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33results about How to "Craft is easy to get" patented technology

Method for producing nickel-cobalt metal powder

The invention discloses a preparation method for nickel cobalt metal powders, which belongs to the technical field for preparation of non-ferrous metal metallurgy, powder metallurgy and material preparation. The preparation method is characterized in that nanometer or ultrafine nickel and cobalt metal powders is adopted as a seed crystal, which is mixed with ammoniacal water solution with nickel sulfate, cobalt sulfate, ammonia and ammonium sulfate, the preparation method adopts a hydrometallurgical hydrothermal hydrogen reducing technology and a device thereof, and the nanometer, ultrafine or tenuous nickel powder, cobalt powder and nickel cobalt alloy powder are prepared through the procedures such as ingredient, high-pressure hydrothermal hydrogen reduction, filtration, washing, drying and the like. The preparation method can be used for the field such as hydrogen storage alloy, galvanization, catalyst, sintering activating agent, magnetic materials, electric conduction slurry, battery materials, wave-absorbing materials, hard alloy, multi-layer porcelain capacitor, powder metallurgy and the like. The preparation method has the advantages of simple raw materials, simple process, short technological process, low manufacturing cost, controllable manufacturing process, high production efficiency, even graininess of metal powders, controllable size and composition and good quality of products.
Owner:张建玲

Improved method for preparing superfine high length-diameter-ratio anhydrous calcium sulfate crystal whiskers by using hydrothermal process

The invention discloses an improved method for preparing superfine high length-diameter-ratio anhydrous calcium sulfate crystal whiskers by using a hydrothermal process and belongs to the technical field of preparation of inorganic chemical materials. The improved method for preparing the superfine high length-diameter-ratio anhydrous calcium sulfate crystal whiskers by using the hydrothermal process takes calcium sulphate dihydrate as the raw material and comprises the following steps: firstly activating and roasting at the low temperature to prepare active calcium sulfate hemihydrates, subsequently doping, acidizing, hydrating and drying to prepare a quick-soluble calcium sulfate hemihydrates precursor with the structure defects; then adding the precursor into a saturated calcium sulphate liquid containing a chaotropic agent and a polar solvent, carrying out hydrothermal reaction at 100-200 DEG C for 2-20 minutes, cooling, filtering, washing and drying to prepare superfine high length-diameter-ratio calcium sulfate hemihydrate crystal whiskers with diameter of 0.005-10 microns, length of 10-5000 microns, length-diameter-ratio of 100-10000, and main content of greater than 95%; then mixing the calcium sulfate hemihydrates crystal whiskers with a trace solvent, roasting at 600-800 DEG C for 1-6 hours, cooling, filtering, washing and drying to prepare the superfine high length-diameter-ratio anhydrous calcium sulfate crystal whiskers with appearance which is as same as that of the calcium sulfate hemihydrates crystal whiskers and main content of greater than 95wt%. The improved method for preparing the superfine high length-diameter-ratio anhydrous calcium sulfate crystal whiskers by using the hydrothermal process is rapid and simple in process and low in costs; and the prepared superfine high length-diameter-ratio anhydrous calcium sulfate crystal whiskers can be used as reinforcement materials.
Owner:TSINGHUA UNIV

Microwave assisted extraction method of lemon essential oil

The invention relates to a microwave assisted extraction method of lemon essential oil. The extraction method comprises the following steps: (1) cleanly cleaning lemon peel, then, drying and crushing, so as to obtain lemon peel powder; (2) putting the lemon peel powder into a nonmetallic vessel, adding water and salt into the nonmetallic vessel, putting the nonmetallic vessel into a microwave extraction device, and then, heating materials in the nonmetallic vessel until the materials in the nonmetallic vessel are boiled; applying microwave radiation to the materials in the nonmetallic vessel after the materials in the nonmetallic vessel are boiled, and collecting generated vapor and condensing, so as to obtain crude lemon essential oil, wherein the manner of microwave radiation applying is intermittent; (3) separating water and impurities from the crude lemon essential oil, thereby obtaining the lemon essential oil. The extraction method disclosed by the invention has the advantages of environmental friendliness, rapidness, energy saving and the like, and is less in environmental pollution, easy in raw material obtaining, simple in process, convenient in operation, low in energy consumption, low in cost and high in efficiency; the prepared lemon essential oil is free from organic solvent residues and is high in quality and high in purity, and the natural quality of the lemon essential oil is kept.
Owner:广东添乐化妆品有限公司

Special catalyst for removing hydrogen sulfide through selective catalytic oxidation and preparation method for special catalyst

The invention provides a special catalyst for removing hydrogen sulfide through selective catalytic oxidation and a preparation method for the special catalyst, and belongs to the technical field of catalyst. A catalyst DXY-1 comprises the following components in percentage by mass: 25 percent of titantium oxide, 15 percent of aluminum oxide, 10 percent of iron oxide, 8 percent of boehmite powder, 5 percent of ferric citrate ammonium, 30 percent of silicon oxide, 5 percent of triamine citrate, 1 percent of sodium aluminate and 1 percent of aluminum sulfate; and A catalyst DXY-2 comprises the following components in percentage by mass: 32 percent of titanium oxide, 18 percent of aluminum oxide, 5 percent of palladium oxide, 3 percent of boehmite powder, 10 percent of ferric citrate ammonium, 25 percent of silicon oxide, 1 percent of lemon chrome, 1 percent of triamine citrate, 3 percent of sodium silicate and 2 percent of aluminum sulfate. The invention further provides a preparation method for catalysts DXY-1 and DXY-2. The catalyst provided by the invention is high in selection, gives priority to hydrogen sulfide removal, is wide in adaption, can be suitable for gas desulfuration with smallest hydrogen sulfide content being 3000ppm, and biggest hydrogen sulfide content being 100000ppm, and has relatively high catalytic efficiency.
Owner:CHANGCHUN DONGSHI TECH & TRADING INDAL

