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122results about How to "Easy to disperse evenly" patented technology

Preparation method of micro-nano tin dioxide solid spheres

The invention relates to the preparation of micro-nano materials, and aims to provide a preparation method of micro-nano tin dioxide solid spheres. The method comprises the following steps: respectively preparing a SnCl4.5H2O aqueous solution and a NaOH solution, uniformly dropwise adding the NaOH solution into the SnCl4.5H2O aqueous solution, and stirring at a high speed; transferring the mixed solution to a polytetrafluoroethylene reaction kettle, and carrying out a hydrothermal reaction on the mixed solution; carrying out centrifugal separation or filtering on the obtained product, washing the obtained object until no soluble ion exists in the solution, and drying, so that white powder is obtained; and putting the powder into a chamber electric furnace or a muffle furnace to calcine, and carrying out furnace cooling on the obtained product, so that white or light yellow powder, namely, micro-nano tin dioxide solid spheres, is obtained. Products prepared according to the preparation method disclosed by the invention are good in sphericity, smooth in surface, and uniform in size; no organic solvent as well as volatile poisonous gas and the like is used in the preparation process, so that only do sodium salts exist in products, and therefore, the product has no pollution to the environment; and no template is used, so that the method is simple in process, easily controlled in reaction process, mild in reaction condition, simple in raw material and low in cost, and therefore, the method is specially suitable for large-scale industrial production.
Owner:ZHEJIANG UNIV

Suspension preparation of temperature change painless nano sulfadiazine metallic compound hyaluronic acid

The invention discloses a suspension preparation of temperature change painless nano sulfadiazine metallic compound hyaluronic acid. The formula comprises a sulfadiazine metallic compound, a hyaluronic acid substance, an analgetic, a dispersing agent aid, a suspension aid and water, wherein the sulfadiazine metallic compound comprises sulfadiazine silver and sulfadiazine zinc; the hyaluronic acid substance is sourced from biological fermentation and animal tissue extraction and the like and can be hyaluronic acid or hyaluronate or crosslinked hyaluronic acid or crosslinked hyaluronate; the analgetic comprises ropivacaine, bupivacaine, levobupivacaine, lidocaine and other local anesthetics or combination of the local anesthetics; the dispersing agent aid comprises chlorhexidine, Tween series, oleic acid or sodium oleate; the suspension aid can comprise glycerinum, celluloses, poloxamer series and hyaluronic acid substances. The suspension preparation is mainly used for burn, scald or the surface of a wound caused by explosion or anabrosis, has the main clinical characteristics that pain is rapidly relieved, the surface of the wound is subjected to rapid film formation and rapid healing of the wound is promoted, and the conventional main administration modes refer to spraying, smearing and coating.
Owner:LIPONT PHARMA

In-situ reaction forming device for differential and integral calculus laminated polymer composite material and in-situ reaction forming method

The invention relates to an in-situ reaction forming device for a differential and integral calculus laminated polymer composite material and an in-situ reaction forming method. The device comprises a plasticizing feeding device, a flow collector, a laminator and a forming device which are sequentially in series connection from front to back. Methods for processing a base layer and an adhesive layer in the differential and integral calculus laminated polymer composite material are unchanged, a functional layer is made of monomer or low polymer and the like which serve as raw materials instead of traditional high polymer, and a vacuum reactor is used as the plasticizing feeding device, so that the problem of difficulty in differential and integral calculus laminated composite of the composite material with base layer materials with low processing temperature is solved. By the aid of in-situ reaction forming technology for the functional layer, corresponding polymer modified auxiliaries can be selected according to different base materials, modifying effects are remarkable, the functional layer is thinner and even far thinner than the base layer, and raw materials are saved. Moreover, negative effects of high time consumption, degradation and the like caused by repeated hot processing are avoided as the functional layer is polymerized at one step.
Owner:BEIJING UNIV OF CHEM TECH

Electroconductive woodceramic powder and its manufacturing method

InactiveCN102515778AWith electromagnetic shieldingChange the amount of platingCeramicwareChemical platingFiltration
Relating to woodceramic materials and their preparation methods, the invention provides electroconductive woodceramic powder and its manufacturing method, and solves the technical problems of great brittleness and easy cracking in bulk woodceramic materials. The electroconductive woodceramic powder of the takes woodceramic powder as the core, the surface of which is chemically plated with electroconductive powder of a layer of metal film, and the metal attaching amount is 1%-50% of the mass of the woodceramic powder, wherein, the metal is nickel, iron or cobalt. The preparation method consists of: subjecting the woodceramic powder to oil removal, oxidation, sensitization, activation, and dispergation, then placing the woodceramic powder into a chemical plating solution for chemical plating, and conducting filtration and washing by deionized water to neutral, then carrying out drying, thus obtaining the electroconductive woodceramic powder with volume resistivity of 4.5*10<-2>omega.cm-5.5*10<-1>omega.cm. The electroconductive woodceramic powder in the invention can be added into coatings for preparing electroconductive coatings, or the powder can be added into resin-based materialsfor preparing molding materials, thus having a wide application range. The electroconductive woodceramic powder in the invention can be used as an electromagnetic shielding material.
Owner:NORTHEAST FORESTRY UNIVERSITY

