion resistance. The aqueous polysiloxane resin is simple in preparation method, gentle in reaction condition and stable in process procedure.
Owner:WUHAN HOSTS COATING MATERIAL CO LTD
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