Absorbable spongy bone wax with hemostatic and bone healing promoting functions and preparation method of absorbable spongy bone wax

The invention discloses a preparation method of absorbable spongy bone wax with hemostatic and bone healing promoting functions. The preparation method comprises the following steps: uniformly mixingquaternized chitosan / modified starch composite microspheres with beta-tricalcium phosphate and a silk fibroin solution, and performing freeze drying to obtain the absorbable spongy bone wax. The absorbable spongy bone wax with hemostatic and bone healing promoting functions is prepared by combining a specific raw material ratio with a preparation process. Due to the fact that the raw materials have good biocompatibility and can be absorbed by the human body, the prepared spongy bone wax can be absorbed by the human body, residues are avoided, and bone wound healing is facilitated. Secondly, due to the action of the quaternized chitosan / modified starch composite microspheres, the bone wax has a good hemostatic effect, has certain antibacterial and anti-inflammatory effects, and has a good effect of promoting bone wound healing. Beta-TCP with bone induction and bone guidance effects is also added into the bone wax, so that the bone wax can promote repair of bone defect parts in bone wounds.
Owner:GUANGZHOU CHUANGSAI BIOLOGICAL MEDICAL MATERIALS CO LTD

Method for producing nickel-cobalt metal powder

The invention discloses a preparation method for nickel cobalt metal powders, which belongs to the technical field for preparation of non-ferrous metal metallurgy, powder metallurgy and material preparation. The preparation method is characterized in that nanometer or ultrafine nickel and cobalt metal powders is adopted as a seed crystal, which is mixed with ammoniacal water solution with nickel sulfate, cobalt sulfate, ammonia and ammonium sulfate, the preparation method adopts a hydrometallurgical hydrothermal hydrogen reducing technology and a device thereof, and the nanometer, ultrafine or tenuous nickel powder, cobalt powder and nickel cobalt alloy powder are prepared through the procedures such as ingredient, high-pressure hydrothermal hydrogen reduction, filtration, washing, dryingand the like. The preparation method can be used for the field such as hydrogen storage alloy, galvanization, catalyst, sintering activating agent, magnetic materials, electric conduction slurry, battery materials, wave-absorbing materials, hard alloy, multi-layer porcelain capacitor, powder metallurgy and the like. The preparation method has the advantages of simple raw materials, simple process, short technological process, low manufacturing cost, controllable manufacturing process, high production efficiency, even graininess of metal powders, controllable size and composition and good quality of products.
Owner:张建玲

Aluminum-doped zinc oxide film coating and nano-rod array material as well as preparation method thereof

The invention discloses an aluminum-doped zinc oxide film coating and nano-rod array material as well as a preparation method thereof. The aluminum-doped zinc oxide film coating and nano-rod array material comprises the components based on the weight percentage: 95-99% of zinc oxide and 1-5% of aluminum-doped quantity. The preparation method adopts a sol-gel method, zinc acetate and aluminium nitrate are added with organic solvent according to the proportion for heating under reflux; the mixed solution is then added with certain quantity of stabilizing agent for water bath heating at certain temperature and added with organic reagents such as absolute ethyl alcohol, methanamide or methanol and the like to prepare sol according to the need; after that, a spin coating method is adopted to form a film, and the aluminum-doped zinc oxide nano film coating material can be obtained by the processes such as drying, pretreating, repeatedly spin coating, annealing, secondary annealing under theatmosphere of hydrogen and nitrogen and the like; then, a hydrothermal method is adopted for preparing highly oriented aluminum-doped zinc oxide nano-rod and array thereof. The invention has high utilization rate of the raw materials, low cost and simplified preparation technique, and can control the performance and the particle size of the material from the molecular design level.
Owner:CENT SOUTH UNIV

Dilute sulfuric acid and graphene oxide co-doped modified titanium dioxide composite material and preparation method and application thereof

The invention discloses a dilute sulfuric acid and graphene oxide co-doped modified titanium dioxide composite material and a preparation method and application thereof. The preparation method comprises the following steps: (1) adding tetrabutyl titanate into ethanol to form a solution A, (2) preparing an ethanol-sulfuric acid solution to form a solution B, dropwise adding the solution B into thesolution A, and uniformly stirring to obtain a mixed solution, (3) reacting at constant temperature to obtain slurry, (4) centrifugally separating the slurry, and washing, drying and grinding to obtain powder, (5) calcining to obtain sulfuric acid-titanium dioxide, (6) preparing a graphene oxide dispersion liquid, (7) adding sulfuric acid-titanium dioxide into the graphene oxide dispersion liquidfor a reaction to form a suspension liquid, (8) carrying out constant-temperature reaction on the suspension to obtain a crude product, and (9) washing and drying the crude product to obtain the composite material. The preparation method is simple, low in cost and suitable for large-scale production. The prepared composite material is high in purity, can efficiently degrade tetracycline hydrochloride, and has good application value in the aspect of environmental pollution remediation.
Owner:WUHAN UNIV OF SCI & TECH
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