Preparation method and application of Co/Ni and aluminum pyrophosphate composite hollow microsphere

The invention relates to a preparation method of a Co / Ni and aluminum pyrophosphate composite hollow microsphere. The preparation method comprises the following steps of: preparing a mixed water solution A which contains 10wt%-25wt% of cobalt salt and 1wt%-3.5wt% of nickel salt; preparing a mixed water solution B of aluminum salt and phosphate; preparing a mixed water solution C of vinylamine and carbamide; firstly adding the mixed water solution B to a reaction kettle, then simultaneously adding the mixed water solution A and the mixed water solution C to the reaction kettle, and reacting to obtain a Co / Ni hydroxide and aluminum phosphate composite microsphere; filtering, washing, drying, and then calcinating to obtain a CoO / NiO and aluminum pyrophosphate composite hollow microspher; reducing the CoO / NiO and aluminum pyrophosphate composite hollow microspher by using H2 or CO to obtain the Co / Ni and aluminum pyrophosphate composite hollow microsphere. The whole preparation process flow is simple and can be put into industrial production easily. The prepared Co / Ni and aluminum pyrophosphate composite hollow microsphere is used for catalyzing ammoniation and hydrogenation of IPN (Interpenetrating Polymer Network) to prepare IPDA (Isophorone Diamine), is high in catalysis efficiency and has the IPDA selectivity being higher than 98%.
Owner:WANHUA CHEM GRP CO LTD +1

Polyvinylidene fluoride hollow fiber porous membrane and preparation method thereof

The invention belongs to the technical field of polymer material preparation, relating to an increased polyvinylidene fluoride hollow fiber porous membrane and a preparation method thereof. The preparation method comprises the following steps: dispersing powdery saccharide compounds in organic solvent first and dissolving polyvinylidene fluoride with the solvent to form casting film polymer solution; and preparing a hollow fiber by a gelling phase inversion method; retaining powdery materials in a solid while using a precipitated medium to solidify polymer, and dissolving a saccharide powderymaterial by a hydrolysis method to retain a micropore structure; and controlling the molecular weight of powdery saccharide compounds and the size and quantity of powder particles to obtain films withdifferent apertures and porosity factors. The formula of polymer solution comprises the following components in percentage by weight: 15-30 percent of polyvinylidene fluoride, 40-75 percent of organic solvent and 10-30 percent of powdery saccharide compounds; and the invention has simple and easily-controllable process steps, reasonable film pore size, excellent film structure, favorable performance and low preparation cost and is suitable for industrial production.
Owner:QINGDAO SEACON WATER SERVICE TECH

High-heat-conductivity high-molecular polymer composite heat-conducting material and preparation method thereof

The invention discloses a high-heat-conductivity high-molecular polymer composite heat-conducting material and a preparation method thereof, and relates to the technical field of heat-conducting materials, and the high-heat-conductivity high-molecular polymer composite heat-conducting material is obtained by adding an Ag/MXene sheet composite material into a high-molecular polymer heat-conducting material matrix; the invention also discloses a preparation method of the high-heat-conductivity high-molecular polymer composite heat-conducting material, which comprises the following steps: dispersing the Ag/MXene sheet composite material into an organic solvent, then adding into a polyurethane prepolymer, and heating, stirring and dispersing in a protective atmosphere; and adding polyisocyanate and a catalyst into the reaction system, heating, stirring for reaction, removing bubbles from the mixed material, pouring into a mold, and curing, thereby obtaining the product. The Ag nano particles and the two-dimensional MXene sheet material have a synergistic effect in heat conduction performance, the Ag/MXene sheet composite material is added into a high-molecular polymer heat conduction material matrix such as polyurethane, the heat conduction performance of the material can be remarkably improved, and the material can be applied to an electronic packaging material; and the preparation method is effective, controllable, economical and environment-friendly.
Owner:ANHUI UNIVERSITY
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